Investigation of Carbon Fibre Reinforced Composites Based on Novel Phenylethynyl-Terminated Polyimde

2011 ◽  
Vol 415-417 ◽  
pp. 310-315
Author(s):  
Cheng Xia Tong ◽  
Guo Dong Dang ◽  
Chun Hai Chen ◽  
Hong Wei Zhou

As part of the continuing studies to develop high performance composite based on new kind of phenylethynyl end-capped imide oligomers for aerospace applications, PETI-type polyimide composites were prepared from carbon fibre (CF) and polyimide matrix resin derived from dianhydride (s-BPDA), 2,5-bis(4-aminophenoxy)-biphenyl(p-TPEQ) and 4-phenylethynylphthalic anhydride (PEPA). The mechanical properties were tested at both room temperature and 177 °C. The flexural properties were determined by 3-point-bending at room temperature. Thermal aging test was carried out by exposing samples at 177°C over 1000 hours, and the mechanical properties were also evaluated before and after isothermal aging. It was demonstrated that the composite had good thermal and mechanical properties.

2014 ◽  
Vol 666 ◽  
pp. 8-16
Author(s):  
A. Saad Najim ◽  
Mohammed Adwaa

This work deals with studying the mechanical properties specially fatigue behavior for high performance composite materials of poly ether ether ketone (PEEK)/glass fiber, which are used in Aircraft Industry. Two materials have been used: (PEEK natural) and (PEEK+30% glass fiber).To identify the type of (PEEK), infrared (FTIR) test has been conducted. X-ray test has been used to measure the (PEEK) crystalline ,also the tensile properties, impact strength and the fatigue test are performed.The results show that FTIR test peaks are for standard PEEK polymer and that GFRP increases the crystalline of (PEEK) material , while the tensile , impact and fatigue properties of (PEEK) decreases by adding GF to PEEK .


2001 ◽  
Vol 13 (4) ◽  
pp. 235-250 ◽  
Author(s):  
Roberto J Cano ◽  
Tan H Hou ◽  
Erik S Weiser ◽  
Terry L St Clair

Four NASA Langley-developed polyimide matrix resins, LaRC™-IA, LaRC™-IAX, LaRC™-8515 and LaRC™-PETI-5, were produced via a ‘salt-like’ process developed by Unitika Ltd. The salt-like solutions (65% solids in NMP) were prepregged onto Hexcel IM7 carbon fibre using the NASA LaRC™ multipurpose tape machine. Process parameters were determined and composite panels fabricated. The temperature dependent volatile depletion rates, the thermal crystallization behaviour and the resin rheology were characterized. Composite moulding cycles were developed which consistently yielded well consolidated, void-free laminated parts. Composite mechanical properties such as the short beam shear strength; the longitudinal and transverse flexural strength and flexural modulus; the longitudinal compression strength and modulus; and the open hole compression strength and compression after impact strength were measured at room temperature and elevated temperatures. The processing characteristics and the composite mechanical properties of the four intermediate modulus carbon fibre/polyimide matrix composites were compared to existing data on the same polyimide resin systems and IM7 carbon fibre manufactured via poly(amide acid) solutions (30–35% solids in NMP). This work studies the effects of varying the synthetic route on the processing and mechanical properties of the polyimide composites.


Forests ◽  
2021 ◽  
Vol 12 (5) ◽  
pp. 567
Author(s):  
Hong Yang ◽  
Mingyu Gao ◽  
Jinxin Wang ◽  
Hongbo Mu ◽  
Dawei Qi

