Influence of PNA012 on Crystallization and Mechanical Properties of Polybutylene Terephthalate

2012 ◽  
Vol 624 ◽  
pp. 264-268 ◽  
Author(s):  
Duo You Zhang ◽  
Peng Liu ◽  
Chun Fa Ouyoung ◽  
Qun Gao ◽  
Kang Sheng Zheng ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Differential Scanning Calorimetry ◽  
Tensile Strength ◽  
Bending Strength ◽  
Testing Machine ◽  
Nucleating Agent ◽  
Polybutylene Terephthalate ◽  
Scanning Calorimetry ◽  
Universal Testing ◽  
Crystallization Degree

PNA012 is a new nucleating agent on polybutylene terephthalate. The effect of different dosage of PNA012 on crystallization and mechanical properties were investigated by means of differential scanning calorimetry, universal testing machine, melt flow indexer and vicat softening testing machine. It was revealed that the PNA012 could substantially accelerate the crystallization of PBT. Compared with the pure PBT,the crystallization temperature of PBT/PNA012 rises from 196.3 °C to 199.7 °C and crystallization degree from 34.2% to 39.9%. The tensile Strength of PBT/PNA012 is increased 9.7%. The Bending Strength has a rise of 9.3% and the heat distortion temperatures of PBT/PNA012 is increased from 115.07°C to 125.94°C.

scholarly journals Comparative Analysis of the Mechanical Properties between the Fiber-Reinforced Composite and Zirconium Posts

PRILOZI ◽  
2015 ◽  
Vol 36 (3) ◽  
pp. 138-149
Author(s):  
Vesna Jurukovska-Shotarovska ◽  
Biljana Kapusevska
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Comparative Analysis ◽  
Bending Strength ◽  
Testing Machine ◽  
Fracture Force ◽  
Fiber Reinforced Composite ◽  
Reinforced Composite ◽  
Universal Testing ◽  
Subgroup Ii

Abstract Objectives: To make a comparative analysis of the mechanical properties between FRC and zirconium posts Methods: The patients with FRC and zirconium posts were divided in two groups with three subgroups, each of them composed of 10 samples. Subgroup I with 1.2 mm; Subgroup II with 1.35 mm and Subgroup III with 1.5 mm post diameter. The fracture force, bending and tensile strength of each group were measured with Shimadzu Universal Testing Machine. Results: The fracture force for the first group measured in the first, second and third subgroup was 34.80900N; 67.15390N; 46.53100N and for the second group, first, second and third subgroup was 34.80900N; 46.53100N; 67.15390N correspondingly. The bending strength for the first group measured in the first, second and third subgroup was 401.4420N; 444.6425N; 333.6828N and for the second group, first, second and third subgroup was 307.9352N; 289.1030N; 304.1649N correspondingly. The tensile strength for the first group measured in the first, second and third subgroup was 5.442267N; 4.350545N; 2.943465N and for the second group, first, second and third subgroup was 4.224141N; 3.751466N; 3.168756N correspondingly. Conclusions: The longest diameter of the posts significantly increases the resistance to fracture in relation to the two smaller diameters. The larger diameter, the higher values of the bending strength, as well as the lowest values of the tensile strength of the material contribute to improved mechanical properties of the fiber and zirconium posts.

Influence of Novel Nucleating Agent on the Mechanical Properties and Crystallinity of Polyoxymethylene

2012 ◽  
Vol 466-467 ◽  
pp. 31-35 ◽  
Author(s):  
Li Zhong Jiang ◽  
Feng Dan Jiang ◽  
Jun Zhong Yang ◽  
Rui Kang Li ◽  
Yan Ping Hu
Keyword(s):  
Mechanical Properties ◽  
Growth Rate ◽  
Differential Scanning Calorimetry ◽  
Potential Application ◽  
Testing Machine ◽  
Nucleating Agent ◽  
Scanning Calorimetry ◽  
Mechanical Properties Testing

A novel nucleating agent for polyoxymethylene (POM) was successfully prepared. The effect of nucleating agent on POM was characterized by using mechanical properties testing machine and differential scanning calorimetry (DSC). The results demonstrate that the addition of nucleating agent can improve the crystallization growth rate and mechanical properties of POM, and the nucleating agent maybe have potential application in POM field.

