scholarly journals Fracture Behavior of Long Fiber Reinforced Geopolymer Composites at Different Operating Temperatures

Materials ◽  
2022 ◽  
Vol 15 (2) ◽  
pp. 482
Author(s):  
Kinga Korniejenko ◽  
Beata Figiela ◽  
Celina Ziejewska ◽  
Joanna Marczyk ◽  
Patrycja Bazan ◽  
...  

The aim of this article was to analyze the fracture behavior of geopolymer composites based on fly ash or metakaolin with fine aggregate and river sand, with three types of reinforcement: glass, carbon, and aramid fiber, at three different temperatures, approximately: 3 °C, 20 °C, and 50 °C. The temperatures were selected as a future work temperature for composites designed for additive manufacturing technology. The main research method used was bending strength tests in accordance with European standard EN 12390-5. The results showed that the addition of fibers significantly improved the bending strength of all composites. The best results at room temperature were achieved for the metakaolin-based composites and sand reinforced with 2% wt. aramid fiber—17 MPa. The results at 50 °C showed a significant decrease in the bending strength for almost all compositions, which are unexpected results, taking into account the fact that geopolymers are described as materials dedicated to working at high temperatures. The test at low temperature (ca. 3 °C) showed an increase in the bending strength for almost all compositions. The grounds of this type of behavior have not been clearly stated; however, the likely causes of this are discussed.

Materials ◽  
2021 ◽  
Vol 14 (18) ◽  
pp. 5183
Author(s):  
Kinga Korniejenko ◽  
Beata Figiela ◽  
Krzysztof Miernik ◽  
Celina Ziejewska ◽  
Joanna Marczyk ◽  
...  

The aim of the article is to analyze the structure and mechanical properties in terms of the cracking mechanics of geopolymer composites based on fly ash and river sand, as well as metakaolin and river sand with three types of reinforcement material: glass fiber, carbon fiber, and aramid fiber, in terms of their use in additive manufacturing. Geopolymer composites were reinforced with fibers in a volume ratio of 0.5%, 1.0%, and 2.0%. Subsequently, these samples were subjected to bending strength tests in accordance with the European standard EN 12390-3. The addition of fibers significantly improved the bending strength of all composites made of metakaolin and sand. The reinforcement with aramid fiber in the amount of 2.0% resulted in more than a 3-fold increase in strength compared to the reinforcement-free composites. An analysis of the morphology of the fibers was carried out on the basis of photos taken from an electron microscope. The correct addition of fibers changes the nature of the fracture from brittle to more ductile and reduces the number of cracks in the material.


2021 ◽  
Vol 13 (8) ◽  
pp. 4169
Author(s):  
Congtao Sun ◽  
Ming Sun ◽  
Tao Tao ◽  
Feng Qu ◽  
Gongxun Wang ◽  
...  

Chloride binding capacity and its effect on the microstructure of mortar made with marine sand (MS), washed MS (WMS) and river sand (RS) were investigated in this study. The chloride contents, hydration products, micromorphology and pore structures of mortars were analyzed. The results showed that there was a diffusion trend for chloride ions from the surface of fine aggregate to cement hydrated products. During the whole curing period, the free chloride content in the mortars made by MS and WMS increased firstly, then decreased and stabilized finally with time. However, the total chloride content of three types of mortar hardly changed. The bound chloride content in the mortars made by MS and WMS slightly increased with time, and the bound chloride content included the MS, the WMS and the RS arranged from high to low. C3A·CaCl2·10H2O (Friedel’s salt) was formed at the early age and existed throughout the curing period. Moreover, the volume of fine capillary pore with a size of 10–100 nm increased in the MS and WMS mortar.


Author(s):  
Katsumasa Miyazaki ◽  
Kunio Hasegawa ◽  
Koichi Saito

The fitness-for-service codes require the characterization of non-aligned multiple flaws for flaw evaluation, which is performed using a flaw proximity rule. Worldwide, almost all such codes provide their own proximity rule, often with unclear technical bases of the application of proximity rule to ductile or fully plastic fracture. In particular, the effect of flaw dimensions of multiple surface flaws on fully plastic fracture of non-aligned multiple flaws had not been clear. To clarify the effect of the difference of part through-wall and through-wall flaws on the behavior of fully plastic fracture, the fracture tests of flat plate specimens with non-aligned multiple part through-wall flaws were conducted. When the flaw depth a was shallow with 0.4 in ratio of a to thickness t, the maximum load Pmax occurred at penetration of multiple flaws and the effect of vertical distance of non-aligned multiple flaws H on Pmax was not so significant. However, when flaw depth was deep with 0.8 in a/t, Pmax occurred after penetration of flaws and the effect of H on Pmax could be seen clearly. It was judged that the through-wall flaw tests were appropriate for discussion of the effect of H on Pmax and the alignment rule of multiple flaws. In addition, in order to clarify the appropriate length parameter to estimate Pmax of test specimens with dissimilar non-aligned through-wall multiple flaws, the fracture tests of plate specimens were also conducted. The effect of different flaw length on Pmax was discussed with maximum, minimum and averages of dissimilar non-aligned multiple flaw lengths. Experimental results showed that the maximum length lmax would be an appropriate length parameter to estimate Pmax, when the non-aligned multiple through-wall flaws were dissimilar.


