scholarly journals Characterization of Chitosan Film Incorporated with Curcumin Extract

Polymers ◽  
2021 ◽  
Vol 13 (6) ◽  
pp. 963
Author(s):  
Pornchai Rachtanapun ◽  
Warinporn Klunklin ◽  
Pensak Jantrawut ◽  
Kittisak Jantanasakulwong ◽  
Yuthana Phimolsiripol ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Antioxidant Activity ◽  
Infrared Spectroscopy ◽  
Water Vapor ◽  
Moisture Content ◽  
Water Solubility ◽  
Chitosan Film ◽  
Water Vapor Permeability ◽  
Vapor Permeability ◽  
Chitosan Films

Curcumin is a phenolic compound derived from turmeric roots (Curcuma longa L.). This research studied the effects of curcumin extract on the properties of chitosan films. The film characteristics measured included mechanical properties, visual aspects, color parameters, light transmission, moisture content, water solubility, water vapor permeability, infrared spectroscopy, and antioxidant activity. The results suggest that adding curcumin to chitosan-based films increases yellowness and light barriers. Infrared spectroscopy analysis showed interactions between the phenolic compounds of the extract and the chitosan, which may have improved the mechanical properties and reduced the moisture content, water solubility, and water vapor permeability of the films. The antioxidant activity of the films increased with increasing concentrations of the curcumin extract. This study shows the potential benefits of incorporating curcumin extract into chitosan films used as active packaging.

scholarly journals Physical Properties of Starch/Powdered Activated Carbon Composite Films

Polymers ◽  
2021 ◽  
Vol 13 (24) ◽  
pp. 4406
Author(s):  
Anita Kwaśniewska ◽  
Michał Świetlicki ◽  
Adam Prószyński ◽  
Grzegorz Gładyszewski
Keyword(s):  
Mechanical Properties ◽  
Activated Carbon ◽  
Water Vapor ◽  
Water Solubility ◽  
Composite Films ◽  
Water Vapor Permeability ◽  
Barrier Properties ◽  
Carbon Composite ◽  
Powdered Activated Carbon ◽  
Vapor Permeability

In the present study, starch/powdered activated carbon composite films were prepared by incorporating various amounts of powdered activated carbon (PAC)—1–5, 10, and 15 %—into a starch matrix, using the solvent casting method. The effect of PAC addition on the biopolymer film was investigated. The mechanical properties were examined by ultra-nanoindentation, nanoscratch, and micro-tensile tests. Since the mechanical properties of biopolymer films are correlated with their structure, the effect of PAC addition was tested using X-ray diffraction. The surface parameters morphology and wettability were analyzed by atomic force microscopy (AFM) and contact angle measurements. The barrier properties were examined by determining water vapor permeability and the water solubility index. The obtained results did not show a monotonic dependence of the mechanical parameters on PAC content, with the exception of the maximum strain, which decreased as the amount of the additive increased. The visible effect of PAC addition was manifested in changes in the adhesive force value and in water vapor permeability (WVP). The barrier properties decreased with the increase of the filler content.

Research on Preparation and Properties of Edible Composite Protein Films

2011 ◽  
Vol 87 ◽  
pp. 213-222 ◽  
Author(s):  
Gui Yun Chen ◽  
Qiao Lei
Keyword(s):  
Mechanical Properties ◽  
Water Vapor ◽  
Water Solubility ◽  
Water Vapor Permeability ◽  
Sodium Caseinate ◽  
Barrier Properties ◽  
Edible Films ◽  
Protein Isolate ◽  
Vapor Permeability ◽  
Protein Films

Edible films based on whey protein isolate and sodium caseinate were prepared by uniform design method. Glycerol has been incorporated into the edible films as a plasticizer. For all types of films, the influences of components and forming temperature on film properties, such as mechanical properties, water solubility, optical properties, gas and water vapor permeability were investigated. The results suggested that glycerol was the most important factor influencing all the properties of edible composite protein films. However, both increases of sodium caseinate concentration and glycerol content contributed to decrease the barrier properties of gas and water vapor. Among the films studied, group D (prepared with 5% whey protein isolate, 2% sodium caseinate, 50% glycerol at the temperature of 50 °C) showed moderate mechanical properties, optical properties, water solubility and maximum barrier properties of gas and water vapor, with tensile strength=5.85MPa, elongation=101.20%, transparency=91.4%, gas permeability rate=49.92cm3m-2d-10.1MPa-1and water vapor permeability of 0.128×10-11g m-1s-1Pa-1, 0.260×10-11g m-1s-1Pa-1, 0.513×10-11g m-1s-1Pa-1, 1.252×10-11g m-1s-1Pa-1at the RH gradient of 10-40%, 10-50%, 10-60%, 10-70%, respectively.

