scholarly journals Effect of Ausforming on the Macro- and Micro-texture of Bainitic Microstructures

Author(s):  
Adriana Eres-Castellanos ◽  
Lucia Morales-Rivas ◽  
Jose Antonio Jimenez ◽  
Francisca G. Caballero ◽  
Carlos Garcia-Mateo

Abstract The reason why variant selection phenomena occur in ausforming treatments is still not known. For that reason, in this work, the effect of compressive deformation on the macro and micro-texture of a bainitic microstructure was analyzed in a medium-carbon high-silicon steel subjected to ausforming treatments, where deformation was applied at 520 °C, 400 °C and 300 °C. The as-received material presented a very weak $$\left\langle {3\, 3\, 1} \right\rangle$$ 3 3 1 fiber texture along the rod axis, due to prior thermomechanical processing. For the samples isothermally heat-treated, it was detected that the bainitic ferrite inherited a $$\left\langle {1\, 0\, 0} \right\rangle$$ 1 0 0 fiber texture from the $$\left\langle {1\, 1\, 0} \right\rangle$$ 1 1 0 fiber texture present in the prior austenite. The intensity of this transformation texture was more pronounced as the deformation temperature decreased. Also, variant selection was examined at different scales by combining Electron-Backscattered Diffraction and X-ray Diffraction. The quantification of the fraction of crystallographic variants under certain conventions for every condition revealed variant selection in samples subjected to ausforming treatments, where these phenomena were stronger as the deformation temperature was lower. Finally, some of the theories proposed so far to explain these variant selection phenomena were tested, showing that variants were not selected based on their Bain group and that their selection can be better described in terms of their belonging to packets, if these are defined according to a global reference frame. This suggests that the phenomena might have to do with the effect of deformation mechanisms on the prior austenite.

2011 ◽  
Vol 172-174 ◽  
pp. 123-128 ◽  
Author(s):  
Peter D. Hodgson ◽  
Ilana Timokhina ◽  
Xiang Yuan Xiong ◽  
Yoshitaka Adachi ◽  
Hossein Beladi

A 0.79C-1.5Si-1.98Mn-0.98Cr-0.24Mo-1.06Al-1.58Co (wt%) steel was isothermally heat treated at 200°C for 10 days to form a nano-scale bainitic microstructure consisting of nanobainitic ferrite laths with high dislocation density and retained austenite films. The crystallographic analysis using TEM and EBSD revealed that the bainitic ferrite laths are close to the Nishiyama-Wassermann orientation relationship with the parent austenite. There was only one type of packet identified in a given transformed austenite grain. Each packet consisted of two different blocks having variants with the same habit plane, but different crystallographic orientations. The presence of fine C-rich clusters and Fe-C carbides with a wide range of compositions in bainitic ferrite was revealed by Three-dimensional Atom Probe Tomography (APT). The high carbon content of bainitic ferrite compared to the para-equilibrium level of carbon in ferrite, absence of segregation of carbon to the austenite/bainitic ferrite interface and absence of partitioning of substitutional elements between the retained austenite and bainitic ferrite were also found using APT.


2019 ◽  
Vol 821 ◽  
pp. 244-249
Author(s):  
Qian Su ◽  
Jie Xu ◽  
Lei Shi ◽  
De Bin Shan ◽  
Bin Guo

Micro-embossing tests were performed on ultrafine-grained pure Al processed by equal-channel angular pressing (ECAP) with 100 μm width of female die at different deformation temperature ranging from 298 K to 523 K under a force of 5 kN. The filling height, surface topography and microstructure of the cross section were measured by confocal scanning laser microscopy (CSLM), scanning electron microscopy (SEM) and electron backscattered diffraction (EBSD), respectively. The effects of deformation temperature on formability of ultrafine-grained (UFG) pure Al during micro-embossing were analyzed. The results show that increase in deformation temperature can improve the formability of UFG pure Al on micro-embossing. Micro hot embossing of UFG pure aluminum is characterized by the rib sidewall, surface quality, and fully transferred patterns, which shows ultrafine-grained pure Al has potential application in micro-forming.


