scholarly journals Novel Microwave-Assisted Method of Y2Ti2O7 Powder Synthesis

Materials ◽  
2020 ◽  
Vol 13 (24) ◽  
pp. 5621
Author(s):  
Vladimir Chishkala ◽  
Serhiy Lytovchenko ◽  
Bohdan Mazilin ◽  
Edwin Gevorkyan ◽  
Vladimir Shkuropatenko ◽  
...  

In the paper, a novel technique for highly dispersed pyrochlore Y2Ti2O7 is proposed. The experimental results proved that the application of microwave irradiation at a certain stage of calcination allowed synthesizing of Y2Ti2O7 in much shorter time, which ensured substantial energy savings. An increase up to 98 wt.% in the content of the preferred phase with a pyrochlore-type structure Y2Ti2O7 was obtained after 25 h of yttrium and titanium oxides calcination at a relatively low temperature of 1150 °C, while the microwave-supported process took only 9 h and provided 99 wt.% of pyrochlore. The proposed technology is suitable for industrial applications, enabling the fabrication of large industrial amounts of pyrochlore without solvent chemistry and high-energy mills. It reduced the cost of both equipment and energy and made the process more environmentally friendly. The particle size and morphology did not change significantly; therefore, the microwave-assisted method can fully replace the traditional one.

2019 ◽  
Vol 6 (3) ◽  
pp. 659-670 ◽  
Author(s):  
Zhiqin Sun ◽  
Xue Yang ◽  
Huiming Lin ◽  
Feng Zhang ◽  
Qian Wang ◽  
...  

FeS2, prepared using a rapid microwave assisted method, exhibits excellent electrochemical performance for supercapacitor and OER applications.


2021 ◽  
Vol 6 (2) ◽  
pp. 03-17
Author(s):  
Gazal Dandia ◽  
◽  
Pratheek Sudhakaran ◽  
Chaitali Basu ◽  
◽  
...  

Introduction: High energy consumption by buildings is a great threat to the environment and one of the major causes of climate change. With a population of 1.4 billion people and one of the fastest-growing economies in the world, India is extremely vital for the future of global energy markets. The energy demand for construction activities continues to rise and it is responsible for over one-third of global final energy consumption. Currently, buildings in India account for 35% of total energy consumption and the value is growing by 8% annually. Around 11% of total energy consumption are attributed to the commercial sector. Energy-efficient retrofitting of the built environments created in recent decades is a pressing urban challenge. Presently, most energy-efficient retrofit projects focus mainly on the engineering aspects. In this paper, we evaluate various retrofitting options, such as passive architectural interventions, active technological interventions, or a combination of both, to create the optimum result for the selected building. Methods: Based on a literature study and case examples, we identified various energy-efficient retrofit measures, and then examined and evaluated those as applied to the case study of Awas Bhawan (Rajasthan Housing Board Headquarters), Jaipur, India. For the evaluation, we developed a simulation model using EQuest for each energy measure and calculated the resultant energy savings. Then, based on the cost of implementation and the cost of energy saved, we calculated the payback period. Finally, an optimum retrofit solution was formulated with account for the payback period and ease of installation. Results and discussion: The detailed analysis of various energy-efficient retrofit measures as applied to the case study indicates that the most feasible options for retrofit resulting in optimum energy savings with short payback periods include passive architecture measures and equipment upgrades.


2007 ◽  
Vol 7 (12) ◽  
pp. 4552-4556 ◽  
Author(s):  
Ming-Guo Ma ◽  
Ying-Jie Zhu

SrCO3 with an olive-like or flower-like morphology has been successfully synthesized by a microwave-assisted method using Sr(NO3)2 and (NH4)2CO3 in ethylene glycol (EG)or water. The solvent plays an important role in the size and morphology of SrCO3. The products were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM). This method is simple, fast, low-cost, and suitable for large-scale production.


Author(s):  
Norlin Pauzi ◽  
Norashikin Mat Zain ◽  
Nurul Amira Ahmad Yusof

The conventional heating methods of nanoparticle synthesis regularly depend on the energy inputs from outer heat sources that resulted high energy intake and low reaction competences. In this paper ZnO nanoparticles stabilized with gum arabic are synthesized using precipitating method assisted by simple and cost effective microwave heating technique. The objective of this work is to investigate the effect of microwave irradiation time towards ZnO nanoparticles morphology and size. The effect of microwave irradiation time has been investigated at 2, 4, 6, and 10 minutes. Dynamic Light Scattering (DLS) was employed to measure the size of ZnO nanoparticles. Ultraviolet–Visible spectroscopy (UV-vis), Fourier-Transform Infrared Spectroscopy (FTIR) and X-Ray Diffraction (XRD) were used for the characterization of the ZnO nanoparticles. UV-vis absorption spectrum was found in the range of 350 nm indicating the absorption peak of ZnO nanoparticles. FTIR spectra showed peaks range from 424 to 475 cm–1 which indicating standard of Zn–O stretching. The presence of (100), (002), and (101) planes were apparent in the XRD result, indicating the crystalline phase of ZnO nanoparticles. The increase in the microwave irradiation time affected the processes of nucleation and crystal growth promoted larger ZnO nanoparticles size. Microwave irradiation time at 2 minutes was selected as the best microwave irradiation time for smallest ZnO nanoparticles averaging about 168 nm sizes based on DLS analysis. Copyright © 2019 BCREC Group. All rights reservedReceived: 1st October 2018; Revised: 22nd November 2018; Accepted: 12nd December 2018; Available online: 25th January 2019; Published regularly: April 2019How to Cite: Pauzi, N., Zain, N.M., Yusof, N.A.A. (2019). Microwave-assisted Synthesis of ZnO Nanoparticles Stabilized with Gum Arabic: Effect of Microwave Irradiation Time on ZnO Nanoparticles Size and Morphology. Bulletin of Chemical Reaction Engineering & Catalysis, 14 (1): 182-188 (doi:10.9767/bcrec.14.1.3320.182-188)Permalink/DOI: https://doi.org/10.9767/bcrec.14.1.3320.182-188 


