scholarly journals Kinetic Study on Chlorophyll and Antioxidant Activity from Polyscias fruticosa (L.) Harms Leaves via Microwave-Assisted Extraction

Molecules ◽  
2021 ◽  
Vol 26 (12) ◽  
pp. 3761
Author(s):  
Thi-Thuy-Dung Nguyen ◽  
Quoc-Duy Nguyen ◽  
Thi-Van-Linh Nguyen
Keyword(s):  
Antioxidant Activity ◽  
Microwave Power ◽  
Order Kinetic ◽  
Microwave Assisted Extraction ◽  
Total Polyphenols ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Order Kinetic Model ◽  
High Antioxidant Activity ◽  
Kinetics Of

Polyscias fruticosa (L.) leaves contain significant bioactive compounds with high antioxidant activity such as chlorophylls, total polyphenols, etc. but these have still been underutilized. In this study, the kinetics of chlorophyll and antioxidant activity extraction from P. fruticosa leaves by microwave-assisted extraction (MAE) were investigated. Microwave power was 300, 450, or 600 (W); the ratio of material/solvent varied from 1:40 to 1:80 (g/mL). In this study, the second-order kinetic model successfully predicted the change of chlorophyll and antioxidant activity during MAE. The increase of microwave power or/and the solvent amount increased saturated extraction efficiency and the extraction rate constant. However, the saturated concentration of chlorophyll and antioxidant activity increased with the increment of microwave power and the decrease in solvent amount.

scholarly journals Influences of Microwave-Assisted Extraction Parameters on Antioxidant Activity of the Extract from Akebia trifoliata Peels

Foods ◽  
2021 ◽  
Vol 10 (6) ◽  
pp. 1432
Author(s):  
Min Luo ◽  
Dan-Dan Zhou ◽  
Ao Shang ◽  
Ren-You Gan ◽  
Hua-Bin Li
Keyword(s):  
Antioxidant Activity ◽  
Antioxidant Capacity ◽  
Microwave Power ◽  
Ethanol Concentration ◽  
Trolox Equivalent Antioxidant Capacity ◽  
Extraction Temperature ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Extraction Parameters

Akebia trifoliata is a fruit with rich nutritional properties, and its peel is produced as a by-product. In this research, we investigated the influences of microwave-assisted extraction parameters on antioxidant activity of the extract from Akebia trifoliata peels, and the ferric-reducing antioxidant power (FRAP) and Trolox equivalent antioxidant capacity (TEAC) as well as total phenolic contents (TPC) were used to optimize extraction parameters. The influences of ethanol concentration, microwave power and solvent-to-material ratio, as well as extraction temperature and time on TPC, FRAP and TEAC values, were assessed using single-factor tests. Three parameters with obvious effects on antioxidant capacity were selected to further investigate their interactions by response surface methodology. The optimal extraction parameters of natural antioxidants from Akebia trifoliata peels were ethanol concentration, 49.61% (v/v); solvent-to-material ratio, 32.59:1 mL/g; extraction time, 39.31 min; microwave power, 500 W; and extraction temperature, 50 °C. Under optimal conditions, the FRAP, TEAC and TPC values of Akebia trifoliata peel extracts were 351.86 ± 9.47 µM Fe(II)/g dry weight (DW), 191.12 ± 3.53 µM Trolox/g DW and 32.67 ± 0.90 mg gallic acid equivalent (GAE)/g DW, respectively. Furthermore, the main bioactive compounds (chlorogenic acid, rutin and ellagic acid) in the extract were determined by high-performance liquid chromatography. The results are useful for the full utilization of the by-product from Akebia trifoliate fruit.

scholarly journals Optimization of the Vacuum Microwave Assisted Extraction of the Natural Polyphenols and Flavonoids from the Raw Solid Waste of the Pomegranate Juice Producing Industry at Industrial Scale

