scholarly journals Mechanical Behaviour of Multifunctional Epoxy/Hollow Glass Microspheres/Paraffin Microcapsules Syntactic Foams for Thermal Management

Polymers ◽  
2021 ◽  
Vol 13 (17) ◽  
pp. 2896
Author(s):  
Francesco Galvagnini ◽  
Giulia Fredi ◽  
Andrea Dorigato ◽  
Luca Fambri ◽  
Alessandro Pegoretti

Epoxy/hollow glass microsphere (HGM) syntactic foams (SFs) are peculiar materials developed to combine low density, low thermal conductivity, and elevated mechanical properties. In this work, multifunctional SFs endowed with both structural and thermal management properties were produced for the first time, by combining an epoxy matrix with HGM and a microencapsulated phase change material (PCM) having a melting temperature of 43 °C. Systems with a total filler content (HGM + PCM) up to 40 vol% were prepared and characterized from the mechanical point of view with a broad experimental campaign comprising quasi-static, impact, and fracture toughness tests. The experimental results were statistically treated and fitted with a linear model, to produce ternary phase diagrams to provide a comprehensive interpretation of the mechanical behaviour of the prepared foams. In quasi-static tests, HGM introduction helps to retain the specific tensile elastic modulus and to increase the specific compressive modulus. The brittle nature of HGMs decreases the Charpy impact properties of the SFs, while the PCM insertion improve their toughness. This result is confirmed in KIC and GIC tests, where the composition with 20 vol% of PCM shows an increase of 80% and 370% in KIC and GIC in to neat epoxy, respectively. The most promising compositions are those combining PCM and HGMs with a total particle volume fraction up to 40 vol%, thanks to their optimal combination of thermal management capability, lightness, thermal insulation, and mechanical properties. The ability to fine-tune the properties of the SFs, together with the acquired thermal energy storage (TES) capability, confirm the great potential of these multifunctional materials in automotive, electronics, and aerospace industries.

Author(s):  
Yongsheng Chen ◽  
Zesheng Ji ◽  
Maoliang Hu ◽  
Hongyu Xu ◽  
Guangjie Feng

Abstract AlCrFeCoNi particles were added to Mg-9Al-1Zn alloy in a rotary blowing process. The microstructures and mechanical properties of Mg-9Al-1Zn based composites were characterized by means of X-ray diffraction, optical microscopy, scanning electron microscopy, transmission electron microscopy, and tensile and compression tests at room temperature. Results revealed that AlCrFeCoNi particles could effectively refine the grains, and the rotary blowing process enabled the uniform distribution of these particles. The mechanical properties of composites improved with the increase of particle volume fraction. The superior wettability of AlCrFeCoNi particles supported their reliable bonding with the Mg-9Al-1Zn matrix. The Hall–Petch strengthening and stress transfer effect played a dominant role in the improvement of compressive and tensile properties.


2012 ◽  
Vol 629 ◽  
pp. 105-109
Author(s):  
Yi Qiang He ◽  
Jian Ming Yang ◽  
Bin Qiao ◽  
Li Chao Feng

SiCP/Cu composite was prepared by metal injection molding process. Microstructure, mechanical properties, fracture surface, and wear resistance of SiCP/Cu composite were investigated in this study. The research results show that SiCP/Cu were sintered sucessfully by the sintering process with hydrogen protection and high temperature of 1050°C. The tensile strength of the composites depends on the fraction and distribution of SiC particles which is resulted from microcracks nucleate in the matrix between SiC particles because of SiC particle aggregation. The tensile strengths of 5vol.%, 10vol.%, and15vol.%SiCP/Cu are 254MPa, 291MPa and 278MPa separately. SiC particles are contribute to enhance the abrasive resitance of the composite when particle volume fraction increase from 10% to 15%.


2007 ◽  
Vol 353-358 ◽  
pp. 1390-1393
Author(s):  
Bai Feng Luan ◽  
Gao Hui Wu ◽  
Qing Liu ◽  
Niels Hansen ◽  
Ting Quan Lei

An experimental study of microstructure and mechanical properties in the Al2O3 particulate reinforced 6061 Aluminum composites has been used to determine the effect of extrusion and particle volume fraction (20, 26, 30, 40, 50, 60%Vf) in deformed metal matrix composites. The microstructure of Al2O3 /6061Al composite before and after hot extrusion is investigated by TEM and SEM. Results show that dislocation and subgrain generated after hot extrusion as well as the particle distribution of composite become more uniform with extrusion ratio of 10:1. The ultimate strength, yield strength and elongation of the composite also increase after hot extrusion. Dispersion strengthening and subgrain boundary strengthening is discussed and also the effect of precipitate introduced by heat treatment both after casting and after extrusion. The yield stress (0.2% offset) of the composites has been calculated and predicted using a standard dislocation hardening model. Whilst the correlation between this and the measured value of yield stress obtained in previous experimental test is reasonable.