2019 ◽  
Vol 2019 (4) ◽  
pp. 7-22
Author(s):  
Georges Bridel ◽  
Zdobyslaw Goraj ◽  
Lukasz Kiszkowiak ◽  
Jean-Georges Brévot ◽  
Jean-Pierre Devaux ◽  
...  

Abstract Advanced jet training still relies on old concepts and solutions that are no longer efficient when considering the current and forthcoming changes in air combat. The cost of those old solutions to develop and maintain combat pilot skills are important, adding even more constraints to the training limitations. The requirement of having a trainer aircraft able to perform also light combat aircraft operational mission is adding unnecessary complexity and cost without any real operational advantages to air combat mission training. Thanks to emerging technologies, the JANUS project will study the feasibility of a brand-new concept of agile manoeuvrable training aircraft and an integrated training system, able to provide a live, virtual and constructive environment. The JANUS concept is based on a lightweight, low-cost, high energy aircraft associated to a ground based Integrated Training System providing simulated and emulated signals, simulated and real opponents, combined with real-time feedback on pilot’s physiological characteristics: traditionally embedded sensors are replaced with emulated signals, simulated opponents are proposed to the pilot, enabling out of sight engagement. JANUS is also providing new cost effective and more realistic solutions for “Red air aircraft” missions, organised in so-called “Aggressor Squadrons”.


RSC Advances ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 5432-5443
Author(s):  
Shyam K. Pahari ◽  
Tugba Ceren Gokoglan ◽  
Benjoe Rey B. Visayas ◽  
Jennifer Woehl ◽  
James A. Golen ◽  
...  

With the cost of renewable energy near parity with fossil fuels, energy storage is paramount. We report a breakthrough on a bioinspired NRFB active-material, with greatly improved solubility, and place it in a predictive theoretical framework.


e-Polymers ◽  
2021 ◽  
Vol 21 (1) ◽  
pp. 200-209
Author(s):  
Caiyun Zhang ◽  
Chunhong Li ◽  
Bolin Ji ◽  
Zhaohui Jiang

Abstract A fast, simple, and energy-saving microwave-assisted approach was successfully developed to prepare carbon microspheres. The carbon microspheres with a uniform particle size and good dispersity were prepared using glucose as the raw material and HCl as the dehydrating agent at low temperature (90°C) in an open system with the assistance of microwave heating. The carbon microspheres were characterized by elemental analysis, XRD, SEM, FTIR, TG, and Raman. The results showed that the carbon microspheres prepared under the condition of 18.5% (v/v) HCl and heating for 30 min by microwave had a narrow size distribution. The core–shell structure of the carbon core and TiO2 shell was prepared with (NH4)2TiF6, H3BO3 using the microwave-assisted method. The hollow TiO2 microspheres with good crystallinity and high photocatalytic properties were successfully prepared by sacrificing the carbon microspheres.


2021 ◽  
Vol 112 ◽  
pp. 110801
Author(s):  
Alif Syafiq Kamarol Zaman ◽  
Tong Ling Tan ◽  
Yamuna A/P Chowmasundaram ◽  
Norhanisah Jamaludin ◽  
Amir Reza Sadrolhosseini ◽  
...  

Metals ◽  
2020 ◽  
Vol 10 (12) ◽  
pp. 1690
Author(s):  
Jian Qiao ◽  
Peng Yu ◽  
Yanxiong Wu ◽  
Taixi Chen ◽  
Yixin Du ◽  
...  

Amorphous alloys have emerged as important materials for precision machinery, energy conversion, information processing, and aerospace components. This is due to their unique structure and excellent properties, including superior strength, high elasticity, and excellent corrosion resistance, which have attracted the attention of many researchers. However, the size of the amorphous alloy components remains limited, which affects industrial applications. Significant developments in connection with this technology are urgently needed. Laser welding represents an efficient welding method that uses a laser beam with high energy-density for heating. Laser welding has gradually become a research hotspot as a joining method for amorphous alloys due to its fast heating and cooling rates. In this compact review, the current status of research into amorphous-alloy laser welding technology is discussed, the influence of technological parameters and other welding conditions on welding quality is analyzed, and an outlook on future research and development is provided. This paper can serve as a useful reference for both fundamental research and engineering applications in this field.


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