Physical Properties of Chitosan Edible Films Incorporated with Essential Oil Monomers

2012 ◽  
Vol 550-553 ◽  
pp. 993-999 ◽  
Author(s):  
Yun Bin Zhang ◽  
Jun Peng
Keyword(s):  
Mechanical Properties ◽  
Essential Oil ◽  
Physical Properties ◽  
Water Solubility ◽  
Water Vapor Permeability ◽  
Antibacterial Activities ◽  
Edible Films ◽  
Vapor Permeability ◽  
Monomer Content ◽  
Chitosan Films

In this study, physical properties of chitosan edible films incorporated with essential oil monomers were tested. Emulsifying nature of chitosan could be combined essential oil monomer forming emulsions, hence homogeneous, thin and pale yellow membranes were achieved. With different of the essential oil monomer content, the nature of the films had undergone a drastic change. Water-solubility and water vapor permeability of chitosan edible films reduced when essential oil monomers concentration increased. All the mechanical properties(tensile strength and elongation) increased when essential oil monomers concentration gradual increased. Compared with single chitosan films, essential oil-chitosan films have been greatly enhanced their mechanical properties and antibacterial activities.

Conducting/biodegradable chitosan-polyaniline film; Antioxidant, color, solubility and water vapor permeability properties

2021 ◽  
Vol 20 (2) ◽  
pp. 133-147
Author(s):  
Sajad Pirsa ◽  
Behzad Mohammadi
Keyword(s):  
Water Vapor ◽  
Food Packaging ◽  
Water Solubility ◽  
Light Transmission ◽  
Antioxidant Properties ◽  
Chitosan Film ◽  
Water Vapor Permeability ◽  
Vapor Permeability ◽  
Surface Color ◽  
Synthesis Time

In this study, chitosan-polyaniline nanocomposite film was prepared in combination with different concentrations of polyaniline at various synthesis times. Surface morphology, antioxidant properties, water solubility, water vapor permeability (WVP), color properties and light transparency properties of the films were investigated. The size, shape and morphology of the synthesized particles were examined with scanning electron microscopy (SEM) technique. The results indicated that the synthesized polyaniline particles were spherical and in the range of 45–70 nm. The results obtained from the study of the effect of polyaniline on the physical properties of the chitosan film showed that increasing polyaniline concentration and synthesis time causes a decrease in the rate of the water solubility and water vapor permeability. This is an important factor in expanding its use in food packaging. The results of the colorimetric studies showed that the polyaniline sharply changed the surface color of the film. Polyaniline also increased antioxidant properties of composite film. Investigating the light transmission and transparency of the films showed that the polyaniline reduced the transparency and transmission of light, which could be used to package products that are susceptible to oxidation in the light.

scholarly journals Effects of Pine Bark Extract on Physicochemical Properties and Biological Activity of Active Chitosan Film by Bionic Structure of Dragonfly Wing

Coatings ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 1077
Author(s):  
Kang Wan ◽  
Mengdi Cong ◽  
Xu Teng ◽  
Miao Feng ◽  
Lili Ren ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Water Vapor ◽  
Physicochemical Properties ◽  
Chitosan Film ◽  
Water Vapor Permeability ◽  
Pine Bark ◽  
Bark Extract ◽  
Vapor Permeability ◽  
Bionic Structure ◽  
Dragonfly Wings

Bionic and active films based on chitosan were developed with the bionic structure of dragonfly wings incorporating pine bark extract (PBE). Physicochemical properties of the films, including thickness, opacity, moisture content, color, mechanical properties, and water vapor permeability were measured. Antioxidant activity of the films was characterized by DPPH free radical scavenging activity. The interaction between chitosan and PBE was explored by attenuated total reflectance Fourier transform infrared spectrometry, X-ray diffraction, and differential scanning calorimetry. The results indicated that the addition of PBE gave rise to the films greater opacity, redness, and darker appearance. Compared with pure chitosan film, the thickness, opacity, mechanical properties, and oxidation resistance of the bionic chitosan–PBE film increased, and the water vapor permeability decreased. The films based on chitosan incorporated PBE and with the bionic structure of dragonfly wings can potentially be applied to food packaging.

scholarly journals Feasibility of Using Carvacrol/Starch Edible Coatings to Improve the Quality of Paipa Cheese

Polymers ◽  
2021 ◽  
Vol 13 (15) ◽  
pp. 2516
Author(s):  
Alex López-Córdoba
Keyword(s):  
Water Vapor ◽  
Moisture Content ◽  
Water Solubility ◽  
Potato Starch ◽  
Water Vapor Permeability ◽  
Aerobic Bacteria ◽  
Vapor Permeability ◽  
Edible Coatings ◽  
Starch Films

Paipa cheese is the only Colombian semi-ripened cheese with protected geographical indication. In the current work, the effect of applying starch coatings carrying carvacrol on Paipa cheeses was analyzed. Coatings were prepared based on blends of potato starch (2 g/100 g), carvacrol (0.1 g/100 g), polysorbate 80, glycerol, and water and applied to the cheese’s surface by brushing. Uncoated cheeses were also analyzed for comparison. Moreover, films were prepared and characterized in terms of their moisture content, water vapor permeability, mechanical properties, transparency, water solubility, swelling (%), and antioxidant activity. Carvacrol/starch films showed a slight decrease in their water solubility and Young’s modulus, while not significant changes were observed in water vapor permeability, moisture content, transparency, and swelling behavior, in comparison with the starch films. After application on the Paipa cheeses, the carvacrol/starch coatings enhanced the brightness of the cheeses without causing significant changes in water activity, moisture content, color attributes, and mesophilic aerobic bacteria and molds/yeasts count. Moreover, edible coatings have a significant effect on the hardness, the gumminess, the springiness, and the chewiness of the Paipa cheese. Coated cheeses were better preserved at day 60 of storage because they did not show changes in their lightness, hardness, and springiness.

