Effect of the Temperature on Diamond-Like Carbon (DLC) Thin Film Based on LIS

2013 ◽  
Vol 421 ◽  
pp. 212-216 ◽  
Author(s):  
Lei Huang ◽  
Jun Tang Yuan ◽  
Zhen Hua Wang ◽  
Bin Bin Yu
Keyword(s):  
Thin Films ◽  
Surface Roughness ◽  
Intensity Ratio ◽  
Failure Load ◽  
Ion Source ◽  
Diamond Like Carbon ◽  
Anode Layer ◽  
Effect Mechanism ◽  
Atomic Force ◽  
Different Temperatures

Diamond-like carbon (DLC) thin films were deposited on YG6 cemented carbide by an anode-layer linear ion source (LIS). The effect of different temperatures (20°C, 80°C, 115°C and 150°C) on DLC thin films was investigatedby using atomic force microscope (AFM), scanning electron microscope (SEM) and Raman spectroscopy. It was found thatthe surface roughness of the film decreased at first and then increased with the increase of the temperature, and reached the trough at 80°C. The intensity ratio (ID/IG) and the adhesion of the film increased at first and then decreased, and both of them reached the peak at 80°C. When the temperature was 80°C, the surface roughness was 6.9nm, the intensity ratio (ID/IG) was1.91 and the critical failure load was 107.23N. The results show that the temperatures have a great effect on the surface morphology and mechanism properties of DLC thin films. Consequently, this paperfurther studied the effect mechanism of different temperatures on DLC thin films based on the experiment.

Investigation of Friction Over a Wide Range of Normal Forces

2007 ◽  
Author(s):  
Dirk Drees ◽  
Satish Achanta
Keyword(s):  
Surface Roughness ◽  
Dual Phase Steel ◽  
Normal Force ◽  
Diamond Like Carbon ◽  
Dual Phase ◽  
Normal Forces ◽  
Atomic Force ◽  
Wide Range ◽  
Atomic Interactions ◽  
The Coefficient Of Friction

Friction at different force, length, and time scales is of great interest in tribology. The mechanical, chemical, and physical (atomic) interactions, each operating at their own time length and force scale, makes friction complex. This work is an attempt to improve the understanding of friction at normal forces ranging from nN up to N. This investigation was carried out under reciprocating ball-on-flat sliding conditions on engineering surfaces like diamond-like carbon (DLC) and dual phase steel. The test equipments used for this investigation are an atomic force microscope, a microtribometer, and a macrofretting tester. It was observed that for a hard/hard tribocouple like DLC/Si3N4, the variation in the coefficient of friction is negligible whereas the variation is large when the tribocouple is hard / soft like in dual phase steel / Si3N4. By changing the surface roughness of the material, the dependence of friction on normal force could be altered or manipulated.

Effect of Annealing Atmosphere on the Morphology of Copper Oxide Thin Films Deposited on TiO2 Substrates Prepared by Sol-Gel Process

2013 ◽  
Vol 594-595 ◽  
pp. 113-117 ◽  
Author(s):  
Dewi Suriyani Che Halin ◽  
Ibrahim Abu Talib ◽  
Abdul Razak Daud ◽  
Muhammad Azmi Abdul Hamid
Keyword(s):  
Thin Films ◽  
Surface Roughness ◽  
Grain Size ◽  
Copper Oxide ◽  
Spin Coating ◽  
Sol Gel ◽  
Annealing Atmosphere ◽  
Oxide Thin Films ◽  
Different Temperatures ◽  
Xrd Patterns

Copper oxide films were prepared via sol-gel like spin coating starting from methanolic solutions of cupric chloride onto the TiO2 substrates. Films were obtained by spin coating under room conditions (temperature, 25-30 °C) and were subsequently annealed at different temperatures (200-400 °C) in oxidizing (air) and inert (N2) atmospheres. X-ray diffraction (XRD) patterns showed crystalline phases, which were observed as a function of the annealing conditions. The film composition resulted single or multi-phasic depending on both temperature and atmosphere. The grain size of film was measured using scanning electron microscopy (SEM) and the surface roughness of thin films was characterized by atomic force microscopy (AFM). The grain size of which was annealed in air at 300 °C was 30.39 nm with the surface roughness of 96.16 nm. The effects of annealing atmosphere on the structure and morphology of copper oxide thin films are reported.

