Liquid-Metal Foams – Feasible In Situ Experiments under Low Gravity

2006 ◽  
Vol 508 ◽  
pp. 275-280 ◽  
Author(s):  
N. Babcsán ◽  
F. Garcia-Moreno ◽  
D. Leitlmeier ◽  
John Banhart

Metal foams are quite a challenge to materials scientists due to their difficult manufacturing. In all processes the foam develops in the liquid or semiliquid state. Liquid-metal foams are complex fluids which contain liquid metals, solid particles and gas bubbles at the same time. An X-ray transparent furnace was developed to monitor liquid metal foam evolution. Aluminium foams - similar to the commercial Metcomb foams - were produced by feeding argon or air gas bubbles into an aluminium composite melt. The foam evolution was observed in-situ by X-ray radioscopy under normal gravity. Drainage and rupture were evaluated during the 5 min foam decay and 2 min solidification. Argon blown foams showed significant drainage and cell wall rupture during the first 20 s of foam decay. Air blown foams were stable and neither drainage nor rupture occurred. We demonstrated the feasibility of experiments during parabolic flight or drop tower campaigns. However, the development of a foam generator for low gravity is needed.

Author(s):  
N. Babcsán ◽  
F. Garcia-Moreno ◽  
D. Leitlmeier ◽  
John Banhart

Soft Matter ◽  
2014 ◽  
Vol 10 (36) ◽  
pp. 6955-6962 ◽  
Author(s):  
F. García-Moreno ◽  
S. T. Tobin ◽  
M. Mukherjee ◽  
C. Jiménez ◽  
E. Solórzano ◽  
...  

The foaming process of a thixocast AlSi6Cu4 precursor material followed in situ by X-ray radioscopy shown for different experimental stages with and without drainage during the plane parabolic trajectory and the corresponding temperature T(t) (red line) and gravity g(t) profiles (blue line) during the parabolas.


2007 ◽  
Vol 561-565 ◽  
pp. 1677-1680 ◽  
Author(s):  
Tomomi Ohgaki ◽  
Y. Takami ◽  
Hiroyuki Toda ◽  
Toshiro Kobayashi ◽  
Y. Suzuki ◽  
...  

Three-dimensional zinc mapping based on X-ray K-edge scanning has been performed. By microtomographies with energies above and below the K-absorption edges of the elements, the concentration distribution of the elements is evaluated during in-situ experiments, respectively. It is found that the Zn concentration distribution during the heat treatment was changed inside the cell wall of the aluminum foams and it has been homogenized. Also several precipitated phase transformation can be three-dimensionally visualized by the CT-method tuning X-ray energies.


Author(s):  
Thiago Piazera de Carvalho ◽  
Hervé P. Morvan ◽  
David Hargreaves

In aero engines, the oil and air interaction within bearing chambers creates a complex two-phase flow. Since most aero engines use a close-loop oil system and releasing oil out is not acceptable, oil-air separation is essential. The oil originates from the engine transmission, the majority of which is scavenged out from the oil pump. The remainder exits via the air vents, where it goes to an air oil separator called a breather. In metal-foam-style breathers separation occurs by two physical processes. Firstly the largest droplets are centrifuged against the separator walls. Secondly, smaller droplets, which tend to follow the main air path, pass through the metal foam where they ideally should impact and coalesce on the material filaments and drift radially outwards, by the action of centrifugal forces. Although these devices have high separation efficiency, it is important to understand how these systems work to continue to improve separation and droplet capture. One approach to evaluate separation effectiveness is by means of Computational Fluid Dynamics. Numerical studies on breathers are quite scarce and have always employed simplified porous media approaches where a momentum sink is added into the momentum equations in order to account for the viscous and/or inertial losses due to the porous zone [1]. Furthermore, there have been no attempts that the authors know of to model the oil flow inside the porous medium of such devices. Normally, breathers employ a high porosity open-cell metal foam as the porous medium. The aim of this study is to perform a pore-level numerical simulation on a representative elementary volume (REV) of the metal foam with the purpose of determining its transport properties. The pore scale topology is represented firstly by an idealized geometry, namely the Weaire-Phelan cell [2]. The pressure drop and permeability are determined by the solution of the Navier-Stokes equations. Additionally, structural properties such as porosity, specific surface area and pore diameter are calculated. The same procedure is then applied to a 3D digital representation of a metallic foam sample generated by X-ray tomography scans [3]. Both geometries are compared against each other and experimental data for validation. Preliminary simulations with the X-ray scanned model have tended to under predict the pressure drop when compared to in-house experimental data. Additionally, the few existing studies on flow in metal foams have tended to consider laminar flow; this is not the case here and this also raises the question that Reynolds-averaged turbulence models might not be well suited to flows at such small scales, which this paper considers.