2007 ◽  
Vol 26-28 ◽  
pp. 73-76 ◽  
Author(s):  
J.S. Kang ◽  
S.S. Ahn ◽  
C.Y. Yoo ◽  
Chan Gyung Park

In the present study, focused ion beam (FIB) technique was applied to make site-specific TEM specimens and to identify the 3-dimensional grain morphologies of bainitic microstructure in low carbon HSLA steels such as granular bainite, acicular ferrite and bainitic ferrite. Granular bainite consisted of fine subgrains and 2nd phase constituents like M/A or pearlite located at grain and subgrain boundaries. Acicular ferrite was characterized by an aggregate of ramdomly orientated and irregular shaped grains. The high angle boundaries between adjacent acicular ferrite grains caused by intragranular nucleation during continuous cooling process. Bainitic ferrite revealed uniform and parallel lath structure within the prior austenite grain boundaries and its’ packet size could effectively decreased by the formation of intragranular acicular ferrite.


2010 ◽  
Vol 654-656 ◽  
pp. 2338-2341 ◽  
Author(s):  
A. Sankaran ◽  
Emmanuel Bouzy ◽  
Matthew R. Barnett ◽  
Alain Hazotte

Rapid cooling of TiAl-based alloy from α phase (disordered hexagonal, A3) generates  phase (ordered tetragonal, L1o) grains through massive transformation nucleating mostly over the α/α grain boundaries. This current work deals with the identification and the validation of different nucleation mechanisms during  massive transformation in TiAl-based alloys. Special attention has been given to the variant selection criteria for the nucleation of the massive structures along different types of α/α grain boundaries. The  massive domains formed along the grain boundaries were analysed using high resolution electron backscattered diffraction (EBSD). Statistical studies were made on different nucleation sites and different mechanisms are proposed. Two–dimensional studies of the nucleation mechanism suggest that the minimization of the interfacial energy could be the predominant criteria during the grain boundary nucleation. In order to verify this nucleation criterion in three-dimensions, serial sections were made and EBSD maps were taken and analysed in each section. The variant selection observed during the nucleation and the growth of the  massive grains is further discussed after getting a broader view under three-dimensional investigations.


2019 ◽  
Vol 798 ◽  
pp. 32-37
Author(s):  
Kittichai Sojiphan ◽  
Phongsathon Wangsupangkul ◽  
Tanapat Chailampangsuksakul

Ultrasonic inspection is one of the most widely used non-destructive testing methods for inspection of fabricated structures and components. During ultrasonic inspection, mechanical waves in form of ultrasound are transmitted and propagate through volume of parts or components and reflect when the waves meet with the existing interface such as flaws in the welds. In addition to detection of flaws or defects within the structures, ultrasonic inspection is also used for determination of component thickness as well as characterization of microstructure of different materials. As the ultrasound is transmitted through media, the loss of ultrasound amplitude is referred to as acoustic attenuation. This attenuation effects greatly result from heterogeneity, anisotropy, and different grain sizes of crystalline media the ultrasound goes through. In order to develop the ultrasonic backscattering models for polycrystalline materials, experimental results of the correlation between the changes in attenuation coefficient and the actual microstructure of polycrystalline materials are necessary. This research article presents the preliminary results of this correlation study in stainless steel 304L specimens in as-received conditions compared with different annealed and heat-treated conditions. Such correlations of attenuation coefficient, hardness, and grain size will be used as baseline for future additional characterization technique such as electron backscattered diffraction to better understand the attenuation effects for textured polycrystalline materials.


2018 ◽  
Vol 140 (2) ◽  
Author(s):  
Khaled Al-Fadhalah

Repetitive thermomechanical processing (TMP) has been applied to evaluate the effect of compression strain and temperature on microstructure and texture development in an alpha-brass alloy. Two TMP schemes were employed using four cycles of low-strain compression (ε = 0.15) and annealing, and two cycles of medium-strain compression (ε = 0.3) and annealing. Compression tests were conducted at 25, 250, and −100 °C, while annealing was made at 670 °C for 10 min. Examination by electron backscattered diffraction (EBSD) indicated that the low-strain scheme was capable to increase the fraction of Σ3n boundaries (n = 1, 2, and 3) with increasing cycles, producing maximum fraction of 68%. For medium-strain scheme, a drop in the fraction of Σ3n boundaries occurred in cycle 2. Reducing compression temperature lowered the fraction of Σ3n boundaries for low-strain scheme, while it enhanced the formation of Σ3n boundaries for medium-strain scheme. Annealing textures showed that 〈101〉 compression fiber was strongly retained for samples processed by small-strain scheme, while weakening of 〈101〉 fiber accompanied by the formation of 〈111〉 recrystallization fiber occurred for the medium-strain scheme. The results indicate that the increase in strain energy stored during compression, via increasing strain and/or decreasing deformation temperature, is responsible to favor recrystallization twinning over strain-induced grain boundary migration (SIBM). Both mechanisms are important for the formation of Σ3n boundaries. Yet, SIBM is thought to strongly promote regeneration of Σ3n boundaries at higher TMP cycles. This is consistent with the development of microstructure and texture using small-strain scheme.


