Comparison of Mechanical Properties of Three Different Orthodontic Latex Elastic Bands Leached with NaOH Solution

2017 ◽  
Vol 730 ◽  
pp. 135-140
Author(s):  
Thipsupar Pureprasert ◽  
Niwat Anuwongnukroh ◽  
Surachai Dechkunakorn ◽  
Surapich Loykulanant ◽  
Chaveewan Kongkaew ◽  
...  

Orthodontic elastic bands made from natural rubber continue to be commonly used due to their favorable characteristics. However, there are concerns associated cytotoxicity due to harmful components released during conventional vulcanization (sulfur-based method). With the co-operation of The National Metal and Materials Technology Center (MTEC) and Faculty of Dentistry Mahidol University, a new method was introduced to reduce toxic components by leaching the orthodontic elastic bands with NaOH solution. The objective of this study was to evaluate the mechanical properties of Thai and commercial orthodontic elastic brands (Ormco and W&H) leached with NaOH solution. Three elastic brands (N =30, size 1⁄4 inch ,4.5 oz.) were tested for mechanical properties in terms of initial extension force, residual force, force loss, breaking strength and maximum displacement using a Universal Testing Machine. The results showed that force loss significantly decreased in Thai-LEACH and W&H-LEACH, whereas the values increased in Ormco-LEACH (P<0.05). The data exhibited a significantly decrease in breaking strength with Thai-LEACH and Ormco-LEACH, whereas all 3 brands revealed a significantly decrease in maximum displacement with the leaching process (P<0.05). In conclusion, leaching with NaOH solution is a new method, which can remove toxic components from orthodontic latex elastic bands. However, this process can affect their mechanical properties. Leached elastic bands from Thai had comparable properties with Ormco and have potential to be developed as a promising product.

2011 ◽  
Vol 378-379 ◽  
pp. 580-584
Author(s):  
N. Anuwongnukroh ◽  
Porntiwa Senarak ◽  
Surachai Dechkunakorn ◽  
Theeralaksna Suddhasthira ◽  
C. Kongkaew ◽  
...  

Introduction: The most widely used preservative system for natural rubber latex to date is the ammonia-based system preventing spontaneous coagulation and putrefaction due mainly to bacteria contamination. Objectives: The study compared 2 types of Thai orthodontic elastics, produced from natural rubber latex with different ammonia contents with commercial orthodontic elastics in terms of initial extension force, residual force, force loss, swelling index, breaking strength and maximum displacement. Materials and Methods: Thai orthodontic elastics were developed from 2 types of natural rubber latex; low ammonia < 0.15% (Thai-L), and high ammonia not < 0.6% (Thai-H). The mechanical properties of Thai orthodontic elastics were compared with commercial elastics (Ormco). Mechanical properties were tested using a universal testing machine (Instron 5566). Data were analyzed by One-way ANOVA and Tukey’s test compared the measurements among groups. Results: Ormco had the highest initial extension force and showed significant differences with Thai-L and Thai-H. Thai-L had the highest residual force but showed no significant difference compared with Ormco. Thai-L had the lowest percent of force loss and showed significant differences with Thai-H and Ormco. Thai-L had lower force loss than Thai-H. For swelling index, Thai-L had the highest elasticity. For breaking strength and maximum displacement, both Thai elastics met the Australian Standard (AS) for breaking strength and maximum displacement, similar to Ormco elastics. Conclusion: All elastics met the specifications of the AS for breaking strength and maximum displacement. Thai-L had comparable properties with commercial orthodontic elastics in terms of mechanical properties. Thai-L had comparable properties with Ormco in terms of mechanical properties and may be developed for orthodontic purposes.