Molecules ◽  
2021 ◽  
Vol 26 (4) ◽  
pp. 1033
Author(s):  
Konstantinos Petrotos ◽  
Ioannis Giavasis ◽  
Konstantinos Gerasopoulos ◽  
Chrysanthi Mitsagga ◽  
Chryssoula Papaioannou ◽  
...  
Keyword(s):  
Solid Waste ◽  
Microwave Power ◽  
Extraction Time ◽  
Pomegranate Juice ◽  
Industrial Scale ◽  
Microwave Assisted Extraction ◽  
Total Polyphenols ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Vacuum Microwave

Pomegranate pomace (PP) is the solid waste produced in bulk by the pomegranate juice industry which is rich in polyphenols and flavonoids that can replace the hazardous chemical antioxidants/antimicrobials currently used in the agro-food and cosmetics sectors. In the present work, the vacuum microwave assisted extraction (VMAE) of natural antioxidants from raw pomegranate pomace was investigated and successfully optimized at an industrial scale. For the optimization of PP VMAE a novel, highly accurate response surface methodology (RSM) based on a comprehensive multi-point historical design was employed. The optimization showed that the maximum recovery of PP total polyphenols as well as total PP flavonoids were obtained at microwave power = 4961.07 W, water to pomace ratio = 29.9, extraction time = 119.53 min and microwave power = 4147.76 W, water to pomace ratio = 19.32, extraction time = 63.32 min respectively. Moreover, the optimal VMAE conditions on economic grounds were determined to be: microwave power = 2048.62 W, water to pomace ratio = 23.11, extraction time = 15.04 min and microwave power = 4008.62 W, water to pomace ratio = 18.08, extraction time = 15.29 min for PP total polyphenols and PP total flavonoids respectively. The main conclusion of this study is that the VMAE extraction can be successfully used at industrial scale to produce, in economic manner, high added value natural extracts from PP pomace.

scholarly journals Simultaneous Optimization of Microwave-Assisted Extraction of Phenolic Compounds and Antioxidant Activity of Avocado (Persea americana Mill.) Seeds Using Response Surface Methodology

2020 ◽  
Vol 2020 ◽  
pp. 1-11
Author(s):  
Alexander Weremfo ◽  
Felix Adulley ◽  
Martin Adarkwah-Yiadom
Keyword(s):  
Antioxidant Activity ◽  
Response Surface Methodology ◽  
Phenolic Compounds ◽  
Response Surface ◽  
Microwave Power ◽  
Ethanol Concentration ◽  
Extraction Time ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Assisted Extraction

This study was designed to optimize three microwave-assisted extraction (MAE) parameters (ethanol concentration, microwave power, and extraction time) of total phenolics, total flavonoids, and antioxidant activity of avocado seeds using response surface methodology (RSM). The predicted quadratic models were highly significant (p<0.001) for the responses studied. The extraction of total phenolic content (TPC), total flavonoid content (TFC), and antioxidant activity was significantly (p<0.05) influenced by both microwave power and extraction time. The optimal conditions for simultaneous extraction of phenolic compounds and antioxidant activity were ethanol concentration of 58.3% (v/v), microwave power of 400 W, and extraction time of 4.8 min. Under these conditions, the experimental results agreed with the predicted values. MAE revealed clear advantages over the conventional solvent extraction (CSE) in terms of high extraction efficiency and antioxidant activity within the shortest extraction time. Furthermore, high-performance liquid chromatography (HPLC) analysis of optimized extract revealed the presence of 10 phenolic compounds, with rutin, catechin, and syringic acid being the dominant compounds. Consequently, this optimized MAE method has demonstrated a potential application for efficient extraction of polyphenolic antioxidants from avocado seeds in the nutraceutical industries.

scholarly journals Sifat Fisikokimia Zat Pewarna dari Bunga Eceng Gondok (Eichhornia crassipes) yang Diekstrak dengan Metode Microwave Asissted Extraction (MAE)

