Experimental Statistics Applied to Porous Ceramics Processing

2018 ◽  
Vol 912 ◽  
pp. 230-233
Author(s):  
Déborah Caroline de Oliveira ◽  
Patrícia Neves Mendes ◽  
Lucas Marcello Godinho ◽  
Sylma Carvalho Maestrelli ◽  
Ana Gabriela Storion

Statistical techniques are particularly useful in the engineering, objecting the optimization of fabrication processes. This paper had the purpose of evaluating if the variables such as mechanical resistance, linear shrinkage, apparent porosity, density and water absorption are influenced by the amount of peat added to refractory clay, to ensure the porosity on the production of porous ceramics used as ceramic filters. In order to treat the data it was used the technique of variance analysis, with the regression analysis and the Scott-Knott test. According to the variance analysis, there were some differences between the treatments for all properties analyzed and, by the regression analysis, optimum peat levels were found for all properties analyzed, for some properties these levels were considered inadequate for being superior to the limit stablished.

2018 ◽  
Vol 15 (1) ◽  
pp. 59-69
Author(s):  
K.G. Akpomie ◽  
C.C. Ezeofor ◽  
O.L. Alum ◽  
U.A. Augustine ◽  
F.N. Ibeanu

The effect of Dioscorea rotundata peel environmental waste as an insulating additive for local clay was studied. The potential of a low cost indigenous clay mineral obtained from Akpugu-Ezedike in Nigeria for industrial application was also evaluated. The clay was characterized by the Fourier transform infrared spectroscopy, X-ray diffraction and Scanning electron microscopy (SEM). Prepared slurry mixture of the clay and peels were shaped, dried and fired. The chemical composition of the clay was determined by classical methods. Physical properties such as linear shrinkage, total shrinkage, modulus of rupture, apparent density, bulk density, apparent porosity,s welling index and water absorption, modulus of plasticity and refractoriness of the fired samples were determined. The clay was found to have a refractoriness of 12000C. SEM analysis revealed an increase in porosity of the fired clay bodies with increase in dosage of Dioscorea rotundata added. This result was corroborated by the high apparent porosity 49.67 – 60.02% and water absorption recorded 30.92 – 48.44% for the mixed fired samples. The result of this study clearly indicated the potential of Dioscorea rotundata peel as additive in enhancing insulating properties of fired clay as well as the usefulness of the local clay mineral for industrial purposes.


2020 ◽  
Vol 1012 ◽  
pp. 250-255
Author(s):  
Wendell Bruno Almeida Bezerra ◽  
Fabio da Costa Garcia Filho ◽  
Artur Camposo Pereira ◽  
Sergio Neves Monteiro ◽  
M.T. Marvila ◽  
...  

Residues incorporation into construction building materials is a promising sustainable alternative for the correct disposal of this kind of material. Brazil is one of the largest world producers of ornamental stones. Nevertheless, the disposal of these residues usually is made outside the industry, which contributes to environmental pollution. This work aimed to evaluate the incorporation of residues from the marble industry into ceramic bricks. Specimens of clay ceramic containing 10, 20, 30 and 40 wt.% of marble residue were prepared and fired at 900oC. The evaluation of the ceramic bricks added with marble residue was based on linear shrinkage, water absorption and mechanical resistance. These properties were compared with Brazilian standards. It was concluded that the incorporation of marble residues, with up to 20 wt%, into the ceramic body is technically feasible and positively influences the properties of the material.


2015 ◽  
Vol 1120-1121 ◽  
pp. 38-42
Author(s):  
Daniel Véras Ribeiro ◽  
S.C. Figueiredo ◽  
Alexandre T. Machado ◽  
F.R. Valenzuela Diaz ◽  
C.A.C. Souza

Rotary-vacuum-filter mud (RVFM) is waste generated during the manufacturing process of titanium dioxide. In this work, RVFM and ceramic bricks containing different ratios of this waste are investigated. The mud samples were characterized using thermal analysis (TG/DTG). The aim of the present work was to determine the effect of adding RVFM on the ceramic properties of clay, such as apparent porosity, water absorption, linear shrinkage and flexural strength, used to produce blocks and tiles. Samples were dried out at 110°C and fired at 800°C, 950°C and 1100°C. The addition of RVFM tends to increase the apparent porosity and water absorption and to decrease the flexural strength of the ceramic specimens. Based on the results, ceramic specimens with 20% RVFM content burned at 800°C can not be used as bricks, and ceramic specimens with 20% RVFM content fired at 800°C and 950°C can not be used as tiles, according to Brazilian standards.


