scholarly journals Revealing the Microstructural Aspects of the Corrosion Dynamics in Rapidly Solidified Mg-Zn-Y Alloys Using the Acoustic Emission Technique

Materials ◽  
2021 ◽  
Vol 14 (24) ◽  
pp. 7828
Author(s):  
Daria Drozdenko ◽  
Michiaki Yamasaki ◽  
Kristián Máthis ◽  
Patrik Dobroň ◽  
Shin-ichi Inoue ◽  
...  
Keyword(s):  
Acoustic Emission ◽  
Strain Distribution ◽  
Protective Layer ◽  
Internal Strain ◽  
Hydrogen Release ◽  
Uniform Corrosion ◽  
Secondary Phases ◽  
Extrusion Speed ◽  
Average Grain Size ◽  
Rapidly Solidified

This work was focused on revealing the relation between the microstructure and corrosion dynamics in dilute Mg97.94Zn0.56Y1.5 (at.%) alloys prepared by the consolidation of rapidly solidified (RS) ribbons. The dynamics of the corrosion were followed by common electrochemical methods and the acoustic emission (AE) technique. AE monitoring offers instantaneous feedback on changes in the dynamics and mode of the corrosion. In contrast, the electrochemical measurements were performed on the specimens, which had already been immersed in the solution for a pre-defined time. Thus, some short-term corrosion processes could remain undiscovered. Obtained results were completed by scanning electron microscopy, including analysis of a cross-section of the corrosion layer. It was shown that the internal strain distribution, the grain morphology, and the distribution of the secondary phases play a significant role in the corrosion. The alloys are characterized by a complex microstructure with elongated worked and dynamically recrystallized α-Mg grains with an average grain size of 900 nm. Moreover, the Zn- and Y-rich stacking faults (SFs) were dispersed in the grain interior. In the alloy consolidated at a lower extrusion speed, the homogeneous internal strain distribution led to uniform corrosion with a rate of 2 mm/year and a low hydrogen release. The consolidation at a higher extrusion speed resulted in the formation of uneven distribution of internal strains with remaining high strain levels in non-recrystallized grains, leading to inhomogeneous growth and breakdown of the corrosion layers. Therefore, homogeneity of the internal strain distribution is of key importance for the uniform formation of a protective layer.

Observation of Fatigue Damage to Gear Tooth Using Image Processing

2007 ◽  
Author(s):  
Tomoya Masuyama ◽  
Takuya Ikeda ◽  
Satoshi Yoshiizumi ◽  
Katsumi Inoue
Keyword(s):  
Image Processing ◽  
Acoustic Emission ◽  
Strain Distribution ◽  
Cyclic Load ◽  
Early Stage ◽  
Gear Tooth ◽  
Digital Camera ◽  
Correlation Method ◽  
Point Of View ◽  
Strain Diagram

The detection of damage in early stage of fatigue is important for a reliable evaluation of gear life and strength. From this point of view, the variation of strain distribution in a tooth due to cyclic load contains useful information because the fatigue crack will initiate as a result of the accumulation of plastic strain. Meanwhile, digital image equipments are widely used in our life and the performance is in progress. We took digital pictures of cyclic loaded tooth by the digital camera and compared with the picture of no load to find displacement. The strain distribution of tooth is calculated by the correlation method using those pictures. The initiation of a micro crack is observed by the method. It is also confirmed by the detection of acoustic emission wave with higher energy. The variation of stress-strain diagram in fatigue process is presented, and this illustrates the increase of strain in the final stage of fatigue.

Structure and Electrical Properties of BNKT-Based Ceramics

2018 ◽  
Vol 283 ◽  
pp. 147-153 ◽  
Author(s):  
Supalak Manotham ◽  
Pichitchai Butnoi ◽  
Pharatree Jaita ◽  
Tawee Tunkasiri
Keyword(s):  
Grain Size ◽  
Perovskite Phase ◽  
Ferroelectric Properties ◽  
Tetragonal Symmetry ◽  
Secondary Phases ◽  
X Ray Diffraction ◽  
Average Grain Size ◽  
Influence Of Temperature On ◽  
Polarization Electric Field ◽  
Xrd Patterns

In this work, the properties of lead-free 0.92(Bi0.5Na0.42K0.08)TiO3-0.08(BaNb0.01Ti0.99)O3 or 92BNKT-8BNbT ceramic has been investigated. The sample was fabricated by a solid-state reaction technique. The 92BNKT-8BNbT sample was well sintered and dense with high density value of 5.86 g/cm3. X-Ray diffraction (XRD) patterns showed a single perovskite phase with tetragonal symmetry and no impurity or secondary phases. The microstructure was analysed using a scanning electron microscopy (SEM). Average grain size was measured and calculated based on a mean linear intercept method. The ceramics had a cubic-like grain shape with an average grain size of 0.39 µm. The influence of temperature on the dielectric and ferroelectric properties of the ceramic was investigated. The dielectric curves exhibited broad transition peaks at Td and Tm, which were the characteristics of a diffuse phase transition. The polarization-electric field (P-E) hysteresis loop changed from well-saturated at room temperature (RT) to pinched-type loop at high temperature (HT) and the remanent polarization decreased from 21.25 µC/cm2 (at RT) to 5.96 µC/cm2 (at 150 °C).

scholarly journals In-Situ Monitoring and Analysis of the Pitting Corrosion of Carbon Steel by Acoustic Emission

2019 ◽  
Vol 9 (4) ◽  
pp. 706 ◽  
Author(s):  
Junlei Tang ◽  
Junyang Li ◽  
Hu Wang ◽  
Yingying Wang ◽  
Geng Chen
Keyword(s):  
Acoustic Emission ◽  
Carbon Steel ◽  
Pitting Corrosion ◽  
Optical Microscope ◽  
Open Circuit ◽  
In Situ Monitoring ◽  
Localized Corrosion ◽  
Uniform Corrosion ◽  
Corrosion Morphology

