Synthesis Edible Film Chitosan/Polyethylene Glycol/ Carboxymethylcellulose with Lemongrass Oils as Insect Ovipositing Repellent

2020 ◽  
Vol 840 ◽  
pp. 142-148
Author(s):  
M.G. Cinthya S. Perwita ◽  
Tutik Dwi Wahyuningsih ◽  
Endang Astuti ◽  
Deni Pranowo

Chitosan is a long linear chain polymer that has biodegradable properties. Chitosan can be found naturally in marine and terrestrial environments. However, chitosan as an edible film has brittle and weak properties. Therefore, addition of plasticizers such as polyethylene glycol and also emulsifiers such as carboxymethylcellulose (CMC) could improve the chitosan properties. In this study, the potency of modified chitosan as an edible film will be tested as an Insect Ovipositing Repellent (IOR) against B. carambolae fruit fly, which is known as one of the main pests on fruits in Southern East Asia. Chitosan-based films plasticized with polyethylene glycol, emulsified with carboxymethylcellulose and lemongrass oils as essential oils were prepared. Then the films was characterized; intermolecular interactions were determined by Fourier-transform infrared spectroscopy (FT-IR), surface morphology was observed by scanning electron microscopy (SEM), and the mechanical properties such as elongation, tensile strength, the thickness was tested using universal testing machine (UTM). Guava (Psidium guajava L), as a sample was used for testing the potential of chitosan film as IOR against the B. carambolae fruit fly. The addition of CMC and lemongrass oils to the chitosan/PEG films increased tensile strength and reduced elongation at break of the blended films. The best film resulted from composite of Chitosan/PEG/CMC/Lemongrass oil with a ratio of 1%/0.5%/0.1%/2%, and it is active as fruit fly repellent with IOA and ER of -0.745 and 85.412%, respectively.

Author(s):  
Giyatmi Giyatmi ◽  
Tika Annisa Eka Poetri ◽  
Hari Eko Irianto ◽  
Dina Fransiska ◽  
Agusman Agusman

Waste disposal problems have attracted scientists around the world to explore the use of renewable resources to produce biodegradable films and coatings. Indonesia has diverse renewable resources of biopolymers that originated from seaweeds such as carrageenan, agar, and alginate. Carrageenan is considered as a potential biopolymer for edible film manufacture due to its characteristic range. This study aimed to develop carrageenan-based edible film using alginate and polyethylene glycol as plasticizers. Edible film made from k-carrageenan with the addition of alginate and polyethylene glycol (PEG) as plasticizers was tested for its mechanical properties, water vapor transmission rate (WVTR) and water solubility.  Blending k-carrageenan with alginate (0%, 0.25%, 0.5%, 0.75%, and 1.0% w/v) increased tensile strength, thickness, and water solubility, but reduced elongation at break, WVTR, and moisture content. The addition of PEG (1%, 2%, and 3% w/v) reduced tensile strength and water solubility, but increased elongation at break, thickness, and moisture content. This study recommended that the best carrageenan-based edible film was obtained from a formula using 1% alginate (w/v) and 1% PEG (w/v).


Author(s):  
A. A. Gorbatovskiy

The article presents results of strength tests of bismuth telluride prismatic samples obtained by growing crystals. These crystals have semiconductor properties and are used in the heat machines, the run-ability of which largely depends on the strength of crystals. Data available in the literature are significantly different from each other. It has been shown that, the most consistent strength tests results are obtained in case of bend testing. The measurement results of the elasticity modulus and tensile strength are given. For tests, an INSTRON testing machine with maximum direct stress of the 1000 H was used.