2019 ◽  
Vol 814 ◽  
pp. 354-359
Author(s):  
Sasatorn Malanon ◽  
Surachai Dechkunakorn ◽  
Niwat Anuwongnukroh ◽  
Wassana Wichai

Orthodontic elastic bands are commonly made from natural rubber because they provide high resiliency at a reasonable cost. However, hypersensitivity related to protein present in latex have been reported in some patients which has led to increased usage of non-latex elastic alternatives. Therefore, the assessment of their mechanical properties is of importance. The objective of this study was to compare the physical and mechanical properties of three commercial latex and non-latex type orthodontic elastic bands. Samples of latex and non-latex type orthodontic elastics from manufacturers – AO (6.5oz), MASEL (6.0oz), GAC (6.0oz), with 3/16-inch diameter were selected. Firstly, the physical characteristics (width, cross-sectional thickness, and inner diameter) of the elastic bands were determined, following which their mechanical properties [initial extension force (F0), 24 h-residual force (F24), percentage of force decay, force exerted at 3 times the inner diameter (F3xID) and breaking force] were tested. The data were analyzed with Mann-Whitney U test and multiple comparisons among the groups were done with Kruskal-Wallis Test (p< 0.05). Significant differences were found in the physical characteristics and mechanical properties among each brand and type of elastics. AO elastic bands had significantly low F0 and F24 compared with the others. While the percentage of force decay at 24 h was greatest in AO followed by MASEL and GAC. Non-latex type elastics showed greater force decay than latex type ones, approximately 30-40% and 20-30% of the initial force in non-latex and latex type elastic, respectively. AO elastics showed the highest F3xID and also the lowest breaking force. Overall, non-latex type elastics exhibited lower breaking force compared to latex type ones. Wide variations were observed in the physical and mechanical characteristics among same manufacturer and same elastic type. All commercial brands presented higher F3xID than that stated by the manufacturers. Non-latex type elastics showed greater force decay over 24 h than latex type ones. The differences in the properties between the 2 types of the elastics could be due to the differences in their structure and polymers composition.


2011 ◽  
Vol 378-379 ◽  
pp. 668-673
Author(s):  
Surachai Dechkunakorn ◽  
Vantida Jittanonda ◽  
Niwat Anuwongnukroh ◽  
Theeralaksna Suddhasthira ◽  
Wassana Wichai ◽  
...  

Natural rubber latex products are used as orthodontic elastics but the increased incidence of latex allergies has led to the development of nonlatex orthodontic products. In Thailand, commercial nonlatex orthodontic elastics are not readily available and the cost of imported non latex products is relatively high. Thai non latex elasticshave been developedas alternative orthodontic products for latex-allergic patients and their costs are affordable.Objective: Tocomparethe mechanical properties of Thai nonlatex elastics with commercial natural latex orthodontic elastics for orthodontic application. Materials and Methods: Samples of imported latex orthodontic elastics [Ormco(USA), G&H (USA), Creative Orthodontics (China), Tomy Elastics (Japan)]were selected to compare their dimensional characteristics and mechanical properties with Thai non latex elastics. The dimensional characteristics of the elastics (i.e., inner diameter, cross-sectional thickness and cross-sectional area) were determined and their mechanical properties [(i.e., initial extension force (F0), 24 h- residual force (F24), percentage of force loss, force exerted at 3x the specified inner diameter(F3xID) and breaking force] were tested next. The data were analyzed with One-way ANOVA and multiple comparison by Tukey’s test was used among groups (p<0.05). Results:Significant differences of dimensional characteristics and mechanical properties were found among each brand of elastics. Thai non latex elastics had significantly different mechanical properties from natural latex elastics as reported in previous studies(p<0.05). Thai non latex elastics had the lowest initial extension force (0.82N), 24-h residual force (0.56 N) and breaking force (19.63 N, 8.183 MPa) but the highest percentage of force loss after 24 h (32.62%).However, the percentage of force loss was higher than commercial non latexelastics as previously reported. Conclusion:Thai nonlatex elastics were not comparable to those of the latex elasticsregardingmechanical properties;however,these are acceptable for orthodontic application. Therefore, the clinical selection of elastics should be based on the patient’s medical history and the specific mechanical properties of the type of elastic. Thai nonlatex orthodontic elastics can be a valid alternativefor patients with latex allergy in Thailand and this study contributes to the continuous development of Thai nonlatex orthodontic elastics.