2014 ◽  
Vol 21 (4) ◽  
pp. 505-515 ◽  
Author(s):  
Aykut Canakci ◽  
Fazli Arslan ◽  
Temel Varol

AbstractIn this study, metal matrix composites of an aluminum alloy (AA2024) and B4C particles with volume fractions 3, 5, 7, and 10 vol% and with sizes 29 and 71 μm were produced using stir-casting technique. The effects of B4C particle content and size of boron carbide on the mechanical properties of the composites such as hardness, 0.2% yield strength, tensile strength, and fracture were investigated. Furthermore, the relation between particle content, microstructure, and particle distribution has been investigated. The hardness of the composites increased with increasing particle volume fraction and with decreasing particle size, although the tensile strength of the composites decreased with increasing particle volume fraction and with decreasing particle size. Scanning electron microscopic observations of the microstructures revealed that dispersion of the coarser sizes of B4C particles was more uniform while the finer particles led to agglomeration of the particles and porosity.


2016 ◽  
Vol 723 ◽  
pp. 68-73
Author(s):  
Hong Tu Song

When blending rubbers into polymers, different rubber distribution status and fraction due to different mechanical property. In this research, effective mechanical properties of rubber-toughened polymers with four blending fraction in six kinds of particle distribution status are simulated numerically by using finite element method. Rubber particle distribution model include four 2D models and two 3D models. Typical effective mechanical properties such as yield stress, Young's modulus, Poisson's ratio and stress-strain curve of each status are obtained. The Results show that all models Young's modulus and Poisson's ratio decrease with rubber particle volume fraction increasing. Young's modulus and Poisson's ratio of three-dimensional body-centered cubic and face-centered cubic models are in a close magnitude range, it means rubber particle volume fraction has less effect on 2D models and two 3D models. As we all known, Matrix yielding, crazing and interface debond. All play an important role in the toughening process of rubber-toughened polymers. So in this paper we also study on toughening mechanism using same models. Our simulation takes use of stress concentration factor, yield ratio and interface elements' strain difference which is related with matrix yielding, crazing and interface debond to study the toughening mechanism. Simulation shows that the maximum stress concentration factor increases with particle volume fraction. The shear yielding occurs first at the equator of rubber particle, and then yield region expands from the equator to the pole of the particle with loads increasing.


2016 ◽  
Vol 45 (6) ◽  
pp. 426-430 ◽  
Author(s):  
Yingjie Qiao ◽  
Xiaodong Wang ◽  
Xiaohong Zhang ◽  
Zhipeng Xing

Purpose The purpose of this paper is to investigate the preparation and the flexural property of hollow glass microspheres (HGMs) filled resin-matrix composites, which have been widely applied in deep-sea fields. Design/methodology/approach The composites with different contents of HGMs from 47 to 57 Wt.% were studied. The voids in syntactic foams and their flexural properties were investigated. Findings The results showed that the voids quantity increased because of the increment of HGM content, whereas the exural strength and the exural modulus decreased. The fracture mechanism of the composites was also investigated by scanning electron microscope, which indicated that the composites failed by the crack extending through the microspheres. Research limitations/implications The advantages of HGMs with similar hollow spheres will be further investigated in a future research. Practical implications Results demonstrated that the properties of the composite might be tailored for specific application conditions by changing the HGM volume fraction. Originality/value The HGM filled resin-matrix composite materials have their unique properties and significant application potential. In this work, the resin-HGM composites were synthesized by mechanically mixing defined quantities of HGMs into epoxy resin, by which a kind of syntactic foams with good flexural properties could be obtained.


Fractals ◽  
1994 ◽  
Vol 02 (02) ◽  
pp. 249-252 ◽  
Author(s):  
FAUSTIN DOSSOU ◽  
RAYNALD GAUVIN

The mechanical properties of a 6061 aluminium alloy and of a composite material 6061/ Al 2 O 3/10-20% p have been mesured after heat treatments using a tensile test. Fracture surfaces profiles were used to mesure fractal dimension using the step divider method. The fractal dimension of the fractured surfaces of the composite material 6061/ Al 2 O 3/10-20% p depend on the aging and on the particle volume fraction but is independent of aging time for the unreinforced alloy.


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