scholarly journals Mechanical and Barrier Properties of Composite Films Based on Kappa-Carrageenan-Polyvinyl Alcohol

2019 ◽  
Vol 8 (6S3) ◽  
pp. 489-499
Keyword(s):  
Tensile Strength ◽  
Water Vapor ◽  
Moisture Content ◽  
Polyvinyl Alcohol ◽  
Water Solubility ◽  
Composite Films ◽  
Water Vapor Permeability ◽  
Vapor Permeability ◽  
Burst Strength ◽  
Kappa Carrageenan

Optimization of film formula-based kappa-carrageenan and polyvinyl alcohol (PVA) was studied using a two-level, two-factor Design Expert 11® by Response Surface Methodology (RSM) Central Composite Design (CCD). The aim of this study was to obtain the optimal concentration of kappa-carrageenan and polyvinyl alcohol in producing films. The influence composition ⱪ-carrageenan and polyvinyl alcohol was characterized. The results showed the effects of k-carrageenan and polyvinyl alcohol had a significant effect on the response thickness, tensile strength, burst strength, elongation, solubility, water vapor barrier, opacity, color, and moisture content. The optimized condition for production k-carrageenan and PVA was 1.21% carrageenan and 1.93% polyvinyl alcohol, which was giving film with thickness 0.044 mm, tensile strength 16.69 MPa, burst strength 167.86 kPa, elongation 81.79%, water solubility 65.04%, water vapor permeability 7.49 g/m s Pa x 10-11, opacity 2.31, ΔE 2.42, and moisture content 19.13%

scholarly journals Development of PE/PCL Bilayer Films Modified with Casein and Aluminum Oxide

Molecules ◽  
2021 ◽  
Vol 26 (11) ◽  
pp. 3090
Author(s):  
Anita Ptiček Siročić ◽  
Ana Rešček ◽  
Zvonimir Katančić ◽  
Zlata Hrnjak-Murgić
Keyword(s):  
Mechanical Properties ◽  
Thermal Properties ◽  
Water Vapor ◽  
Aluminum Oxide ◽  
Water Vapor Permeability ◽  
Vapor Permeability ◽  
Mechanical And Thermal Properties ◽  
Oxide Compound ◽  
Bilayer Films ◽  
Oxide Particles

The studied samples were prepared from polyethylene (PE) polymer which was coated with modified polycaprolactone (PCL) film in order to obtain bilayer films. Thin PCL film was modified with casein/aluminum oxide compound to enhance vapor permeability as well as mechanical and thermal properties of PE/PCL films. Casein/aluminum oxide modifiers were used in order to achieve some functional properties of polymer film that can be used in various applications, e.g., reduction of water vapor permeability (WVTR) and good mechanical and thermal properties. Significant improvement was observed in mechanical properties, especially in tensile strength as well as in water vapor values. Samples prepared with aluminum oxide particles indicated significantly lower values up to 60%, and samples that were prepared with casein and 5% Al2O3 showed the lowest WVTR value.

scholarly journals Characterization of Food Packaging Films with Blackcurrant Fruit Waste as a Source of Antioxidant and Color Sensing Intelligent Material

Molecules ◽  
2021 ◽  
Vol 26 (9) ◽  
pp. 2569
Author(s):  
Mia Kurek ◽  
Nasreddine Benbettaieb ◽  
Mario Ščetar ◽  
Eliot Chaudy ◽  
Maja Repajić ◽  
...  
Keyword(s):  
Food Packaging ◽  
Water Solubility ◽  
Color Change ◽  
Chitosan Film ◽  
Water Vapor Permeability ◽  
Vapor Permeability ◽  
Color Changes ◽  
Insoluble Particles ◽  
Polymer Stability ◽  
Food Packaging Films

Chitosan and pectin films were enriched with blackcurrant pomace powder (10 and 20% (w/w)), as bio-based material, to minimize food production losses and to increase the functional properties of produced films aimed at food coatings and wrappers. Water vapor permeability of active films increased up to 25%, moisture content for 27% in pectin-based ones, but water solubility was not significantly modified. Mechanical properties (tensile strength, elongation at break and Young’s modulus) were mainly decreased due to the residual insoluble particles present in blackcurrant waste. FTIR analysis showed no significant changes between the film samples. The degradation temperatures, determined by DSC, were reduced by 18 °C for chitosan-based samples and of 32 °C lower for the pectin-based samples with blackcurrant powder, indicating a disturbance in polymer stability. The antioxidant activity of active films was increased up to 30-fold. Lightness and redness of dry films significantly changed depending on the polymer type. Significant color changes, especially in chitosan film formulations, were observed after exposure to different pH buffers. This effect is further explored in formulations that were used as color change indicators for intelligent biopackaging.

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