Microstructure and Deposition Relations in Alumina Particle Strengthened Ni-W Matrix Composites

2012 ◽  
Vol 186 ◽  
pp. 234-238 ◽  
Author(s):  
Paulina Indyka ◽  
Ewa Beltowska-Lehman ◽  
Magdalena Bieda ◽  
Jerzy Morgiel ◽  
Leszek Tarkowski
Keyword(s):  
Composite Coatings ◽  
Metallic Matrix ◽  
Electrolyte Solutions ◽  
Ultrasonic Field ◽  
Matrix Composites ◽  
Field Frequency ◽  
Plating Bath ◽  
Electron Microscopies ◽  
The Matrix ◽  
Average Size

The nanostructured Ni-W/Al2O3 composite coatings were prepared by electrodeposition technique on ferritic steel substrates from aqueous electrolyte solutions containing ultrafine alumina particles in suspension. The effects of plating parameters like current density, inert particle concentration in plating bath and ultrasonic field frequency on the incorporation of α-Al2O3 particles (TM-DAR Taimicron) into an Ni-W matrix were investigated. The MMC coatings microstructure, phase and chemical composition were studied by means of scanning (E-SEM FEI XL-30) and transmission (TECNAI G2 SuperTWIN) electron microscopies, as well as XRD measurements (Bruker D8 Discover). SEM and TEM observations of composite cross-section microstructure showed that the presence of ultrasounds considerably reduces the particles agglomeration and enables a uniform distribution of particles in the Ni-W matrix. The electron diffraction pattern analysis revealed that the composite metallic matrix consists of an α-Ni(W) solid solution. The matrix was characterized by quasifibrous, nanocrystalline grains of an average size about 10 nm.

Fracture Mechanics Characterization of Sintered 30 Vol.-% Al2O3/TRIP Steel Composites Using SENB Miniature Samples

2015 ◽  
Vol 825-826 ◽  
pp. 899-906 ◽  
Author(s):  
Ralf Eckner ◽  
Alexander Illgen ◽  
Markus Radajewski ◽  
Lutz Krüger
Keyword(s):  
Trip Steel ◽  
Metallic Matrix ◽  
Stable Crack Growth ◽  
Ceramic Particle ◽  
Mechanical Tests ◽  
Matrix Composites ◽  
Operational Design ◽  
The Matrix ◽  
Microstructural Studies

Ceramic particle reinforced metal matrix composites (PRMMCs) combine the strength and brittleness of ceramics with the toughness of a metallic matrix. In order to use these materials in construction and operational design their fracture mechanical behavior must be evaluated. In this study, a 30 vol.-% Al2O3 reinforced austenitic TRIP steel processed by powder metallurgical technique was investigated using precracked miniature SENB-specimens in 3-point-bending. An elastic-plastic analysis by means of the J-integral method in combination with optical crack observation showed the materials ability of stable crack growth, i. e. R-curve behavior. In addition to the mechanical tests microstructural studies were performed, whereby particle debonding and fracture as well as martensitic phase transformation and crack bridging within the matrix were identified as fracture energy dissipating mechanisms.

Effect of Mg Content on the Characteristics of Al/SiC Nanocomposite Powders Produced via In Situ Powder Metallurgy Method

2011 ◽  
Vol 471-472 ◽  
pp. 420-425 ◽  
Author(s):  
Mohammad Moazami-Goudarzi ◽  
Farshad Akhlaghi
Keyword(s):  
Powder Metallurgy ◽  
Influencing Factor ◽  
Metallic Matrix ◽  
Matrix Alloy ◽  
Powder Metallurgy Method ◽  
Sic Particles ◽  
The Matrix ◽  
Average Size ◽  
Mg Content

In the present study the effect of Mg addition on the characteristics of Al/SiC nanocomposite powder particles produced via a relatively new method called in situ powder metallurgy (IPM) is investigated. Commercially pure Al and Al-Mg alloy melts containing different amounts of Mg were used as the matrix alloy. Nano-sized SiC particles with the average size of 60 nm were used as the reinforcing material. The effect of Mg content on the fluidity of the melt as an influencing factor affecting both the process yield and wettability of SiC with molten metal was investigated. The size distribution of produced powders was characterized using a laser particle size analyzer. Scanning electron microscopy was utilized to investigate the possibility of embedding of SiC nanoparticles within the metallic matrix. Results of microhardness measurements together with SEM micrographs and EDS analysis showed that nano-sized SiC particles could be embedded in the relatively coarse Al-Mg powders containing at least 1 wt.% Mg.