Evaluating the Strength of the Friction Stir Welded Joints at Various Rotational Speeds

2013 ◽  
Vol 446-447 ◽  
pp. 312-315
Author(s):  
Ramaraju Ramgopal Varma ◽  
Abdullah Bin Ibrahim ◽  
B. Ravinder Reddy
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Friction Stir Welding ◽  
Yield Strength ◽  
Welded Joints ◽  
Rotational Speed ◽  
Testing Machine ◽  
Friction Stir ◽  
Universal Testing ◽  
Welding Technique

The present research paper aims in evaluating the strength of the welded AA6351 alloy plates of 6 mm thick by using friction stir welding technique at different rotational speeds The applied welding technique is capable of achieving the mechanical properties of the alloy close to that of the original alloy. In the present investigation, the speeds of the spindle were varied from 1100 rpm to 1500 rpm with a constant transverse speed of 20 mm/min. The tensile strength of the joints is determined by an universal testing machine. The results from the present investigation show that the values of the yield strength were very much closer to the values of the AA6351Alloy prior to welding. It has been found from the experiments that the strength of the joints increases with the increase in the rotational speed; however, the same is decreasing after achieving certain speed.

The Mechanical Properties and Thermodynamic Study on Polypropylene/Talc Composites

2014 ◽  
Vol 915-916 ◽  
pp. 751-754
Author(s):  
Shao Hui Wang
Keyword(s):  
Mechanical Properties ◽  
Differential Scanning Calorimetry ◽  
Tensile Strength ◽  
Electron Microscope ◽  
Impact Strength ◽  
Scanning Electron Microscope ◽  
Stearic Acid ◽  
Crystallization Rate ◽  
Scanning Calorimetry ◽  
Scanning Electron

The composites of PP/Talc modified by stearic acid were prepared and its effect on the properties of PP/Talc composites was investigated in this paper. The tensile strength and impact strength of PP/Talc composites increased about 15% and 30% compared with pure PP respectively. Based on surface analysis by scanning electron microscope (SEM), the Talcparticles buried well in PP matrix when the Talc was coated with the stearic acid. At the same time, it was found that Talc significantly increased the crystallization temperature and crystallization rate of PP by differential scanning calorimetry (DSC).

scholarly journals Properties Enhancement of High Molecular Weight Polylactide Using Stereocomplex Polylactide as a Nucleating Agent

Polymers ◽  
2021 ◽  
Vol 13 (11) ◽  
pp. 1725
Author(s):  
Purba Purnama ◽  
Muhammad Samsuri ◽  
Ihsan Iswaldi
Keyword(s):  
Mechanical Properties ◽  
Molecular Weight ◽  
Crystallization Behavior ◽  
Testing Machine ◽  
Nucleating Agent ◽  
Mechanical And Thermal Properties ◽  
Nucleating Agents ◽  
Thermal And Mechanical Properties ◽  
X Ray ◽  
Universal Testing

As one of the most attractive biopolymers nowadays in terms of their sustainability, degradability, and material tune-ability, the improvement of polylactide (PLA) homopolymer properties by studying the utilization of stereocomplex polylactide (s-PLA) effectively and efficiently is needed. In this sense, we have studied the utilization of s-PLA compared to poly D-lactide (PDLA) homopolymers as a nucleating agent for PLA homopolymers. The mechanical and thermal properties and crystallization behavior of PLA homopolymers in the presence of nucleating agents have been evaluated using a universal testing machine, differential scanning calorimeter, and X-ray diffractometer instruments, respectively. PDLA and s-PLA materials can be used to increase the thermal and mechanical properties of poly L-lactide (PLLA) homopolymers. The s-PLA materials increased the mechanical properties by increasing crystallinity of the PLLA homopolymers. PLLA/s-PLA enhanced mechanical properties to a certain level (5% s-PLA content), then decreased them due to higher s-PLA materials affecting the brittleness of the blends. PDLA homopolymers increased mechanical properties by forming stereocomplex PLA with PLLA homopolymers. Non-isothermal and isothermal evaluation showed that s-PLA materials were more effective at enhancing PLLA homopolymer properties through nucleating agent mechanism.