2014 ◽  
Vol 6 (1) ◽  
pp. 27 ◽  
Author(s):  
Desi Mustika Amaliyah

Durian (Durio zibethinus) and cempedak (Artocarpus integer) peels waste are not used by the society. The research aim is to extract pectin from durian and cempedak peels and to formulate the pectin into edible films for food packaging. The research stages were first pre-treatment of durian and cempedak peels, pectin extraction, pectin drying, and  pectin application as edible films with concentration of 0%, 5%, and 15%. Based on this research it was concluded that pectin can be extracted from durian and cempedak peels with yield result of 27.97 % and 55.58 %, respectively. Edible film obtained has  similar characteristics between raw materials cempedak and durian peels. The higher concentration of cempedak peel  pectin increased the thickness, but decreased the tensile strength and elongation at a concentration of 15%. While in edible films from durian peel pectin, the higher concentration of pectin decreased the thickness of edible film on pectin concentration of 15%, lowered tensile strength and raised the edible film elongation.Keywords: waste, durian, cempedak, pectin extraction, edible film


1970 ◽  
pp. 01-04
Author(s):  
Esameldin B. M. Kabbashi, Ghada H. Abdelrahman and Nawal A. Abdlerahman

Guava (Psidium guajava L.) is a lovely tropical and subtropical fruit that originates in Mexico, Central America, and then taken to other distant and near parts around the world. In Sudan this popular fruit is produced in orchards and household and is so profitable but yet attacked by a lot of fruit fly species of the Genera Ceratitis and Bactrocera and the result is a loss of more than 70%. This research aimed at evaluating the effect of Gum Arabic coating (GAC) in extending the shelf life of guava fruit and disinfesting it from these notorious pests. Guava fruits from Kadaro orchards, Khartoum North, were tested using seven concentrations of Gum Arabic solutions. The results reflect that 1: 4 (25%) and 1: 8 (12.5%) (GA: water) concentrations attained 56 and 40% disinfestation, respectively whereas the other lower concentrations effected corresponding results in a range from 20 – 08%. The reduction in maggots per test fruit reached upto 188% as compared to the control.  The highest concentrations (1: 4 & 1: 8) effected a sustainability of 52% in fruit firmness (FF) with an average of medium (3) FF compared to soft FF (4) in the control. The corresponding results in other lower concentrations (1: 16; 1: 32; 1: 64; 1: 72 & 1: 96) were 36, 24, 24, 20 and 16%, respectively. In addition to an average FF of 4 (soft) for all these concentrations and 5 (very soft) for all the corresponding controls. Nevertheless, the sustainability of fruit color (FC) effected by the test concentrations was 52, 44, 24, 22, 24, 20, and 24%, respectively. Regarding these results, the two highest test concentrations effected a sizeable disinfestation and control of fruit flies and a good extension of shelf life of guava in Khartoum State. These findings support using this treatment as an effective IPM tool to extend guava fruit shelf life and upgrading its postharvest quality.


2019 ◽  
Vol 821 ◽  
pp. 89-95
Author(s):  
Wanasorn Somphol ◽  
Thipjak Na Lampang ◽  
Paweena Prapainainar ◽  
Pongdhorn Sae-Oui ◽  
Surapich Loykulnant ◽  
...  

Poly (lactic acid) or PLA was reinforced by nanocellulose and polyethylene glycol (PEG), which were introduced into PLA matrix from 0 to 3 wt.% to enhance compatibility and strength of the PLA. The nanocellulose was prepared by TEMPO-mediated oxidation from microcrystalline cellulose (MCC) powder and characterized by TEM, AFM, and XRD to reveal rod-like shaped nanocellulose with nanosized dimensions, high aspect ratio and high crystallinity. Films of nanocellulose/PEG/PLA nanocomposites were prepared by solvent casting method to evaluate the mechanical performance. It was found that the addition of PEG in nanocellulose-containing PLA films resulted in an increase in tensile modulus with only 1 wt% of PEG, where higher PEG concentrations negatively impacted the tensile strength. Furthermore, the tensile strength and modulus of nanocellulose/PEG/PLA nanocomposites were higher than the PLA/PEG composites due to the existence of nanocellulose chains. Visual traces of crazing were detailed to describe the deformation mechanism.