Energies ◽  
2020 ◽  
Vol 13 (13) ◽  
pp. 3378
Author(s):  
Martin Beer ◽  
Marcela Taušová ◽  
Radim Rybár ◽  
Michal Kaľavský

The presented paper deals with the metal foams, which have a wide application potential ranging from power engineering, through catalysts to impact energy absorbers. The main aim of the paper is to propose an economical non-destructive method of determining the basic characteristics and dimensions using affordable devices. The basic principle of the proposed method lies in the image capture of metal foam and their subsequent analysis in image analysis software. An important element of the work is a comparison of results obtained by the proposed method with results obtained by high-resolution X-ray microtomography. The proposed method was evaluated in terms of measurement uncertainty and propagation of error in overall results. The use of the method is limited to the metal foams, characterized by an ordered structure, which are produced mainly by the electrophoretic deposition process. Based on the descriptive statistical analysis of results, it is possible to state, that the proposed method is in great agreement with accurate, but more expensive high-resolution X-ray microtomography.


2006 ◽  
Vol 514-516 ◽  
pp. 1678-1681 ◽  
Author(s):  
Nuno Franco ◽  
Eduardo Alves ◽  
Nuno P. Barradas

The Hotbird is a state of the art X-ray laboratory for advanced materials characterisation, installed at ITN since 1999. Several major improvements in its capabilities have been implemented. On the one hand, new hardware developments have extended the applications that can be studied and on the other hand, new software has enabled both enhanced automated control of the system, and improved data analysis that leads to extraction of further precise information from the data. One improvement was the implementation of the x-ray reflectometry (XRR) technique, which is a major expansion of the Hotbird capabilities. XRR is well-suited to characterise film thickness and roughness with high resolution. Furthermore, several optics improvements, such as a Göbel mirror and monochromators were introduced. The combination of this optics allows one to use either a higher intensity beam (orders of magnitude better) or a higher resolution beam configuration. A new high-temperature chamber was developed, which allows one to perform in-situ experiments with excellent temperature control up to 800 °C, in all possible configurations. Data simulation/fitting analysis software for XRR was developed. Also, to control the diffractometer and perform experiments, a new user-friendly software package was developed. In order to illustrate the Hotbird capabilities improvements, several experimental examples will be described.


2011 ◽  
Vol 208 (11) ◽  
pp. 2499-2504 ◽  
Author(s):  
A. N. Danilewsky ◽  
J. Wittge ◽  
A. Hess ◽  
A. Cröll ◽  
A. Rack ◽  
...  

2018 ◽  
Vol 20 (29) ◽  
pp. 19560-19571 ◽  
Author(s):  
Pietro Guccione ◽  
Luca Palin ◽  
Benny Danilo Belviso ◽  
Marco Milanesio ◽  
Rocco Caliandro

A new algorithm to extract in an automatic way kinetic parameters from a set of measurements from in situ experiments is presented and applied to X-ray powder diffraction and Raman spectroscopy.


Sign in / Sign up

Export Citation Format

Share Document