Preparation and Research of α-Fe/Montmorillonite Magnetic Material

2014 ◽  
Vol 809-810 ◽  
pp. 433-437
Author(s):  
Cheng Cheng Shi ◽  
Long Gui Peng ◽  
Zhi Wang
Keyword(s):  
Magnetic Material ◽  
Particle Size ◽  
Composite Material ◽  
Saturation Magnetization ◽  
Average Particle Size ◽  
Average Particle ◽  
X Ray Diffraction ◽  
Layer Spacing ◽  
Particle Size Analyzer

α-Fe/montmorillonite (MMT) magnetic material was successfully prepared by the in-situ pillared-reduction method. The composite material was characterized by X-ray diffraction (XRD), laser particle size analyzer and other instruments. The magnetic property was researched by saturation magnetization. The results showed that: when 0.1mol/L hydroxyl-Fe was added as pillared agent, hydroxyl-Fe and cation of the MMT exchanged, leading to the inter-layer spacing expanded to 1.41nm and reached saturated pillared point. MMT interlayer hydroxyl-Fe was completely restored to α-Fe grains of 116nm when reducing agent was 0.2mol/L and produced α-Fe/MMT composite material. The average particle size of the composite was 5.529μm, the specific saturation magnetization was 0.812emu/g (9×103A/moutside magnetic field) and exhibited ferromagnetism.

Preparation of Nano-Kaolinite and Mechanism

2011 ◽  
Vol 204-210 ◽  
pp. 1217-1220
Author(s):  
Shu Li Ding ◽  
B.H. Xu ◽  
Q.F. Liu ◽  
Y.Z. Sun
Keyword(s):  
Particle Size ◽  
Average Particle Size ◽  
Potassium Acetate ◽  
Basal Spacing ◽  
Average Particle ◽  
X Ray Diffraction ◽  
Particle Size Analyzer ◽  
Intercalation Complexes ◽  
Space Expansion ◽  
Crystal Space

With potassium acetate as an intercalation agent, kaolinite-potassium acetate(KAc) intercalation complexes was prepared. Afterwards, nano-kaolinite was successfully made through exfoliated intercalation complexes using power ultrasonic. The intermediate and final products were characterized by X-ray diffraction(XRD), infrared spectroscopy(IR), laser particle size analyzer, and scanning electron microscope (SEM). The results show that intercalation of KAc into kaolinite resulted in a crystal space expansion, from a basal spacing of 7.14Ǻ to 14.20 Ǻ, and the intercalation rate was about 80%. KAc intercalation causes the weakening of interlayer stability. It was shown that the particles of nano-kaolinite is very thin lamellar in shape, whose average thickness, average particle size, are 50 nm and 450 nm respectively.

scholarly journals Thermal, Structural, and Physical Properties of Freeze Dried Tropical Fruit Powder

2014 ◽  
Vol 2014 ◽  
pp. 1-10 ◽  
Author(s):  
K. A. Athmaselvi ◽  
C. Kumar ◽  
M. Balasubramanian ◽  
Ishita Roy
Keyword(s):  
Particle Size ◽  
Physical Properties ◽  
Average Particle Size ◽  
Average Particle ◽  
X Ray Diffraction ◽  
Tropical Fruit ◽  
X Ray ◽  
Freeze Dried ◽  
Fruit Powder ◽  
Lcr Meter

This study evaluates the physical properties of freeze dried tropical (guava, sapota, and papaya) fruit powders. Thermal stability and weight loss were evaluated using TGA-DSC and IR, which showed pectin as the main solid constituent. LCR meter measured electrical conductivity, dielectric constant, and dielectric loss factor. Functional groups assessed by FTIR showed presence of chlorides, and O–H and N–H bonds in guava, chloride and C–H bond in papaya, and chlorides, and C=O and C–H bonds in sapota. Particle size and type of starch were evaluated by X-ray diffraction and microstructure through scanning electronic microscopy. A semicrystalline profile and average particle size of the fruit powders were evidenced by X-ray diffraction and lamellar/spherical morphologies by SEM. Presence of A-type starch was observed in all three fruits. Dependence of electric and dielectric properties on frequency and temperature was observed.

scholarly journals Synthesis of MgO Nanoparticles by Solvent Mixed Spray Pyrolysis Technique for Optical Investigation

2014 ◽  
Vol 2014 ◽  
pp. 1-4 ◽  
Author(s):  
K. R. Nemade ◽  
S. A. Waghuley
Keyword(s):  
Particle Size ◽  
Spray Pyrolysis ◽  
Spray Pyrolysis Technique ◽  
Average Particle Size ◽  
Band Gap Energy ◽  
Average Particle ◽  
Optical Investigation ◽  
X Ray Diffraction ◽  
Mgo Nanoparticles ◽  
Electron Microscope Analysis