2015 ◽  
Vol 754-755 ◽  
pp. 1017-1022 ◽  
Author(s):  
Petrică Vizureanu ◽  
Mirabela Georgiana Minciună ◽  
Dragoş Cristian Achiţei ◽  
Andrei Victor Sandu ◽  
Kamarudin Hussin

.The paper present aspects about the obtaining of non-precious dental alloys (type CoCrMo and CoCrMoSi7), the determination of chemical composition by optical emission spectrometry and the experimental tests for determining the tensile strength, made on standard plate samples. The base material used in experiments was a commercial alloy, from CoCrMo system, which belongs to the class of dental non-precious alloys, intended to medical applications. The obtaining of studied alloy was made on arc re-melting installation, under vacuum, type MRF ABJ 900. The process followed to realize a rapid melting, with a maximum admissible current intensity. The samples for tests were obtained by casting in an electric arc furnace, under vacuum, in optimal conditions for melting and solidification and processing by electro-erosion, to eliminate all the disturbing factors which come by processing conditions for the samples. The determination of chemical composition for cobalt based alloys, by optical emission spectrometry, was made on SpectromaxX equipment with spark. The electrical discharge is made with the elimination of an energy quantity, fact which determine plasma forming and light issue. Tensile tests for standard samples, made from cobalt based alloy, was made on Instron 3382 testing machine, and assisted by computer. The obtained results are: elongation, elasticity modulus, tensile strength and offer complete information about the analyzed mechanical properties. For the certitude of obtained experimental results, the tests were made on samples with specific dimensions according ISO 6892-1:2009(E) standard, both for the tensile strength, and also machine operation.


2005 ◽  
Vol 127 (2) ◽  
pp. 257-262 ◽  
Author(s):  
William Jordan

This research project used hot embossing to create a strong and tough polymeric based composite structure. A honeycomb type structure was created by pressing small grooves into thin polycarbonate sheets. A trapezoidal die was used to create hexagonal shaped channels in the polymeric sheet. A number of these sheets were then bonded together to form a composite material. Carbon fibers were embedded into the channels in some of the laminates. The embossing process was carried out at an elevated temperature in an environmental chamber attached to an MTS servo hydraulic testing machine. The grooved structure had a 31% to 45% decrease in the apparent density compared to the ungrooved specimens. Bend tests, tensile tests, and Charpy impact tests were performed on laminates made from this material. The specific values of tensile strength, flexural modulus, and Charpy impact toughness were increased. A small percentage of fibers significantly increased both the stiffness and strength of the laminate.


Polymers ◽  
2021 ◽  
Vol 13 (9) ◽  
pp. 1406
Author(s):  
Daoyuan Chen ◽  
Mingjin Ding ◽  
Zhixiong Huang ◽  
Yanbing Wang

In order to study the dynamic mechanical properties of styrene–acrylic latex with a core/shell structure, a variety of latexes were synthesized by semi-continuous seeded emulsion polymerization based on “particle design” with the same material. The latexes were characterized by rotary viscosimeter, dynamic light scattering (DLS), Fourier transform infrared spectroscopy (FTIR), transmission electron microscope (TEM), dynamic mechanical analysis (DMA), and universal testing machine. The effects of difference at the glass transition temperature (Tg) of core and shell and the introduction of the “transition layer” on the damping and mechanical properties of latex film were studied. The results indicate that as the Tg of core and shell gets closer, the better the compatibility of core and shell, from phase separation to phase continuity. Furthermore, the introduction of the “transition layer” can effectively improve the tensile strength and tan δ (max) of the latex film. The tensile strength and maximum loss factor (f = 1 Hz) of latex with the “transition layer” increased by 36.73% and 29.11% respectively compared with the latex without the “transition layer”. This work provides a reference for the design of emulsion for damping coating.


2021 ◽  
Vol 410 ◽  
pp. 617-623
Author(s):  
Elena N. Gryadynova ◽  
Andrey V. Gorin ◽  
Alexey Yu. Rodichev

The article contains the analysis of thermoplastics used in prototyping machine parts. We used several types of experimental samples with different filling percentages. The equipment on which the experimental studies were carried out is shown. During the experiment, a specialized tensile testing machine was used. The experimental samples were installed in the developed centering device. Normal conditions were observed during the tests. The results of an experimental tensile study of PLA-plastic specimens are presented. The typical stress-strain diagram of an experimental sample is described, which describes the dependence of stress on relative deformation. An equation of the linear dependence of the tensile strength on the percentage of filament filling has been compiled, which makes it possible to determine the tensile strength of the product at any percentage of the filling of the plastic filament. The assessment is adequately verified by Fisher's criterion. Recommendations for filament filling in prototyping machine parts are given.


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