Pulsed Laser Deposition and Characterization of InZnO Alloyed Thin Film

2008 ◽  
Vol 368-372 ◽  
pp. 308-311
Author(s):  
F.K. Shan ◽  
G.X. Liu ◽  
Byoung Chul Shin ◽  
Won Jae Lee ◽  
W.T. Oh
Keyword(s):  
Thin Films ◽  
Pulsed Laser Deposition ◽  
Pulsed Laser ◽  
Atomic Ratio ◽  
Laser Deposition ◽  
Morphological Properties ◽  
High Quality ◽  
Atomic Force ◽  
Different Temperatures ◽  
Zno Powder

High-quality In2O3 powder and ZnO powder had been used to make the ceramic target and the atomic ratio of 1 to 1 of indium and zinc had been prepared in this study. The alloyed thin films had been deposited on sapphire (001) substrates at different temperatures (100–600°C) by using pulsed laser deposition (PLD) technique. An x-ray diffractometer and an atomic force microscope were used to investigate the structural and morphological properties of the alloyed thin films. It was observed that the alloyed thin films deposited at the temperatures lower than 300°C were amorphous, and the alloyed thin films deposited at high temperatures were crystallized. A spectrophotometer was used to investigate the transmittances of the alloyed thin films. It was found that the alloyed thin films were of high quality. The band gap energies of the alloys were calculated by linear fitting the sharp absorption edges of the transmittance spectra. The Hall measurements were also carried out to identify the electrical properties of the thin films.

Effect of Molarity on Structural and Optical Properties of Chemically Deposited Nanocrystalline PbS Thin Film

2017 ◽  
Vol 74 ◽  
pp. 22-35 ◽  
Author(s):  
Manash Pratim Sarma ◽  
G. Wary
Keyword(s):  
Thin Films ◽  
Ph Value ◽  
Bath Temperature ◽  
Ion Source ◽  
Complexing Agent ◽  
X Ray ◽  
Force Microscopy ◽  
Nanocrystallite Size ◽  
Atomic Force ◽  
Cbd Method

Thin films of PbS were deposited by chemical bath deposition (CBD) method under various molarities using lead acetate as Pb2+ ion source, thiourea as S2- ion source and ammonia as complexing agent at a fixed pH value of 9 under bath temperature of 333 K. Four different molarities of PbS thin films were prepared. The as-prepared films were characterized by using X-ray diffraction (XRD), X-ray fluorescence (XRF), EDX, field emission scanning electron microscopy (FESEM) and atomic force microscopy (AFM). Parameters like crystallite size, lattice constant, microstrain, dislocation density were calculated. Optical constants such as extinction coefficient, absorption coefficient were measured from absorption spectra. Studies show that average nanocrystallite size increases from14.2 nm to 18.1 nm as the molarity of the film increases. Optical studies reveal the decrease of band gap from 1.75 eV to 1.44 eV with increasing molarity of the film indicating higher electrical conductivity of the films.

Low-Temperature Plasma Deposition of Diamond-Like Carbon and III Nitride Thin-Films for Photovoltaic Devices

2009 ◽  
Vol 610-613 ◽  
pp. 353-356
Author(s):  
Jin She Yuan ◽  
Ming Yue Wang ◽  
Guo Hao Yu
Keyword(s):  
Thin Films ◽  
Low Temperature ◽  
Plasma Deposition ◽  
Diamond Like Carbon ◽  
Low Temperature Plasma ◽  
Photovoltaic Devices ◽  
Temperature Plasma ◽  
Force Microscopy ◽  
Atomic Force ◽  
Gan Film

Low-temperature plasma deposition of diamond-like carbon (DLC) and gallium nitride thin-films grown on Si substrate by PECVD was investigated using atomic force microscopy and reflectance spectra for photovoltaic devices application. It was found that the morphological features of the GaN film depend on the substrates under the optimum deposition conditions. The optical band gap of the films was approximately 5.5eV for PECVD DLC and approximately 3.3 eV for PECVD GaN.

scholarly journals Effect of Gallium Incorporation on the Properties of ZnO Thin Films