2019 ◽  
Vol 8 (1) ◽  
pp. 94-106
Author(s):  
Merynda Indriyani Syafutri ◽  
Filli Pratama ◽  
Gading Putra Yanda
Keyword(s):  
Antioxidant Activity ◽  
Microwave Power ◽  
Water Hyacinth ◽  
Eichhornia Crassipes ◽  
Extraction Time ◽  
Microwave Assisted Extraction ◽  
Color Intensity ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Anthocyanin Stability

Syafutri et al, 2019. Physicochemical Properties of Colorant from Water Hyacinth Flower (Eichhornia crassipes) Extracted by Microwave Assisted Extraction (MAE) Method. JLSO 8(1):94-106.The objective of this research was to determine the effect of oven microwave power and extraction time on color intensity, anthocyanin stability, and antioxidant activity of colorant from water hyacinth flower (Eichhornia crassipes) extracted by microwave assisted extraction (MAE) method. The research was conducted at Agricultural Product Chemical Laboratory, Agricultural Technology Department, Faculty of Agriculture, Sriwijaya University. The experiment used a Factorial Completely Randomized Design with two factors and each treatment was repeated three times.  The first factor was oven microwave power (100 watts and 300 watts) and the second factor was extraction time in oven microwave (1 minute, 2 minutes, and 3 minutes). The parameters were color intensity, anthocyanin stability, and antioxidant activity. The results showed that the oven microwave power and extraction time had significant effects on color intensity and antioxidant activity. The increasing of oven microwave power and extraction time increased a* value and antioxidant activity, and decreased b* value, significantly. The result also showed that the anthocyanin compounds was not stable with heating up to 105°C.

scholarly journals Optimizing Conditions for Microwave-Assisted Extraction of Polyphenolic Content and Antioxidant Activity of Barleria lupulina Lindl.

Plants ◽  
2021 ◽  
Vol 10 (4) ◽  
pp. 682
Author(s):  
Noor Wahida Ismail-Suhaimy ◽  
Siti Salwa Abd Gani ◽  
Uswatun Hasanah Zaidan ◽  
Mohd Izuan Effendi Halmi ◽  
Paiman Bawon
Keyword(s):  
Antioxidant Activity ◽  
Microwave Power ◽  
High Performance ◽  
Experimental Models ◽  
Extraction Time ◽  
Total Phenolic ◽  
Microwave Assisted Extraction ◽  
Leaf Extracts ◽  
Microwave Assisted ◽  
Assisted Extraction

Barleria lupulina Lindl. (Acanthaceae) as an ornamental plant has been widely used in folklore medicine due to its abundancy in polyphenolic compounds. The present study examined conditions for optimal extraction of antioxidants from B. lupulina leaf extracts by using the microwave-assisted extraction (MAE) method. The effects of ethanol concentrations, microwave power, and extraction time on total phenolic content (TPC), total flavonoid content (TFC), 1-diphenyl-2-picrylhydrazyl (DPPH), and 2,20-azino-bis (3-ethylbenzothizoline-6-sulfonic acid) (ABTS) were investigated by single-factor experiments. Response surface methodology (RSM) was applied to observe interactions of three independent variables (ethanol concentrations, microwave power, and extraction time) on the dependent variables (TPC, TFC, DPPH, and ABTS) to establish optimal extraction conditions. Quadratic polynomial equations in all experimental models yielded favorably with fitted models with R2 and R2adj of more than 0.90 and a non-significant lack of fit at p > 0.05. The optimal conditions for the extraction of antioxidant activity were established at 80% (v/v) ethanol, 400 W, and 30 s with TPC (238.71 mg gallic acid equivalent (GAE)/g sample), TFC (58.09 mg QE/g sample), DPPH (87.95%), and ABTS (89.56%). Analysis by ultra-high-performance liquid chromatography–quadrupole time-of-flight mass spectrometry (UHPLC-QTOF/MS) successfully identified four new phenylethanoid glycoside compounds in the species.