2017 ◽  
Vol 264 ◽  
pp. 103-106 ◽  
Author(s):  
M.M. Rahman ◽  
M.A. Ismail ◽  
H. Y. Rahman

This paper presents the development of FeCuAl powder compacts through uniaxial die compaction process. Iron powder ASC 100.29 was mechanically mixed with other elemental powders, i.e., copper (Cu), and aluminum (Al) for 30 minutes at a rotation of 30 rpm. The feedstock was subsequently shaped at three different temperatures, i.e., 30°C, 150°C, and 200°C through simultaneous upward and downward axial loading of 325 MPa. The as-pressed samples termed as green compacts were then sintered in argon gas fired furnace at 800°C for three different holding times, i.e., 30, 60, and 90 min at a rate of 10°C/min. The sintered samples were characterized for their relative density, electrical resistivity, and bending strength. The microstructure of the sintered samples was also evaluated through scanning electron microscopy (SEM). The results revealed that the sample formed at 150°C and sintered for 30 min obtained the best final characteristics, i.e., higher relative density, lower volumetric expansion and electrical resistivity, and higher bending strength. Microstructure evaluation also revealed that the sample formed at 150°C and sintered for 30 min obtained more homogeneous distribution of grains and less interconnected pores compared to the other samples.


2017 ◽  
Vol 743 ◽  
pp. 19-24 ◽  
Author(s):  
Lilia I. Shevtsova ◽  
Anatoliy A. Bataev ◽  
Vyacheslav I. Mali ◽  
Maksim A. Esikov ◽  
Veronika V. Sun Shin Yan ◽  
...  

In the present study, a mixture of powders (87.9 at.% Ni, 12 at.% Al, 0.1 at.% B) was used as the initial material to produce sintered Ni3Al + B alloy. Spark Plasma Sintering (SPS) method was used to compact the powder. The powder mixtures were previously prepared in two ways: mixing the initial powders in a mortar (М1) and mechanical activation (М2). The microstructure was observed using optical microscope (OM). The addition of small amount of boron to the initial mixture of nickel and aluminum improves the density of the sintered Ni3Al intermetallic compound (98.8%). The results of density, bending and microhardness tests showed, that the provisional three-minute mechanical activation improves almost all properties of the sintered material. The compact obtained by SPS by M2 contributes to the formation of a homogeneous fine-grained structure of the material. It leads to further increase in flexural bending strength up to 2200 MPa. This value is almost 8 times the strength of the intermetallic Ni3Al stoichiometric composition obtained by SPS.


Author(s):  
Oleg Khalidullin ◽  

Snowfalls and blizzards block roads and create massive congestion on city streets and long-distance routes. Considering the processes of road surface formation during snowfall, it can be noted that snow during the fall is light fluffs, which, at an indefinite time, with different intensities, at different temperatures, stacked in layers, gradually by the wheels of cars, are compacted into a slippery tuberous canvas. The rubber tread, rolling through the freshly deposited layers, compresses the snow, forming a rut. The resulting trail adheres firmly to the asphalt. Almost all cars go on the trail, therefore the wheels of the following cars condense mainly the same track. On inactive roads, leaving the track during overtaking or detour leads to smoothing and compaction of the freezing walls of the track


This paper presents an experimental investigation on the properties of concrete in which like cement is partially replacing by used nano silica and is partially replacing by used waste foundry sand. Because now a day the world wide consumption of sand as cement and as fine aggregate in concrete production is very high. Nano silica and waste foundry sand are major by product of casting industry and create land pollution. The cement will be replaced with nano silica and the river sand will be replaced with waste foundry sand (0%, 5%, 10%, 15%, 20%). This experimental investigation was done and found out that with the increase in the nano silica and waste foundry sand ratio. Compression test has been done to find out the compressive strength of concrete at the age of 7, 14, 21, and 28. Test result indicates in increasing compressive strength of plain concrete by inclusion of nano silica as a partial replacement of cement and waste foundry sand as a partial replacement of fine aggregate.


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