Solvent mixed spray pyrolysis technique has attracted a global interest in the synthesis of nanomaterials since reactions can be run in liquid state without further heating. Magnesium oxide (MgO) is a category of the practical semiconductor metal oxides, which is extensively used as catalyst and optical material. In the present study, MgO nanoparticles were successfully synthesized using a solvent mixed spray pyrolysis. The X-ray diffraction pattern confirmed the formation of MgO phase with an excellent crystalline structure. Debye-Scherrer equation is used for the determination of particle size, which was found to be 9.2 nm. Tunneling electron microscope analysis indicated that the as-synthesized particles are nanoparticles with an average particle size of 9 nm. Meanwhile, the ultraviolet-visible spectroscopy of the resulting product was evaluated to study its optical property via measurement of the band gap energy value.

scholarly journals Effect of soil textural characteristics on longitudinal dispersion in saturated porous media

2021 ◽  
Vol 69 (2) ◽  
pp. 161-170
Author(s):  
Mojtaba G. Mahmoodlu ◽  
Amir Raoof ◽  
Martinus Th. van Genuchten
Keyword(s):  
Particle Size ◽  
Dispersion Coefficient ◽  
Average Particle Size ◽  
Longitudinal Dispersion ◽  
Average Particle ◽  
Sand Sample ◽  
Average Pore ◽  
Advection Dispersion ◽  
Strong Positive Relationship

Abstract This study focuses on the effects of soil textural heterogeneity on longitudinal dispersion under saturation conditions. A series of solute transport experiments were carried out using saturated soil columns packed with two filter sands and two mixtures of these sands, having d50 values of 95, 324, 402, and 480 µm, subjected to four different steady flow rates. Values of the dispersion coefficient (D) were estimated from observed in-situ distributions of calcium chlo-ride, injected as a short nonreactive tracer pulse, at four different locations (11, 18, 25, 36 cm). Analyses of the observed distributions in terms of the standard advection-dispersion equation (ADE) showed that D increased nonlinearly with travel distance and higher Peclet numbers+. The dispersion coefficient of sand sample S1 with its largest average particle size (d 50) was more affected by the average pore-water velocity than sample S4 having the smallest d 50. Results revealed that for a constant velocity, D values of sample S1 were much higher than those of sample S4, which had the smallest d 50. A correlation matrix of parameters controlling the dispersion coefficient showed a relatively strong positive relationship between D and the Peclet number. In contrast, almost no correlation was evident between D and porosity as well as grain size. The results obtained with the four sandy matrices were consistent and proved that the dispersion coefficient depends mainly on the particle size.

Fe3O4 Magnetic Preparation by Bauxite Ore Washing Fine Mud

2014 ◽  
Vol 1010-1012 ◽  
pp. 961-965
Author(s):  
Jian Qiang Xiao ◽  
Guo Wei He ◽  
Yan Jin Hu
Keyword(s):  
Particle Size ◽  
Aging Time ◽  
Average Particle Size ◽  
Xrd Analysis ◽  
Test Methods ◽  
Raw Material ◽  
Molar Ratio ◽  
Average Particle ◽  
Experimental Conditions ◽  
Particle Size Analyzer

Bauxite waste sludge as a raw material, the use of reverse chemical coprecipitation synthesize Fe3O4. Researching temperature, precipitation concentration, aging time and Fe2+/Fe3+ molar ratio effect on the particle size, morphology. Optimal experimental conditions: temperature 70 °C, the precipitant NaOH mass ratio of 10%, aging time 3h, Fe2+/Fe3+ molar ratio of 2:3. Test methods using a laser particle size analyzer, XRD analysis of the products were characterized, the product is Fe3O4, the average particle size of 0.11mm.

scholarly journals Preparation of ultrafine iron phosphate micro-powder from phosphate slag

2018 ◽  
Vol 238 ◽  
pp. 02002
Author(s):  
Fangjing Sun ◽  
Yi Zhang ◽  
Jiawei Zhang ◽  
Xixi Yan ◽  
Xiaoyu Liu ◽  
...  
Keyword(s):  
Aqueous Solution ◽  
Particle Size ◽  
Electron Microscope ◽  
Average Particle Size ◽  
Iron Phosphate ◽  
Average Particle ◽  
X Ray ◽  
Particle Size Analyzer ◽  
Phosphate Slag ◽  
Scanning Electron

In this experiment, ultrafine iron phosphate micro-powder was prepared by hydrothermal method which used phosphate slag as an iron source. The effects of reaction temperature, surfactants type and amount on its particle size were explored. The samples were characterized by using Malvern Laser Particle Size Analyzer (MS2000), X-Ray Diffractometer (XRD), Scanning Electron Microscope (SEM) and Energy Dispersive X-Ray Spectroscopy (EDX).The results showed that at 160 °C, 1 wt%CTAB, monoclinic iron phosphate micro-powder was obtained with an average particle size about 0.4 μm which also has a good dispersion in aqueous solution.