Evaluation of mechanical, morphological and thermal properties of waste rubber tire powder/LLDPE blends

e-Polymers ◽  
2008 ◽  
Vol 8 (1) ◽  
Author(s):  
Zhen Xiu Zhang ◽  
Shu Ling Zhang ◽  
Jin Kuk Kim
Keyword(s):  
Mechanical Properties ◽  
Thermal Properties ◽  
Testing Machine ◽  
Thermoplastic Elastomers ◽  
Linear Low Density Polyethylene ◽  
Scanning Calorimetry ◽  
Waste Rubber ◽  
Universal Testing ◽  
Rubber Tire ◽  
Thermal Stability Of

AbstractPolymer blends of WRT (waste rubber tire) powder/LLDPE (linear low density polyethylene) have been attempted to prepare thermoplastic elastomers (TPEs). The effects of maleic anhydride-grafted styrene-ethylene-butylene-styrene (SEBS-g-MA) and dicumyl peroxide (DCP) on mechanical, morphological and thermal properties of the blends were evaluated using universal testing machine (UTM), scanning electron microscopy (SEM), differential scanning calorimetry (DSC) and thermogravimetric analyses (TGA). It was found that combination of SEBS-g-MA and DCP could better enhance the mechanical properties of WRT powder/LLDPE blends compared to SEBS-g-MA or DCP alone. Better compatibility between WRT powder and LLDPE was responsible for the enhancement of mechanical properties, as supported by SEM. The incorporation of SEBS-g-MA and DCP with WRT powder/LLDPE blends reduced the crystallizable perfectness of the blends, but slightly increased the thermal stability of the blends, as shown from DSC and TGA results

Biomechanical changes of freezer-storaged and decellularized pig tracheal scaffoldings

2021 ◽  
pp. 088532822098566
Author(s):  
Jinping Wang ◽  
Haixiang Zhang ◽  
Yangmeng Feng ◽  
Yang Sun ◽  
Ruina Ma ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Testing Machine ◽  
Biomechanical Properties ◽  
Universal Testing ◽  
Significant Difference ◽  
Group A ◽  
Biomechanical Changes ◽  
Group B ◽  
Group D

Background As an excellent xenotransplant, the pig trachea can be decellularized and cryopreserved to reduce its immunogenicity. However, few reports are found on the changes of its mechanical properties after cryopreservation and decellularization. Objective To evaluate the structure and biomechanical properties in pig tracheal scaffolds resulting from decellularized and cryopreserved. Material and methods Twenty-five pig tracheal segments were separated into five groups: untreated (group A), only decellularized (group B), only cryopreserved (group C), decellularized after cryopreserved (group D) and cryopreserved after decellularized (group E). Tracheal segments were subjected to uniaxial tension or compression using a universal testing machine to determine structural biomechanical changes. Results It showed that there was no statistically significant difference in the tensile strength of the trachea in each group. The compressive strength of group B, C and D were same as the group A ( P > 0.05), while the group E was lower than that of the group A ( P < 0.05). Conclusions and significance: The histological examination of the decellularization after cryopreservation shows that the removal of epithelial cells and submucosal cells is more thorough, and the biomechanical structure of the trachea is better preserved. This proved to be a new method to prepare xenotransplantation of trachea graft.