In the absence of high-quality hardwood timber resources, we have gradually turned our attention from natural forests to planted fast-growing forests. However, fast-growing tree timber in general has defects such as low wood density, loose texture, and poor mechanical properties. Therefore, improving the performance of wood through efficient and rapid technological processes and increasing the utilization of inferior wood is a good way to extend the use of wood. Densification of wood increases the strength of low-density wood and extends the range of applications for wood and wood-derived products. In this paper, the effects of ultrasonic and vacuum pretreatment on the properties of high-performance wood were explored by combining sonication, vacuum impregnation, chemical softening, and thermomechanical treatments to densify the wood; then, the changes in the chemical composition, microstructure, and mechanical properties of poplar wood before and after treatment were analyzed comparatively by FT-IR, XRD, SEM, and mechanical tests. The results showed that with ultrasonic pretreatment and vacuum impregnation, the compression ratio of high-performance wood reached its highest level and the MOR and MOE reached their maximums. With the help of this method, fast-growing softwoods can be easily prepared into dense wood materials, and it is hoped that this new material can be applied in the fields of construction, aviation, and automobile manufacturing.


RSC Advances ◽  
2021 ◽  
Vol 11 (24) ◽  
pp. 14484-14494
Author(s):  
Yahao Liu ◽  
Jian Zheng ◽  
Xiao Zhang ◽  
Yongqiang Du ◽  
Guibo Yu ◽  
...  

We successfully modified graphene oxide with amino-terminated hyperbranched polyamide (HGO), and obtained a high-performance composite with enhanced strength and elongation at break via cross-linking hydroxyl-terminated polybutadiene chains with HGO.


Materials ◽  
2021 ◽  
Vol 14 (19) ◽  
pp. 5856
Author(s):  
Pragya Mishra ◽  
Pia Åkerfeldt ◽  
Farnoosh Forouzan ◽  
Fredrik Svahn ◽  
Yuan Zhong ◽  
...  

Laser powder bed fusion (L-PBF) has attracted great interest in the aerospace and medical sectors because it can produce complex and lightweight parts with high accuracy. Austenitic stainless steel alloy 316 L is widely used in many applications due to its good mechanical properties and high corrosion resistance over a wide temperature range. In this study, L-PBF-processed 316 L was investigated for its suitability in aerospace applications at cryogenic service temperatures and the behavior at cryogenic temperature was compared with room temperature to understand the properties and microstructural changes within this temperature range. Tensile tests were performed at room temperature and at −196 °C to study the mechanical performance and phase changes. The microstructure and fracture surfaces were characterized using scanning electron microscopy, and the phases were analyzed by X-ray diffraction. The results showed a significant increase in the strength of 316 L at −196 °C, while its ductility remained at an acceptable level. The results indicated the formation of ε and α martensite during cryogenic testing, which explained the increase in strength. Nanoindentation revealed different hardness values, indicating the different mechanical properties of austenite (γ), strained austenite, body-centered cubic martensite (α), and hexagonal close-packed martensite (ε) formed during the tensile tests due to mechanical deformation.


2018 ◽  
Vol 385 ◽  
pp. 39-44 ◽  
Author(s):  
Fernando Carreño ◽  
Oscar A. Ruano

The 7075 (Al-Zn-Mg-Cu) aluminium alloy is the reference alloy for aerospace applications due to its specific mechanical properties at room temperature, showing excellent tensile strength and sufficient ductility. Formability at high temperature can be improved by obtaining superplasticity as a result of fine, equiaxed and highly misoriented grains prone to deform by grain boundary sliding (GBS). Different severe plastic deformation (SPD) processing routes such as ECAP, ARB, HPT and FSP have been considered and their effect on mechanical properties, especially at intermediate to high temperatures, are studied. Refined grains as fine as 100 nm and average misorientations as high as 39o allow attainment of high strain rate superplasticity (HSRSP) at lower than usual temperatures (250-300oC). It is shown that increasing misorientations are obtained with increasing applied strain, and increasing grain refinement is obtained with increasing processing stress. Thus, increasing superplastic strains at higher strain rates, lower stresses and lower temperatures are obtained with increasing processing strain and, specially, processing stress.