The acoustic emission (AE) technique was applied to monitor the pitting corrosion of carbon steel in NaHCO3 + NaCl solutions. The open circuit potential (OCP) measurement and corrosion morphology in-situ capturing using an optical microscope were conducted during AE monitoring. The corrosion micromorphology was characterized with a scanning electron microscope (SEM). The propagation behavior and AE features of natural pitting on carbon steel were investigated. After completion of the signal processing, including pre-treatment, shape preserving interpolation, and denoising, for raw AE waveforms, three types of AE signals were classified in the correlation diagrams of the new waveform parameters. Finally, a 2D pattern recognition method was established to calculate the similarity of different continuous AE graphics, which is quite effective to distinguish the localized corrosion from uniform corrosion.

scholarly journals Rapidly Solidified Gas-Atomized Aluminum Alloys Compared with Conventionally Cast Counterparts: Implications for Cold Spray Materials Consolidation

Coatings ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1035
Author(s):  
Bryer C. Sousa ◽  
Caitlin Walde ◽  
Victor K. Champagne, Jr. ◽  
Aaron T. Nardi ◽  
Richard D. Sisson, Jr. ◽  
...  
Keyword(s):  
Cold Spray ◽  
Material Properties ◽  
In Silico ◽  
Bulk Material ◽  
Processing Parameters ◽  
Fine Tuning ◽  
Secondary Phases ◽  
Scanning Calorimetry ◽  
Rapidly Solidified ◽  
Conventionally Cast

In this work, three commercially available aluminum alloy systems (Al 2024, Al 6061, and Al 7075) were considered to explicitly capture the differences in material properties associated with a rapidly solidified, gas-atomized particulate feedstock as compared with their conventionally cast counterparts. Differences between the microstructural, thermodynamic, mechanical, and kinetic behaviors associated with gas-atomized and conventionally bulk counterparts have been tacitly assumed by the cold spray community. However, many researchers continue to utilize legacy properties from bulk materials when simulating particle impact phenomena in silico, for example. By way of recognizing the fact that bulk material properties may not serve as substitutes for gas-atomized powder property input parameters for cold spray process simulation and computation in silico, enhanced cold spray research and development will be more easily achieved. Therefore, understanding the feedstock powder characteristics for use in cold spray can lead to fine-tuning the properties of cold spray consolidations. Optical microscopy, scanning electron microscopy, nanoindentation, microhardness, differential scanning calorimetry, elemental analysis, and cooling rate calculations were utilized. This work confirms preliminary findings that powder alloys may not be treated the same way as their bulk counterparts in so far as the enactment of heat treatment processing parameters are concerned. Specifically, vast discrepancies were found in the grain size, secondary phases, and mechanical behavior between the powder and cast versions of each alloy.

Effects of Specimen Diameter on Microstructure and Microhardness of Hot Extruded AZ31B Magnesium Alloy

2014 ◽  
Vol 1004-1005 ◽  
pp. 158-162 ◽  
Author(s):  
Xiang Ting Hong ◽  
Fu Chen ◽  
Fei Chen ◽  
Wang Yu ◽  
Bo Rong Sang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Magnesium Alloy ◽  
Size Effects ◽  
Strain Distribution ◽  
Elevated Temperatures ◽  
Az31b Magnesium Alloy ◽  
Specimen Diameter ◽  
Average Grain Size ◽  
Micro Parts

Microstructures of metal micro parts after microforming at elevated temperatures must be evaluated due to mechanical properties depend on average grain size. In this work, the effects of specimen diameter on the microstructure and microhardness of a hot-extruded AZ31B magnesium alloy were studied. Obvious size effect on microstructure and microhardness of the alloy could be observed. The size effects could be explained by strain distribution and dislocation density differences between the two kinds of specimens.

Acoustic Emission Study of Corrosion Fatigue and Fatigue for API 5L X70 Gas Pipeline Steel

2011 ◽  
Vol 138-139 ◽  
pp. 635-639
Author(s):  
Z.H. Hanafi ◽  
Nordin Jamaludin ◽  
Shahrum Abdullah ◽  
M.F.M. Yusof ◽  
M.S.M. Zain
Keyword(s):  
Acoustic Emission ◽  
Fatigue Test ◽  
Corrosion Fatigue ◽  
Pipeline Steel ◽  
Petroleum Industry ◽  
Fatigue Behaviour ◽  
Pressure Vessels ◽  
Uniform Corrosion ◽  
Smooth Specimen ◽  
Steel Pipeline

Acoustic emission is a very important test among non-destructive tests, and it has been applied for the detection of failures in various types of equipment in the petroleum industry, such as pressure vessels, tanks and pipelines. In this study, the effect of pre-existing uniform corrosion on the corrosion fatigue specimen and smooth specimen on fatigue behaviour of API 5L X70 steel pipeline in long life range was investigated by using acoustic emission in fatigue test. The presence of pre-existing uniform corrosion specimen, produces by 4 month immersion in sulphuric acid, H2SO4 (concentration 0.2 ml H2SO4 in 5000 ml deionized water ). Fully reverse (R = -1) constant amplitude fatigue test were done in corrosion fatigue and smooth specimen in different stress amplitudes. It was found that, effect of pre-existing uniform corrosion significantly reduced the fatigue life of the steel pipeline. The correlations of accumulative AE counts for corrosion fatigue higher than fatigue test because of the mechanisms of possible AE sources due to corrosion.

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