2014 ◽  
Vol 783-786 ◽  
pp. 1067-1072 ◽  
Author(s):  
K. Mukherjee ◽  
L.S. Thomas ◽  
C. Bos ◽  
David K. Matlock ◽  
John G. Speer

The potential to utilize controlled thermal processing to minimize banding in a DP780 steel with 2 wt pct Mn was evaluated on samples processed on a Gleeble® 3500 thermomechanical processing simulator. All processing histories were selected to result in final dual-phase steel microstructures simulating microstructures achievable during annealing of initially cold rolled sheet. Strip samples were processed to evaluate the effects of heating rate, annealing time, annealing temperature, and cooling rate. The degree of banding in the final microstructures was evaluated with standard light optical microscopic techniques. Results are presented to illustrate that the extent of banding depended on control of both heating and cooling rates, and a specific processing history based on a two-stage heating rate can be used to minimize visible banding in selected final heat treated products.


2010 ◽  
Vol 297-301 ◽  
pp. 359-364 ◽  
Author(s):  
M. Matsushita ◽  
H. Ohfuji

Recrystallization processing of cold-rolled copper after isothermal annealing was investigated using high-resolution electron backscattered diffraction pattern analysis. The fiber texture is obtained by cold rolling with the rolled direction oriented along {111}, and the transverse and nominal directions have a random orientation. An isothermal recrystallization process at 150°C was investigated. Initially, rotations of the orientations occur from {111} to {100} and then small misfit angle boundaries decreased. Accompanying this change, the fiber-shaped grains change to a round shape grain and their sizes decrease. Considering these tendencies, we determined that rotation at subgrain boundaries is activated by isothermal annealing and subboundaries grow the boundary misfit angle >15 º. With further annealing, those grains surrounded by grain boundaries greater than 15º expanded. The rolling, transverse, and nominal orientations rotate {100}. Subsequently, a twin boundary appeared, and the fraction of twin boundaries increased.


Author(s):  
L. C. D. Fielding ◽  
E. J. Song ◽  
D. K. Han ◽  
H. K. D. H. Bhadeshia ◽  
D.-W. Suh

The diffusion of hydrogen in austenite is slower than in ferrite. Experiments have been conducted to study the behaviour of hydrogen in a nanostructured steel sample consisting of a mixture of thin plates of bainitic ferrite and intervening films of retained austenite, with the latter phase present in a quantity larger than the percolation threshold, i.e. it has three-dimensional connectivity. The structure was then heat treated to control the fraction of austenite, and hence to study the role of hydrogen when the austenite decomposes below the value required to sustain percolation. The experiments have involved both thermal desorption analysis and permeation, and when combined with theoretical analysis, indicate a significant influence of percolating austenite in hindering the passage of hydrogen into the steel during hydrogen charging, and its permeation through the composite nanostructure. The effect is not as large as might be expected from a simple comparison of independent data on the diffusivities of hydrogen in the two lattices, because the effective diffusivity in ferrite is found to be much smaller than in the defect-free ferrite, owing to trapping effects. The morphology of the austenite is demonstrated to play a role by comparing with a sample containing a larger volume fraction of austenite but present as isolated grains which are ineffective to the permeation of hydrogen.


2013 ◽  
Vol 762 ◽  
pp. 14-21 ◽  
Author(s):  
Peter Hodgson ◽  
Subrata Mukherjee ◽  
Hossein Beladi ◽  
Xiang Yuan Xiong ◽  
Ilana B. Timokhina

Two steels, ferritic, high strength with interphase precipitation and nanobainitic, were used to show the advances in and application of atom probe. The coexistence of the nanoscale, interphase Nb-Mo-C clusters and stoichiometric MC nanoparticles was found in the high strength steel after thermomechanical processing. Moreover, the segregation of carbon at different heterogeneous sites such as grain boundary that reduces the solute element available for fine precipitation was observed. The APT study of the solutes redistribution between the retained austenite and bainitic ferrite in the nanobainitic steel revealed: (i) the presence of two types of the retained austenite with higher and lower carbon content and (ii) segregation of carbon at the local defects such as dislocations in the bainitic ferrite during the isothermal hold.


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