2019 ◽  
Vol 815 ◽  
pp. 216-222
Author(s):  
Chao Chen ◽  
Jin Ming Liu ◽  
Yang Yang ◽  
Zhi Guo Guo

The ocean islands are far from inland and the concrete sandstone aggregates are scarce. In this paper, high-performance seawater all-coral concrete was developed by seawater mixing and room temperature maintenance design, and by optimizing the water-to-binder ratio, regulating internal curing, changing auxiliary cementing materials and blending ratio, incorporating expansion agent, adjusting fiber blending, etc. Combined with the consideration of work performance and mechanical properties, the concrete self-shrinkage is adjusted to further optimize the mix design. The mechanical properties of the optimized high-performance seawater all-coral concrete were studied, and the relevant durability tests were carried out according to the natural environment characteristics of the island. This is of great significance to the construction of island projects, repair and construction, and construction of protective projects [1].


2009 ◽  
Vol 79-82 ◽  
pp. 377-380
Author(s):  
Hong Yun Zhao ◽  
Guo Dong Wang ◽  
Chun Hua Xu ◽  
Feng Yuan Shu

After reheated at different temperatures for 5 minutes, the 400MPa Ultrafine Grained Steel specimens were air-cooled to room temperature, and then carried out the mechanical nanocrystallization surface treatment and structure performance testing. On the basis of comparing the test results on the specimens before and after the mechanical nanocrystallization surface treatment, the process of mechanical nanocrystallization was analyzed briefly. The results show that: as the reheating temperature rising, the trend of grain size growing increases markedly, and the mechanical properties also drop down to different degrees; when the reheating temperature is around 800°C, because of the pearlite spheroidized significantly, its mechanical properties drop the most seriously; after the mechanical nanocrystallization surface treatment, not only its surface form a layer of fine nano-layer (about 100 nm) structure, but also its mechanical properties rise obviously, and the yield strength is over 450MPa.


2017 ◽  
Vol 140 (1) ◽  
Author(s):  
Yanming Wang ◽  
Peng Cai ◽  
Tingmei Wang ◽  
Qihua Wang

Tribological and mechanical properties of aramid fiber (AF), graphite (Gr), and hexagonal boron nitride (h-BN) hybrid polyimide composites were investigated under room and high temperature. Results show that, Gr in composite reinforced with AF and h-BN can reduce coefficient of friction (COF) and improve antiwear property of composites under room temperature. Gr can accelerate the formation of transfer film under high temperature without sacrificing the wear resistant of composites. Transfer film of composites reinforced with Gr and h-BN simultaneously present more smooth and uniform compared with that of composites reinforced with only AF and h-BN. However, under higher temperature, composite reinforced with pure Gr present higher COFs and wear rates (WRs) compared with composites filled with h-BN and Gr simultaneously. Comprehensively, composite filled with 10% AF, 3% h-BN, and 4% Gr is the optimum composition.


2012 ◽  
Vol 226-228 ◽  
pp. 1709-1713
Author(s):  
Lan Yan ◽  
Y.M. Xing ◽  
Ji Jun Li

This paper investigated the high temperature mechanical properties of the hybrid fiber reinforced high performance concrete (HFHPC) and normal concrete (NC) .After being subjected to different elevated heating temperatures, two kinds of concretes have been tested for the compressive strength, splitting tensile strength and flexural strength of test specimen at room temperature and 200 °C,400 °C,600 °C,800 °C.Microstructure changes of concrete were also observed by using Scanning Electron Microscopy (SEM) after high temperature. The results show that the hybrid fiber can significantly increase mechanical properties of the concrete at room temperature and high temperature. SEM and XRD analysis shows that there is a permeable diffusion layer in the steel fiber surface because of solid state reaction in the Interfacial Transition Zone of steel fiber and concrete. This permeable diffusion layer is white, bright, serrated and mainly consist of FeSi2 and the complex hydrated calcium silicate. The compounds of this layer change the Interfacial Transition Zone structure, enhance bonding capacity of the steel fiber and matrix, and increase the high temperature mechanical properties of concrete.


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