Facile Synthesis and Characterization of Fe-Co Nanoparticles Supported Silica Rice Husk

2016 ◽  
Vol 709 ◽  
pp. 66-69
Author(s):  
Jeyashelly Andas ◽  
Rahmah Atikah Rosdi ◽  
Nur Izzati Mohd Anuar
Keyword(s):  
Particle Size ◽  
Rice Husk ◽  
Sol Gel ◽  
Average Particle Size ◽  
Average Particle ◽  
Silica Source ◽  
Transmission Electron ◽  
Particle Size Analyzer ◽  
Bimetallic Materials ◽  
Co Nanoparticles

A series of Fe-Co nanoparticles were synthesized via sol-gel route at acidic, neutral and basic condition using rice husk as the silica source. The synthesized nanomaterials were designated as Fe-Co3, Fe-Co7 and Fe-Co9 and characterized by Fourier Transform Infrared (FTIR), Transmission Electron Microscope (TEM) and particle size analyzer. The great effect of pH was clearly evidenced from the shifting in the siloxane bond in the FTIR spectrum. TEM investigation confirmed the existence of discrete and almost sphere like nanoparticles. The particle size decreased with an increase in the pH, registering the smallest average particle size at pH 9. In brief, this study promises a fast, rapid and promising method for the conversion of silica rice husk into nanoscale bimetallic materials.

Molten Salt Synthesis of CaCu3Ti4O12

2008 ◽  
Vol 368-372 ◽  
pp. 115-117 ◽  
Author(s):  
Ke Pi Chen ◽  
Yong He ◽  
Dong Yu Liu ◽  
Zong De Liu
Keyword(s):  
Particle Size ◽  
Molten Salt ◽  
Average Particle Size ◽  
Particle Morphology ◽  
Holding Time ◽  
Molten Salt Synthesis ◽  
Average Particle ◽  
Molten Salt Method ◽  
Particle Size Analyzer ◽  
Size And Morphology

CCTO powders were prepared by using molten salt method in the NaCl-KCl system. The effects of temperature and holding time on phase compositions, particle morphology and size have been investigated by X-ray diffraction, scanning electron microscope and laser particle size analyzer. Using CaCO3, CuO and TiO2 as starting materials, CCTO compound could be synthesized at any temperature from 800oC to 1000oC in the NaCl-KCl system. The average particle size increased obviously with the increasing of temperature above 850 oC. Holding time had great effect on grain size and morphology.

Frequency dependence and fuel effect on optical properties of nano TiO2-based structures

2016 ◽  
Vol 30 (18) ◽  
pp. 1650247 ◽  
Author(s):  
Mahdi Ghasemifard ◽  
Misagh Ghamari ◽  
Meysam Iziy
Keyword(s):  
Particle Size ◽  
Optical Properties ◽  
Average Particle Size ◽  
Combustion Method ◽  
Average Particle ◽  
X Ray Diffraction ◽  
Nano Tio2 ◽  
Transmission Electron ◽  
Auto Combustion ◽  
Xrd Patterns

TiO2-(Ti[Formula: see text]Si[Formula: see text]O2 nanopowders (TS-NPs) with average particle size around 90 nm were successfully synthesized by controlled auto-combustion method by using citric acid/nitric acid (AC:NA) and urea/metal cation (U:MC). The structure of powders was studied based on their X-ray diffraction (XRD) patterns. The XRD of TS-NPs shows that rutile and anatase are the main phases of TS-NPs for AC:NA and U:MC, respectively. Particle size and histogram of nanopowders were characterized by transmission electron microscopy (TEM) and dynamic light scattering (DLS). Optical properties of TS-NPs were calculated by Fourier transform infrared spectroscopy (FTIR) and Kramers–Kroning (KK) relation. Plasma frequencies of TS-NPs obtained from energy loss functions depend on fuels as a result of changes in crystal structure, particle size distribution, and morphology.

Effect of Surfactant on the Preparation of Nano-powder for Yb Doping Laser Transparent YAG Ceramic

2013 ◽  
Vol 32 (5) ◽  
pp. 511-515 ◽  
Author(s):  
Xiao Guo Cao ◽  
Jia Wang ◽  
Qi Bai Wu ◽  
Hai Yan Zhang
Keyword(s):  
Particle Size ◽  
Polyethylene Glycol ◽  
Average Particle Size ◽  
Ammonium Bicarbonate ◽  
Spherical Particles ◽  
Precipitation Method ◽  
Average Particle ◽  
X Ray Diffraction ◽  
Nano Powder ◽  
Co Precipitation

AbstractYb:YAG transparent ceramic nano-powder was prepared by chemical co-precipitation method, with ammonium bicarbonate as the precipitant and polyethylene glycol as surfactant. The addition of polyethylene glycol can reduce the agglomeration and particle size of the prepared Yb:YAG powder. The morphology, thermal stability and phase structure of Yb:YAG nano-powder were charactered by scanning electron microscopy (SEM), thermogravimetry and differential thermal analysis (TG-DTA), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy. The results show that well-crystallized nano-powder was obtained by calcining the precursors at 900 °C for 3 h. The average particle size of Yb:YAG powder is about 100–200 nm. When the volume amount of polyethylene glycol is 2.0%, well-dispersed Yb:YAG powder with spherical particles of 100 nm diameter was obtained.

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