Influence of Bagasse Carboxymethyl Cellulose Addition on the Thermal and Mechanical Properties of PLA Composites

2013 ◽  
Vol 747 ◽  
pp. 157-161
Author(s):  
S. Kamthai ◽  
Rathanawan Magaraphan
Keyword(s):  
Mechanical Properties ◽  
Differential Scanning Calorimetry ◽  
Tensile Strength ◽  
Carboxymethyl Cellulose ◽  
Room Temperature ◽  
Environmental Concern ◽  
Thermal And Mechanical Properties ◽  
Scanning Calorimetry ◽  
Melting Temperatures ◽  
Bagasse Waste

According to the availability of bagasse waste and increasing environmental concern, this research is focused on the preparation of polylactic acid (PLA)/bagasse carboxymethyl cellulose (CMCB) composite in order to improve the thermal and mechanical properties of PLA/CMCB film. PLA were mixed with CMCB at different ratios (1, 2, 4 and 8%, w/w of PLA), by kneading in two roll mills and then hot pressing into film. The results revealed that the addition of CMCB had significant effects on PLA composites properties. Differential scanning calorimetry (DSC) measurement indicated that the presence of CMCB accelerated the reduction of glass transition, and melting temperatures. Moreover the CMCB could improve the storage modulus of PLA composites at high temperature because its cold crystallization was developed. At room temperature, the tensile strength and elongation of PLA composite (but not modulus) were not significantly different with an increase of CMCB contents.

Study on the Mechanical Properties of ABS Enhanced by Magnesium Hydroxide Whiskers

2013 ◽  
Vol 300-301 ◽  
pp. 1289-1292
Author(s):  
Yu Zhi Jiang ◽  
Li Li Zhang ◽  
Zhong Yang Zhang ◽  
Li Hua Wang
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Elastic Modulus ◽  
Magnesium Hydroxide ◽  
Fracture Strength ◽  
Testing Machine ◽  
Fracture Morphology ◽  
Total Elongation ◽  
Zinc Stearate ◽  
Universal Testing

magnesium hydroxide whiskers; ABS; mechanical properties Abstract: The magnesium hydroxide (MH) whiskers/ABS composites were prepared by melt-extrusion with whiskers as fillers. Zinc stearate was used as modifier to improve the compatibility of the composites. The mechanical properties of ABS enhanced by different cotents of magnesium hydroxide whiskers were tested by the RGT-10 universal testing machine. When the content of whiskers was 10%, The comprehensive mechanical properties of the composites were the best, the max load was 0.30KN, the elastic modulus was 0.16Gpa, the tensile strength was 20.11Mpa, the total elongation was 10.24%, the fracture strength was 2.05Mpa. The fracture morphology of the composites was analyzed by SEM, the higher contents of magnesium hydroxide whisker, the worse-distributed whisker in ABS matrix.

scholarly journals Characterization of Fibers Produced from Blends of Polybutylene and Polypropylene

2007 ◽  
Vol 2 (3) ◽  
pp. 155892500700200 ◽  
Author(s):  
Robert L. Shambaugh ◽  
Diana L. Ortiz
Keyword(s):  
Mechanical Properties ◽  
Differential Scanning Calorimetry ◽  
Tensile Strength ◽  
Scanning Calorimetry ◽  
Stress Strain ◽  
Strain Behavior

Blends of polybutylene (PB-1) and polypropylene were used to produce fibers at spinning speeds of 800–2100 m/min. Concentrations ranged from 0% PP to 100% PP. The stress-strain behavior of the resultant fibers was examined, and the fibers were analyzed for crystallinity via DSC (differential scanning calorimetry). Fibers produced from blends of PB-1/PP show mechanical properties that are in between the properties of the pure polymers. The tensile strength of 50% PB-1 fibers is comparable to the tensile strength of pure PP fibers. Fibers produced from blend compositions of 25 and 75% have higher tensile strengths than pure PP fibers, although these blend compositions have lower tensile strengths than pure PB fibers.

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