Effect of SiC particle size on the microstructure and properties of cold-sprayed Al/SiCp composite coating

2017 ◽  
Vol 31 (16-19) ◽  
pp. 1744027 ◽  
Author(s):  
Min Yu ◽  
Junwei Hua
Keyword(s):  
Particle Size ◽  
Wear Resistance ◽  
Kinetic Energy ◽  
Composite Coating ◽  
Composite Coatings ◽  
Cold Spraying ◽  
Cohesion Strength ◽  
The Matrix ◽  
Average Size ◽  
Sic Particle

The Al5056/SiC composite coatings were prepared by cold spraying. Experimental results show that the SiC content in the composite coating deposited with the SiC powder having an average size of 67 [Formula: see text]m (Al5056/SiC-67) is similar to that deposited with the SiC powder having an average size of 27 [Formula: see text]m (Al5056/SiC-27). The microhardness and cohesion strength of Al5056/SiC-67 coating are higher than those of the Al5056/SiC-27 coating. In addition, the Al5056/SiC-67 coating having a superior wear resistance because of the coarse SiC powder with a superior kinetic energy contributes to the deformation resistance of the matrix Al5056 particles.

Morphology and growth mechanism of alumina whiskers in aluminum-based metal matrix composites

1999 ◽  
Vol 14 (7) ◽  
pp. 2997-3000 ◽  
Author(s):  
Y-F. Li ◽  
C-D. Qin ◽  
D. H. L. Ng
Keyword(s):  
Metal Matrix Composite ◽  
Matrix Composite ◽  
Internal Oxidation ◽  
Growth Mechanism ◽  
Metal Matrix ◽  
Oxidation Reaction ◽  
Intermetallic Phases ◽  
Matrix Composites ◽  
The Matrix ◽  
Average Size

A process has been invented for growing alumina (Al2O3) whiskers in the matrix of the aluminum-based metal matrix composite by the internal oxidation reaction between aluminum (Al) and molybdenum oxide (MoO3) at 850 °C. The whiskers were formed during the firing stage and distributed uniformly throughout the metal matrix. The fractional volume of the whiskers was about 30%, and their average size was 1 μm in diameter and 10 μm in length. The growth mechanism of the Al2O3 whiskers was studied. It was found that the nutrient for the growth of the whiskers was supplied from the molten Al at the base of the whiskers where they reacted with MoO3 forming the Al2O3 whiskers and the Al–Mo intermetallic phases.

Preparation of Electron Transparent Metal-Matrix Composites

1968 ◽  
Vol 26 ◽  
pp. 334-335 ◽  
Author(s):  
M. R. Pinnel ◽  
A. Lawley
Keyword(s):  
Stainless Steel ◽  
Load Transfer ◽  
Volume Fraction ◽  
Steel Wire ◽  
Initial Step ◽  
Interfacial Region ◽  
Matrix Composites ◽  
Specific Test ◽  
The Matrix ◽  
The One

Numerous phenomenological descriptions of the mechanical behavior of composite materials have been developed. There is now an urgent need to study and interpret deformation behavior, load transfer, and strain distribution, in terms of micromechanisms at the atomic level. One approach is to characterize dislocation substructure resulting from specific test conditions by the various techniques of transmission electron microscopy. The present paper describes a technique for the preparation of electron transparent composites of aluminum-stainless steel, such that examination of the matrix-fiber (wire), or interfacial region is possible. Dislocation substructures are currently under examination following tensile, compressive, and creep loading. The technique complements and extends the one other study in this area by Hancock.The composite examined was hot-pressed (argon atmosphere) 99.99% aluminum reinforced with 15% volume fraction stainless steel wire (0.006″ dia.).Foils were prepared so that the stainless steel wires run longitudinally in the plane of the specimen i.e. the electron beam is perpendicular to the axes of the wires. The initial step involves cutting slices ∼0.040″ in thickness on a diamond slitting wheel.

Deformation at interfaces of Ti-6Al-4V/SiC fiber composites

1992 ◽  
Vol 50 (1) ◽  
pp. 158-159
Author(s):  
Warren J. Moberly ◽  
Daniel B. Miracle ◽  
S. Krishnamurthy
Keyword(s):  
Thermal Stresses ◽  
Load Transfer ◽  
Coefficient Of Thermal Expansion ◽  
Hot Isostatic Pressing ◽  
Matrix Composites ◽  
Ongoing Research ◽  
Aerospace Applications ◽  
Sic Fiber ◽  
The Matrix ◽  
Intermetallic Matrix Composites

Titanium-aluminum alloy metal matrix composites (MMC) and Ti-Al intermetallic matrix composites (IMC), reinforced with continuous SCS6 SiC fibers are leading candidates for high temperature aerospace applications such as the National Aerospace Plane (NASP). The nature of deformation at fiber / matrix interfaces is characterized in this ongoing research. One major concern is the mismatch in coefficient of thermal expansion (CTE) between the Ti-based matrix and the SiC fiber. This can lead to thermal stresses upon cooling down from the temperature incurred during hot isostatic pressing (HIP), which are sufficient to cause yielding in the matrix, and/or lead to fatigue from the thermal cycling that will be incurred during application, A second concern is the load transfer, from fiber to matrix, that is required if/when fiber fracture occurs. In both cases the stresses in the matrix are most severe at the interlace.

