Thermal Stability of Ultrafine Grains in Al-Fe-Mn-Si Foils Prepared by ARB and Subsequent Rolling

2008 ◽  
Vol 584-586 ◽  
pp. 905-910 ◽  
Author(s):  
Petr Homola ◽  
Margarita Slámová ◽  
P. Sláma ◽  
Miroslav Cieslar

Accumulative Roll Bonding (ARB) is a severe plastic deformation process that allows producing ultrafine-grained materials (UFG). UFG sheets exhibit enhanced strength and very fine grain structure. Foils used as fins in heat exchangers have to be very thin but must exhibit high strength combined with relatively high formability. Thus, materials produced using ARB may fulfil the exacting requirements on foil properties for such applications. The thermal stability of Al-Fe- Mn-Si foils produced using ARB and subsequent cold rolling was studied and compared with conventionally cold rolled (CCR) counterparts. The stability was assessed by isothermal annealing in the temperature range from 200 to 450 °C. Electron back scatter diffraction in a scanning electron microscope and transmission electron microscopy examinations of foils microstructure in the deformed and annealed states allowed the monitoring of structural changes. The magnitude of mechanical properties changes due to annealing was evaluated by microhardness measurements. Significant hardness increase was observed after annealing at 200 °C only in the ARB samples and was assigned to an annealing-induced hardening. The CCR foil exhibits higher non-recrystallized fraction and smaller mean lamellae boundary spacing in the temperature interval of 200-250 °C than ARB foils. The annealing at 450 °C results in identical hardness values and fully recrystallized microstructure of all foils, regardless the method used for their manufacturing. However, the ARB samples show higher stability of the refined substructure than their cold rolled counterparts due to continuous recrystallization occurring in the ARB foils.

2007 ◽  
Vol 546-549 ◽  
pp. 917-922
Author(s):  
Bao Lin Wu ◽  
Gui Ying Sha ◽  
Yi Nong Wang ◽  
Yu Dong Zhang ◽  
Claude Esling

Heavy deformation plus micro alloying could be an effective way to obtain ultrafine grain structure of metals. In the present work, an Al-Cu-Mg alloy was microalloyed with Zr to obtain homogeneous precipitates and then heavily deformed by conventional forging at high temperature. The possible refining processing routes were studied and the superplasticity behaviors of the alloy was investigated. Results show that the micro alloyed alloy can be stably refined to 3-5μm under conventional processing routes. The Al-3Zr precipitates act both as additional sites to enhance recrystallization nucleation rate and pins to impede grain growth to increase the thermal stability of the fine grain structure. However, as the Al3Zr precipitates remains along grain boundaries, the superplastic capability of the material is not high. At 430°C with 1×10-4S-1 strain rate, the elongation obtained was 260%.


2010 ◽  
Vol 667-669 ◽  
pp. 241-246
Author(s):  
Rolf Berghammer ◽  
Wei Ping Hu ◽  
Arman Hasani ◽  
Günter Gottstein

An aluminum alloy with two different precipitation states was processed by Equal Channel Angular Pressing up to 16 passes. The thermal stability of the ultra-fine grain structure was examined during annealing at 300°C up to 1 h. As the present precipitates are coarse they don’t contribute to strengthening where as soluted elements improved the strength of the material. Additionally the soluted elements formed dispersoids upon annealing and thereby retarded softening.


Author(s):  
Shiro Fujishiro ◽  
Harold L. Gegel

Ordered-alpha titanium alloys having a DO19 type structure have good potential for high temperature (600°C) applications, due to the thermal stability of the ordered phase and the inherent resistance to recrystallization of these alloys. Five different Ti-Al-Ga alloys consisting of equal atomic percents of aluminum and gallium solute additions up to the stoichiometric composition, Ti3(Al, Ga), were used to study the growth kinetics of the ordered phase and the nature of its interface.The alloys were homogenized in the beta region in a vacuum of about 5×10-7 torr, furnace cooled; reheated in air to 50°C below the alpha transus for hot working. The alloys were subsequently acid cleaned, annealed in vacuo, and cold rolled to about. 050 inch prior to additional homogenization


Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 2903
Author(s):  
Juvenal Giogetti Nemaleu Deutou ◽  
Rodrigue Cyriaque Kaze ◽  
Elie Kamseu ◽  
Vincenzo M. Sglavo

The present project investigated the thermal stability of cold-setting refractory composites under high-temperature cycles. The proposed route dealt with the feasibility of using fillers with different particle sizes and studying their influence on the thermo-mechanical properties of refractory geopolymer composites. The volumetric shrinkage was studied with respect to particle sizes of fillers (80, 200 and 500 µm), treatment temperature (1050–1250 °C) and amount of fillers (70–85 wt.%). The results, combined with thermal analysis, indicated the efficiency of refractory-based kyanite aggregates for enhancing thermo-mechanical properties. At low temperatures, larger amounts of kyanite aggregates promoted mechanical strength development. Flexural strengths of 45, 42 and 40 MPa were obtained for geopolymer samples, respectively, at 1200 °C, made with filler particles sieved at 80, 200 and 500 µm. In addition, a sintering temperature equal to 1200 °C appeared beneficial for the promotion of densification as well as bonding between kyanite aggregates and the matrix, contributing to the reinforcement of the refractory geopolymer composites without any sign of vitrification. From the obtained properties of thermal stability, good densification and high strength, kyanite aggregates are efficient and promising candidates for the production of environmentally friendly, castable refractory composites.