scholarly journals Microwave Assisted Extraction and Pressurized Liquid Extraction of Sulfated Polysaccharides from Fucus virsoides and Cystoseira barbata

Foods ◽  
2021 ◽  
Vol 10 (7) ◽  
pp. 1481
Author(s):  
Ana Dobrinčić ◽  
Sandra Pedisić ◽  
Zoran Zorić ◽  
Mladenka Jurin ◽  
Marin Roje ◽  
...  
Keyword(s):  
Antioxidant Activity ◽  
Chemical Composition ◽  
Liquid Extraction ◽  
Pressurized Liquid Extraction ◽  
Sulfate Group ◽  
Sulfated Polysaccharides ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Cystoseira Barbata

Sulfated polysaccharide fucoidan isolated from brown algae shows a wide range of biological activities that are significantly dependent on its chemical composition, which is closely related to the applied technique and extraction parameters. Therefore, the objective of this study was to evaluate the influence of microwave assisted extraction (MAE) and pressurized liquid extraction (PLE) parameters (solvent, temperature, time, and number of cycles) on the Fucus virsoides and Cystoseira barbata polysaccharide yield (%PS) and chemical composition (total sugar, fucose, and sulfate group). The optimal MAE parameters that resulted in the highest polysaccharide extraction from F. virsoides and C. barbata were 0.1 M H2SO4 for 10 min at 80 °C, while the optimal PLE parameters were 0.1 M H2SO4, for two cycles of 15 min at 140 °C. Furthermore, the %PS, chemical structure, molecular properties, and antioxidant activity of the F. virsoides and C. barbata polysaccharide extracts obtained with MAE, PLE, and conventional extraction (CE) performed under previously determinate optimal conditions were compared. PLE resulted in a significantly higher %PS from F. virsoides, while for C. barbata, a similar yield was achieved with CE and PLE, as well as CE and MAE, for both algae. Furthermore, the polysaccharides obtained using PLE had the highest polydispersity index, fucose, and sulfate group content, and the lowest uronic acid content; however their antioxidant activity was lower.

scholarly journals Microwave-Assisted Extraction and Ultrasound-Assisted Extraction of Bioactive Compounds from Grape Pomace

2020 ◽  
Vol 16 (1-2) ◽  
Author(s):  
Cassiano Brown da Rocha ◽  
Caciano Pelayo Zapata Noreña
Keyword(s):  
Antioxidant Activity ◽  
Phenolic Compounds ◽  
Bioactive Compounds ◽  
Grape Pomace ◽  
Total Phenolic ◽  
Microwave Assisted Extraction ◽  
Ultrasound Assisted Extraction ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Ultrasound Assisted

AbstractThe grape pomace is a by-product from the industrial processing of grape juice, which can be used as a source of bioactive compounds. The aim of this study was to separate the phenolic compounds from grape pomace using an acidic aqueous solution with 2 % citric acid as a solvent, using both ultrasound-assisted extraction, with powers of 250, 350 and 450 W and times of 5, 10 and 15 min, and microwave-assisted extraction using powers of 600, 800 and 1,000 W and times of 5, 7 and 10 min. The results showed that for both methods of extraction, the contents of total phenolic compounds and antioxidant activity by ABTS and DPPH increased with time, and microwave at 1,000 W for 10 min corresponded to the best extraction condition. However, the contents of phenolic compounds and antioxidant activity were lower than exhaustive extraction using acidified methanol solution.

scholarly journals Microwave-assisted Extraction and Antioxidant Activity of Flavonoids from Sedum aizoon Leaves

2017 ◽  
Vol 23 (1) ◽  
pp. 111-118 ◽  
Author(s):  
Congbin Jin ◽  
Xiaocong Wei ◽  
Shuli Yang ◽  
Lingyun Yao ◽  
Gangming Gong
Keyword(s):  
Antioxidant Activity ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Sedum Aizoon
Sign in / Sign up

Export Citation Format

Share Document