Effect of graphene nano-platelets on mechanical and impact characteristics of carbon/Kevlar reinforced epoxy hybrid nanocomposites

2021 ◽  
pp. 095440622110168
Author(s):  
Mohamad Alsaadi ◽  
Bashar Younus ◽  
Ahmet Erklig ◽  
Mehmet Bulut ◽  
Omer Bozkurt ◽  
...  
Keyword(s):  
Impact Test ◽  
Charpy Impact ◽  
Hybrid Nanocomposites ◽  
Matrix Composites ◽  
Sem Images ◽  
The Matrix ◽  
Impact Characteristics ◽  
Positive Effect ◽  
Hybrid Carbon ◽  
Composite Samples

The influence of various graphene nano-platelets (GNPs) content on the tensile, flexural and Charpy impact characteristics of carbon, Kevlar and hybrid carbon/Kevlar fibers reinforced epoxy matrix composites was investigated. Both of composite configurations as carbon and Kevlar at outer and core skins were experimentally tested. The SEM images for flexural specimens were taken to observe the adhesion mechanism of GnPs particles with fiber/epoxy system. It is found that hybridization with Kevlar layers is contributed a positive effect on the hybrid carbon/Kevlar laminate structures in terms of tensile, flexural and impact behaviour. The incorporation of GnPs particles in hybrid and non-hybrid composite samples results in significant improvements in tensile, flexural and impact properties, and the greatest improvement occurs within the GnPs particle content of 0.1 and 0.25 wt%, indicating that the interfacial bonding between the matrix and the fibers is better due to the large surface area of the GnPs and the good entanglement between the GnPs layers and the matrix chains. The samples of impact test are experimented for edgewise and flatwise directions.

scholarly journals Characterization of the Structure, Mechanical Properties and Erosive Resistance of the Laser Cladded Inconel 625-Based Coatings Reinforced by TiC Particles

Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2225
Author(s):  
Aleksandra Kotarska ◽  
Tomasz Poloczek ◽  
Damian Janicki
Keyword(s):  
Laser Cladding ◽  
Inconel 625 ◽  
Matrix Composites ◽  
Erosion Rates ◽  
Laser Cladding Process ◽  
Composition Variation ◽  
The Matrix ◽  
Reinforcing Material ◽  
Inconel 625 Superalloy

The article presents research in the field of laser cladding of metal-matrix composite (MMC) coatings. Nickel-based superalloys show attractive properties including high tensile strength, fatigue resistance, high-temperature corrosion resistance and toughness, which makes them widely used in the industry. Due to the insufficient wear resistance of nickel-based superalloys, many scientists are investigating the possibility of producing nickel-based superalloys matrix composites. For this study, the powder mixtures of Inconel 625 superalloy with 10, 20 and 40 vol.% of TiC particles were used to produce MMC coatings by laser cladding. The titanium carbides were chosen as reinforcing material due to high thermal stability and hardness. The multi-run coatings were tested using penetrant testing, macroscopic and microscopic observations, microhardness measurements and solid particle erosive test according to ASTM G76-04 standard. The TiC particles partially dissolved in the structure during the laser cladding process, which resulted in titanium and carbon enrichment of the matrix and the occurrence of precipitates formation in the structure. The process parameters and coatings chemical composition variation had an influence on coatings average hardness and erosion rates.

Effect of temperature on matrix multicracking evolution of C/SiC fiber-reinforced ceramic-matrix composites

2020 ◽  
Vol 39 (1) ◽  
pp. 189-199
Author(s):  
Longbiao Li
Keyword(s):  
Strain Energy ◽  
Ceramic Matrix Composites ◽  
Critical Value ◽  
Matrix Cracking ◽  
Interface Debonding ◽  
Matrix Composites ◽  
Temperature Dependent ◽  
Damage State ◽  
The Matrix ◽  
Sic Composites

AbstractIn this paper, the temperature-dependent matrix multicracking evolution of carbon-fiber-reinforced silicon carbide ceramic-matrix composites (C/SiC CMCs) is investigated. The temperature-dependent composite microstress field is obtained by combining the shear-lag model and temperature-dependent material properties and damage models. The critical matrix strain energy criterion assumes that the strain energy in the matrix has a critical value. With increasing applied stress, when the matrix strain energy is higher than the critical value, more matrix cracks and interface debonding occur to dissipate the additional energy. Based on the composite damage state, the temperature-dependent matrix strain energy and its critical value are obtained. The relationships among applied stress, matrix cracking state, interface damage state, and environmental temperature are established. The effects of interfacial properties, material properties, and environmental temperature on temperature-dependent matrix multiple fracture evolution of C/SiC composites are analyzed. The experimental evolution of matrix multiple fracture and fraction of the interface debonding of C/SiC composites at elevated temperatures are predicted. When the interface shear stress increases, the debonding resistance at the interface increases, leading to the decrease of the debonding fraction at the interface, and the stress transfer capacity between the fiber and the matrix increases, leading to the higher first matrix cracking stress, saturation matrix cracking stress, and saturation matrix cracking density.

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