1990 ◽  
Vol 112 (1) ◽  
pp. 10-15 ◽  
Author(s):  
M. I. Flik ◽  
C. L. Tien

Intrinsic thermal stability denotes a situation where a superconductor can carry the operating current without resistance at all times after the occurrence of a localized release of thermal energy. This novel stability criterion is different from the cryogenic stability criteria for magnets and has particular relevance to thin-film superconductors. Crystals of ceramic high-temperature superconductors are likely to exhibit anisotropic thermal conductivity. The resultant anisotropy of highly oriented films of superconductors greatly influences their thermal stability. This work presents an analysis for the maximum operating current density that ensures intrinsic stability. The stability criterion depends on the amount of released energy, the Biot number, the aspect ratio, and the ratio of the thermal conductivities in the plane of the film and normal to it.


Author(s):  
Stephanie Saalfeld ◽  
Thomas Wegener ◽  
Berthold Scholtes ◽  
Thomas Niendorf

AbstractThe stability of compressive residual stresses generated by deep rolling plays a decisive role on the fatigue behavior of specimens and components, respectively. In this regard, deep rolling at elevated temperature has proven to be very effective in stabilizing residual stresses when fatigue analysis is conducted at ambient temperature. However, since residual stresses can be affected not only by plastic deformation but also when thermal energy is provided, it is necessary to analyze the influence of temperature and time on the relaxation behavior of residual stresses at elevated temperature. To evaluate the effect of deep rolling at elevated temperatures on stability limits under thermal as well as combined thermo-mechanical loads, the present work introduces and discusses the results of investigations on the thermal stability of residual stresses in differently deep rolled material conditions of the steel SAE 1045.


Author(s):  
Mehdi Soltan Ali Nezhad ◽  
Sadegh Ghazvinian ◽  
Mahmoud Amirsalehi ◽  
Amir Momeni

Abstract Three steels were designed based on HSLA-100 with additional levels of Mn, Ni, Cr and Cu. The steels were prepared by controlled rolling and tempered at temperatures in range of 550–700°C. The continuous cooling time curves were shifted to longer times and lower temperatures with the increased tendency for the formation of martensite at lower cooling rates. The microstructures revealed that controlled rolling results in austenite with uniform fine grain structure. The steel with the highest amount of Mn showed the greatest strength after tempering at 750 °C. The top strength was attributed to the formation of Cu-rich particles. The steel with 1.03 wt.% Mn, tempered at 650 °C exhibited the best Charpy impact toughness at –85°C. On the other hand, the steel that contained 2.11 wt.% Mn and tempered at 700 °C showed the highest yield strength of 1 097.5 MPa (∼159 ksi) and an impact toughness of 41.6 J at –85°C.


2021 ◽  
Vol 233 ◽  
pp. 02046
Author(s):  
Xiaoxue Fan ◽  
Ming Cheng ◽  
Xiaoning Zhang ◽  
Cunfang Wang ◽  
Hua Jiang

This paper aimed to evaluate the changes in the thermal stability of goat milk, cow milk and homogenized milk under different pH conditions. The results showed that goat milk was of type B milk, and the thermal stability were positively correlated with the pH value. But cow milk was of type A milk, the most stable pH of fresh milk was 6.9, while it was 6.7 for homogenized cow milk. Compared with cow milk, the acidification of goat milk was stronger due to heat. Therefore, in the process of milk production, the germicidal heating conditions of two different milk sources should be determined according to their thermal stability.


1989 ◽  
Vol 160 ◽  
Author(s):  
B. Elman ◽  
Emil S. Koteles ◽  
P. Melman ◽  
C.A. Armiento ◽  
C. Jagannath

AbstractWe present a study of the structural stability of InGaAs/GaAs strained single quantum wells (SQW) grown with a variety of indium compositions and with well widths close to critical thickness values. The samples were grown by molecular beam epitaxy and were subjected to furnace annealing as well as ion implantation followed by rapid thermal annealing. Changes in low temperature photoluminescence linewidths were used to evaluate the stability of strained SQWs. We observed both strain relief, in wide SQWs and strain recovery, in higher indium composition narrow quantum wells which were partially relaxed (low dislocation density) as-grown.


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