2019 ◽  
Author(s):  
Sema Kurtaran ◽  
Serhat Aldağ ◽  
Göksu Öföfoğlu
Keyword(s):  
Thin Films ◽  
Surface Roughness ◽  
Zno Thin Films ◽  
Visible Range ◽  
Zno Films ◽  
Spray Pyrolysis Method ◽  
Chemical Spray Pyrolysis ◽  
Atomic Force ◽  
Doped Zno ◽  
Ga Doping

Ga doped ZnO thin films were formed by the Ultrasonic Chemical Spray Pyrolysis method onto substrates using zinc acetate and gallium (III) nitrate hydrate as precursors. The structural, optical, surface and electrical properties were studied as a function of increasing Ga doping concentration from 0 to 6 at %. Structural studies were shown polycrystalline with a hexagonal crystal structure. The transparency in the visible range was around 85% for thin film deposited using 6 at % Ga doping. With the aim of determining surface images and surface roughness of the films atomic force microscope images were taken. Ga doping of ZnO thin films could markedly decrease surface roughness. Electrical resistivity was determined by four point method. The resistivity 2.0% Ga doped ZnO film was the lowest resistivity of 1.7 cm. In the photoluminescence measurements of the films, existence of UV and defect emission band was observed. As a result, Ga doped ZnO films have advanced properties and promising materials for solar cells.

scholarly journals Modification of Surface and Tribological Properties of DLC Films by Adding Silver Content

2008 ◽  
Author(s):  
H.-S. Zhang ◽  
J. L. Endrino ◽  
A. Anders
Keyword(s):  
Thin Films ◽  
Atomic Force Microscopy ◽  
Tribological Properties ◽  
Silver Content ◽  
Diamond Like Carbon ◽  
Dlc Coatings ◽  
Force Microscopy ◽  
Atomic Force ◽  
Plasma Immersion Ion Implantation ◽  
Scratch Tests

The incorporation of silver into the diamond-like carbon (DLC) coatings has shown excellent potential in various applications; therefore the surface and tribological properties of silver-containing DLC thin films deserve to be investigated. In this study we have deposited silver-containing hydrogenated and hydrogen-free DLC coatings by plasma immersion ion implantation and deposition (PIII-D) methods. Atomic force microscopy (AFM) and nano-scratch tests were used to study the surface and tribological properties. The silver incorporation had only slight effects on hydrogenated DLC coatings. However, the incorporation of silver has significant effect on hydrogen-free DLC of smoothing the surface and increasing the surface energy. Those effects have been illustrated and explained in the context of experimental results.

The Influence of Substrate Temperature on the Morphological and Optical Properties of ZnTiO3 Thin Films Prepared by Magnetron Sputtering

2013 ◽  
Vol 804 ◽  
pp. 3-7
Author(s):  
Chao Zhan ◽  
Wen Jian Ke ◽  
Xin Ming Li ◽  
Wan Li Du ◽  
Li Juan Wang ◽  
...  
Keyword(s):  
Thin Films ◽  
Surface Roughness ◽  
Refractive Index ◽  
Optical Properties ◽  
Magnetron Sputtering ◽  
Substrate Temperature ◽  
Dispersion Model ◽  
Film Surface ◽  
Cubic Phase ◽  
Different Temperatures

Cubic ZnTiO3thin films have been prepared by radio frequency magnetron sputtering on n-type (100) Si substrate at different temperatures. The morphological and optical properties of ZnTiO3films in relation to substrate temperatures are investigated by spectroscopic ellipsometry (SE) and AFM as well as SEM in detail. X-ray diffraction (XRD) measurement shows that all the films have a cubic phase structure and the optimum substrate temperature to form crystalline ZnTiO3thin film is 250 °C. Through SEM and AFM, the particle size in thin films and film surface roughness increase with increasing the substrate temperature. Based on a parameterized TaucLorentz dispersion model, the optical constants and surface roughness of ZnTiO3films related to the substrate temperature are systematically extracted by SE measurement. The surface roughness of the film measured from AFM agrees well with result extracted from SE, which proved that the established SE model is reasonable. With increasing substrate temperature, the refractive index decreases and the main factor in determining the refractive index was deduced to be the surface roughness related to the film packing density. The extinction coefficient of the samples is close to zero, but increases slightly with the increase of the substrate temperature, which is due to the enhancement of scattering effect in the crystalline ZnTiO3film.

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