2021 ◽  
Vol 36 (1) ◽  
pp. 204-208
Author(s):  
Dr.M. Mohan Prasad ◽  
Dr.S. Padmavathy ◽  
P. Gowshick ◽  
P. Kavinkumar ◽  
O.A. Kishore

In this examination the Mechanical Properties of Coconut Leaf Stalk Fibre Peduncle is found for the various lengths (3mm, 6mm, 9mm) are taken and treating with two different process. One set of fibre is washed with the distilled water and another set of fibre is treated with sodium hydroxide (NaOH) solution to increase the strength of the fibre. Here the NaOH mixer is about 5% are considered. After treatment the fibre are dried for 2 days and cut to the required sample size. All sample composite materials were made using the standard die (hand layup method) and samples were cut using high-pressure water jet cutter as per ASTM standard. The test was taken with ASTM D638, ASTM D790 and ASTM D256 standard Universal testing machine (UTM). The result exemplify that the 6 mm alkali-treated CPLSF (6 NTCPLSF) composite exhibited the maximum tensile strength of 26.14MPa, the flexural strength of 79.81MPa and impact strength (Izod) 9.7 kJ/m2.


Materials ◽  
2020 ◽  
Vol 14 (1) ◽  
pp. 155
Author(s):  
Régis Pamponet da Fonseca ◽  
Janaíde Cavalcante Rocha ◽  
Malik Cheriaf

The addition of natural fibers used as reinforcement has great appeal in the construction materials industry since natural fibers are cheaper, biodegradable, and easily available. In this work, we analyzed the feasibility of using the fibers of piassava, tucum palm, razor grass, and jute from the Amazon rainforest as reinforcement in mortars, exploiting the mechanical properties of compressive and flexural strength of samples with 1.5%, 3.0%, and 4.5% mass addition of the composite binder (50% Portland cement + 40% metakaolin + 10% fly ash). The mortars were reinforced with untreated (natural) and treated (hot water treatment, hornification, 8% NaOH solution, and hybridization) fibers, submitted to two types of curing (submerged in water, and inflated with CO2 in a pressurized autoclave) for 28 days. Mortars without fibers were used as a reference. For the durability study, the samples were submitted to 20 drying/wetting cycles. The fibers improved the flexural strength of the mortars and prevented the abrupt rupture of the samples, in contrast to the fragile behavior of the reference samples. The autoclave cure increased the compressive strength of the piassava and tucum palm samples with 4.5% of fibers.


2021 ◽  
Vol 13 (4) ◽  
pp. 2407
Author(s):  
Guang-Zhu Zhang ◽  
Xiao-Yong Wang ◽  
Tae-Wan Kim ◽  
Jong-Yeon Lim ◽  
Yi Han

This study shows the effect of different types of internal curing liquid on the properties of alkali-activated slag (AAS) mortar. NaOH solution and deionized water were used as the liquid internal curing agents and zeolite sand was the internal curing agent that replaced the standard sand at 15% and 30%, respectively. Experiments on the mechanical properties, hydration kinetics, autogenous shrinkage (AS), internal temperature, internal relative humidity, surface electrical resistivity, ultrasonic pulse velocity (UPV), and setting time were performed. The conclusions are as follows: (1) the setting times of AAS mortars with internal curing by water were longer than those of internal curing by NaOH solution. (2) NaOH solution more effectively reduces the AS of AAS mortars than water when used as an internal curing liquid. (3) The cumulative heat of the AAS mortar when using water for internal curing is substantially reduced compared to the control group. (4) For the AAS mortars with NaOH solution as an internal curing liquid, compared with the control specimen, the compressive strength results are increased. However, a decrease in compressive strength values occurs when water is used as an internal curing liquid in the AAS mortar. (5) The UPV decreases as the content of zeolite sand that replaces the standard sand increases. (6) When internal curing is carried out with water as the internal curing liquid, the surface resistivity values of the AAS mortar are higher than when the alkali solution is used as the internal curing liquid. To sum up, both NaOH and deionized water are effective as internal curing liquids, but the NaOH solution shows a better performance in terms of reducing shrinkage and improving mechanical properties than deionized water.