2006 ◽  
Vol 530-531 ◽  
pp. 432-437
Author(s):  
M.A.F. Ramalho ◽  
R.R. Almeida ◽  
Lisiane Navarro de Lima Santana ◽  
Hélio Lucena Lira ◽  
H.C. Ferreira ◽  
...  

Recycling of residues from different industrial process as new raw materials has been studied by several institutions to be applied in the production of ceramic bricks, roof tile. The aim of this work is to study the potentiality of the residues from granite and kaolin industries as raw materials to obtain ceramic tile. The raw materials were fired at temperatures of 1100oC, 1120oC and 1150oC. After fired the specimens were submitted to a physical and mechanical tests, such as, linear shrinkage, mechanical resistance, water absorption and apparent density. The results show that the residues can be used in the composition of the paste to produce ceramic tiles.


Clay Minerals ◽  
2012 ◽  
Vol 47 (2) ◽  
pp. 165-175 ◽  
Author(s):  
M. Medhioub ◽  
W. Hajjaji ◽  
M. Hachani ◽  
A. Lopez-Galindo ◽  
F. Rocha ◽  
...  

AbstractThis study aims to find alternatives to some overexploited deposits in the north of Tunisia. The clays of the Sidi Khalif formation, of Uppermost Jurassic to Lower Cretaceous age, seem suitable to support this strategy, due to their abundance. In terms of mineralogy, they can be divided into two distinct groups, related to their palaeogeographic and eustatic contexts. The clays of the Sidi Khalif formation from Jebel Houareb (JH) and Jebel Meloussi (JM) are richer in clay minerals, while those of Jebel Rhouis (JR) and Jebel Boudinar (JB) zones are dolomite-rich. The compositional differences between the two groups influenced their technological behaviour in production of ceramic tiles. Upon firing, forsterite and gehlenite crystallized in the carbonate-rich JR and JB clays, whereas mullite formed in the JH and JM clays. Concerning their ceramic properties, the tiles made from JR or JB clays showed low bending strength and high water absorption. For JH and JM, the tiles had slightly greater mechanical resistance, but exhibited considerable linear shrinkage. These defects were partially corrected by introducing new formulations based on the same clays and by altering the firing cycles (HM1, HM2, RB1 and RB2). With these modifications, “Porcelanico” and “Monoporosa” technologically conforming tiles were obtained from HM2 and RB2 formulations, respectively.


2021 ◽  
Vol 49 (1) ◽  
pp. 23-30
Author(s):  
Asotah Wisdom ◽  
Udochukwu Mark ◽  
Elakhame Zeberu ◽  
Abraham Adeleke

Optimisation of the physical properties of rice husk ash (RHA) in ceramic materials was carried out using Response Surface Methodology. The independent variables, namely the firing temperature and residue content, were statistically combined in a Central Composite Design with the effects on water absorption, linear shrinkage, bulk density, apparent porosity and apparent specific gravity determined. Physical and microstructural analyses were carried out to obtain information on the processes that occurred within the ceramic materials. The results obtained were analysed to determine the optimum physical properties of the ceramic materials within the range investigated. The residue content had a significant influence (at 95% confidence level) on the bulk density, water absorption, apparent porosity and apparent specific gravity but not on the linear shrinkage. The firing temperature had a more significant effect on the linear shrinkage than on the residue content, so that when elevated it contributed to an increase in linear shrinkage. The optimum residue content and firing temperature to enhance physical properties within the range investigated were 5.85% RHA and 1029.64°celsius, respectively. These optimal conditions are expected to produce a ceramic material with a bulk density, linear shrinkage, apparent porosity, water absorption and apparent specific gravity of 1.64 g/cm3, 0.29%, 0.29 g/cm3, 18.26% and 2.11, respectively with a composite desirability of 100%.