2021 ◽  
Vol 104 (2) ◽  
pp. 003685042110294
Author(s):  
Khaled Abd El-Aziz ◽  
Emad M Ahmed ◽  
Abdulaziz H Alghtani ◽  
Bassem F Felemban ◽  
Hafiz T Ali ◽  
...  

Aluminum alloys are the most essential part of all shaped castings manufactured, mainly in the automotive, food industry, and structural applications. There is little consensus as to the precise relationship between grain size after grain refinement and corrosion resistance; conflicting conclusions have been published showing that reduced grain size can decrease or increase corrosion resistance. The effect of Al–5Ti–1B grain refiner (GR alloy) with different percentages on the mechanical properties and corrosion behavior of Aluminum-magnesium-silicon alloy (Al–Mg–Si) was studied. The average grain size is determined according to the E112ASTM standard. The compressive test specimens were made as per ASTM: E8/E8M-16 standard to get their compressive properties. The bulk hardness using Vickers hardness testing machine at a load of 50 g. Electrochemical corrosion tests were carried out in 3.5 % NaCl solution using Autolab Potentiostat/Galvanostat (PGSTAT 30).The grain size of the Al–Mg–Si alloy was reduced from 82 to 46 µm by the addition of GR alloy. The morphology of α-Al dendrites changes from coarse dendritic structure to fine equiaxed grains due to the addition of GR alloy and segregation of Ti, which controls the growth of primary α-Al. In addition, the mechanical properties of the Al–Mg–Si alloy were improved by GR alloy addition. GR alloy addition to Al–Mg–Si alloy produced fine-grained structure and better hardness and compressive strength. The addition of GR alloy did not reveal any marked improvements in the corrosion properties of Al–Mg–Si alloy.


Sensors ◽  
2020 ◽  
Vol 21 (1) ◽  
pp. 145
Author(s):  
Lesław Kyzioł ◽  
Katarzyna Panasiuk ◽  
Grzegorz Hajdukiewicz ◽  
Krzysztof Dudzik

Due to the unique properties of polymer composites, these materials are used in many industries, including shipbuilding (hulls of boats, yachts, motorboats, cutters, ship and cooling doors, pontoons and floats, torpedo tubes and missiles, protective shields, antenna masts, radar shields, and antennas, etc.). Modern measurement methods and tools allow to determine the properties of the composite material, already during its design. The article presents the use of the method of acoustic emission and Kolmogorov-Sinai (K-S) metric entropy to determine the mechanical properties of composites. The tested materials were polyester-glass laminate without additives and with a 10% content of polyester-glass waste. The changes taking place in the composite material during loading were visualized using a piezoelectric sensor used in the acoustic emission method. Thanks to the analysis of the RMS parameter (root mean square of the acoustic emission signal), it is possible to determine the range of stresses at which significant changes occur in the material in terms of its use as a construction material. In the K-S entropy method, an important measuring tool is the extensometer, namely the displacement sensor built into it. The results obtained during the static tensile test with the use of an extensometer allow them to be used to calculate the K-S metric entropy. Many materials, including composite materials, do not have a yield point. In principle, there are no methods for determining the transition of a material from elastic to plastic phase. The authors showed that, with the use of a modern testing machine and very high-quality instrumentation to record measurement data using the Kolmogorov-Sinai (K-S) metric entropy method and the acoustic emission (AE) method, it is possible to determine the material transition from elastic to plastic phase. Determining the yield strength of composite materials is extremely important information when designing a structure.


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