2020 ◽  
Vol 9 (9) ◽  
pp. e69996773
Author(s):  
Maria Gabriela Araujo Ranieri ◽  
Maria Auxiliadora de Barros Martins ◽  
Patrícia Capellato ◽  
Mirian de Lourdes Noronha Motta Melo ◽  
Adilson da Silva Mello

The modern lifestyle has led to an increase in the amount of solid waste in the world, and waste tires are one of the most generated. Annually billions of tons of waste tires are produced, so in this study, we sought to reuse them to make materials for civil construction. For this, a laboratory research was carried out where samples were made in 50 x 100 mm cylinders with traces of 0, 10, 15 and 20% (by weight) of waste, in addition to cement, natural sand and water. The granulometric distribution of waste tires and sand was also carried out. And, with the samples in cylinders, the physical and mechanical properties were evaluated, such as water absorption and apparent density, in addition to the analysis of the mechanical resistance to compression and the modulus of elasticity. The results showed that the granulometric distribution of the tire residue fits as a fine aggregate, similar to the sand granulometry. The water absorption rate of the waste specimens was less than 10%. However, the mechanical resistance decreases proportionally as the amount of tire waste has increased. However, when analyzing the behavior of the stress x strain curves, the specimens containing residues, became more flexible, as they are capable of supporting loads beyond the maximum stress. In this way, the resistance and the ability to absorb energy were increased. We concluded that it is possible to incorporate certain quantities of waste tires in blocks for civil construction, but without a structural function.


2011 ◽  
Vol 43 (1) ◽  
pp. 81-94 ◽  
Author(s):  
M. Vlasova ◽  
I. Rosales ◽  
M. Kakazey ◽  
Parra Parra ◽  
R. Guardian

Porous ceramics (bricks) was obtained using red clay, milled fusible cullet, and biowaste in the temperature range 950-1000?C. The high content of water in biowaste eliminates the necessity of introducing water in soft mud forming of bricks. The porosity, water absorption capacity, and mechanical properties of the prepared ceramics depend on content of milled cullet and sintering temperature.


2021 ◽  
Author(s):  
Herbet Alves Oliveira

Lightweight concrete has as main characteristic its low density due to the incorporation of light materials such as expanded clay, or even the incorporation of air whose function is to reduce the density, characteristic of cellular concrete. In Aracaju city, there are companies that promote tire reconditioning, generating large amounts of waste dust. The aim of this work is to study the reuse of tire rubber waste in light concrete from expanded clay. An experimental program was developed for the analysis of these concretes, varying the percentage of 1%, 2.5% and 5% of the tire rubber waste to replace the natural fine aggregate and 100% replacing the natural coarse aggregate by expanded clay (50% of expanded clay C1506 and 50% of C2215). The materials (cement, sand, expanded clays and tire rubber waste) were characterized through tests of particle size analysis and unit mass. The hardened concrete was evaluated through mechanical tests of axial compression strength, modulus of elasticity and tensile strength by diametrical compression, physical tests of water absorption and specific mass, in addition to image analysis by scanning electron microscopy. The use of expanded clay with incorporation of 1% of tire rubber waste guaranteed better results in mechanical resistance, lower water absorption and greater specific mass than the mixtures with 2.5 and 5%, reaching values close to the reference concrete. Thus, the residue can be an alternative for reuse, avoiding disposal.


Author(s):  
Adegbenle Bukunmi O

Laterite samples from Ede area with particle components of 19.7% clay, 32.8% silt and 47.5% sand was stabilized with combined cement, lime and bitumen and test for Compressive strength, Linear Shrinkage, Permeability and Water Absorption. The stabilizers were mixed with laterite soil in different ratios and percentage. The laterite carried 90% which is constant while the three stabilizers shared the remaining 10% in varying form. After 28 days of curing, laterite stabilizer with 90% of laterite, 8% of cement, 1% lime and 1% bitumen (LCLB1) possessed compressive strength of 2.01N/mm2. It Water Absorption Capacity was 3.05%. LCLB4 stabilizer (90% laterite, 6% cement, 2% lime and 2% bitumen) has the same compressive strength with LCLB1 stabilizer but with a high Water Absorption Capacity of 4.2%. The stabilizer of 90% laterite, 3.33% cement, 3.33% lime and 3.33% of bitumen (LCLB8) has the lowest compressive strength of 0.74N/mm2 and the highest Water Absorption Capacity of 5.39%. The results shows that LCLB1 stabilizer is a better stabilizer for strength and blocks made from laterite stabilized with it stand a good alternative to sand Crete blocks in building constructions. The combination of these stabilizers in order to determine a most economical volume combination for optimum performance is highly possible and economical.


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