Analysis and characterization of starches from alternative sources

2022 ◽  
pp. 465-488
Author(s):  
Maria Carolina Bezerra Di-Medeiros Leal ◽  
Gislane Oliveira Ribeiro ◽  
Maria Luiza Rezende Ribeiro ◽  
Antônio Gilberto Ferreira ◽  
Anna Rafaela Cavalcante Braga ◽  
...  
Keyword(s):  
2018 ◽  
Vol 67 ◽  
pp. 04024
Author(s):  
Dewi Tristantini ◽  
Andersen Yunan

Scrubs used in other skin care and beauty products usually contain tiny fine grains of synthetic polymer called microbeads that usually pose threats to marine environment. Empty Fruit Bunches (EFB) and Dried Jackfruit Leaves (DJL) as organic and environmentally friendly can be alternative sources for polymer microbeads. Cellulose acetate is prepared by acetylation reaction between cellulose and acetic acid anhydride. Cellulose from EFB and DJL was extracted through a process of delignification with 12% NaOH treatment for EFB and 10% for DJL to obtain maximum yields of 38.964% and 14.449% respectively, followed by bleaching using peroxide 10 %. The formed cellulose acetate with 88.5% and 79.7% yield respectively is then filtered using a sieve mash 60 and 80 to obtain particle sizes ranging that are in the microbeads size range. The density test resulting in 0.73 g/cm3 and 0.52 g/cm3 respectively for EFB and DJL. Then, physical characteristic test was done by water and oil absorption test with variation at 25°C and 40°C. EFB at 25°C and 40°C shows water absorption at 23.39% and 26.09% and oil absorption at 7.59% and 13.95%. DJL at 25°C and 40°C shows water absorption at 22.56% and 27.32% and oil absorption at 13.09% and 15.36%.


2010 ◽  
Vol 5 (2) ◽  
pp. 1934578X1000500 ◽  
Author(s):  
Alessandra Bertoli ◽  
Szilvia Sárosi ◽  
Jenő Bernáth ◽  
Luisa Pistelli

The aromatic profiles of five commercial thyme cultivars (T. vulgaris ‘Silver Poise’, T. vulgaris ‘Erectus’, T. vulgaris ‘Faustini’, T. × citriodorus ‘Anderson's Gold’, and T. × citriodorus ‘Silver Queen’), cultivated in Italy, were defined both by their static headspaces (HS) and essential oils (EOs). In addition, a botanical garden sample of T. vulgaris was considered as reference material to evaluate the morphological and phytochemical differences from the selected market samples. Extractions of the volatile constituents of the different plant material were carried out by SPME (static headspace, HS) and hydrodistillation (HD) processes. GC-MS analysis provided the separation and identification of approximately 70 components in the HS samples and 50 in the hydrodistilled essential oils, accounting for more than 95% of the total. The typical main constituents of T. vulgaris were detected in all the EO samples, although qualitative and quantitative differences were found among the selected ornamental Thymus varieties. Thymol (50-55%) was the marker constituent for the three T. vulgaris cultivars, while geraniol (61-67%) characterized the essential oils of the two T. × citriodorus varieties. In all the analyzed essential oils, non-oxygenated (16-79%) and oxygenated (5-26%) monoterpenes were the typical volatile constituents. Specific target compounds (thymol, geraniol and 6-methyl-5-hepten-2-one) were selected to characterize the five thyme cultivars that are considered at present only as ornamental plants. A comparative evaluation of their EO quality was carried out in order to propose them as alternative sources of Italian raw plant material for industrial production.


1998 ◽  
Vol 27 (2) ◽  
pp. 81-84 ◽  
Author(s):  
B. K. Han ◽  
L. Li ◽  
M. J. Kappers ◽  
R. F. Hicks ◽  
H. Yoon ◽  
...  

Planta Medica ◽  
2019 ◽  
Vol 85 (11/12) ◽  
pp. 856-868 ◽  
Author(s):  
Luis Francisco Salomé Abarca ◽  
Peter G. L. Klinkhamer ◽  
Young Hae Choi

AbstractHistorically, latex-bearing plants have been regarded as important medicinal resources in many countries due to their characteristic latex ingredients. They have also often been endowed with a social or cultural significance in religious or cult rituals or for hunting. Initial chemical studies focused on the protein or peptide content but recently the interest extended to smaller molecules. Latex has been found to contain a broad range of specialized metabolites such as terpenoids, cardenolides, alkaloids, and phenolics, which are partly responsible for their antibacterial, antifungal, anthelmintic, cytotoxic, and insect-repellent activities. The diversity in biology and chemistry of latexes is supposedly associated to their ecological roles in interactions with exogenous factors. Latexes contain unique compounds that are different to those found in their bearing plants. Exploring the feasibility of plant latex as a new type of bioactive chemical resource, this review paper covers the chemical characterization of plant latexes, extending this to various other plant exudates. Also, the factors influencing this chemical differentiation and the production, transportation, and chemistry of the latex exudates are described, based on ecological and biochemical mechanisms. We also proposed a latex coagulation model involving 4 general conserved steps. Therefore, the inherent defensive origin of latexes is recognized as their most valuable character and encourages one to pay attention to these materials as alternative sources to discover metabolites with insecticidal or antimicrobial activity.


2016 ◽  
Vol 38 ◽  
pp. 96-100
Author(s):  
Miguel Sanchez ◽  
Mauro Cesar Terence ◽  
Juan Alfredo Guevara Carrió

Two-dimensional films of graphene oxide (GO) have been synthesized using various oxidation methods such as the conventional or modified Hummers method. The redox method for graphite has shown promise at producing GO films on a large scale. However, this method is a very exothermic process that liberates gases that are harmful to the environment and humans. This article addresses the characterization of graphene oxide from alternative sources of carbon and using the dry method. Comparative studies performed using Raman spectroscopy suggest that this method is both promising and more environmentally friendly.


Molecules ◽  
2021 ◽  
Vol 26 (14) ◽  
pp. 4191
Author(s):  
Evernice Chikukwa ◽  
Edson Meyer ◽  
Johannes Mbese ◽  
Nyengerai Zingwe

The drawbacks of utilizing nonrenewable energy have quickened innovative work on practical sustainable power sources (photovoltaics) because of their provision of a better-preserved decent environment which is free from natural contamination and commotion. Herein, the synthesis, characterization, and application of Mo chalcogenide nanoparticles (NP) as alternative sources in the absorber layer of QDSSCs is discussed. The successful synthesis of the NP was confirmed as the results from the diffractive peaks obtained from XRD which were positive and agreed in comparison with the standard. The diffractive peaks were shown in the planes (100), (002), (100), and (105) for the MoS2 nanoparticles; (002), (100), (103), and (110) for the MoSe2 nanoparticles; and (0002), (0004), (103), as well as (0006) for the MoTe2 nanoparticles. MoSe2 presented the smallest size of the nanoparticles, followed by MoTe2 and, lastly, by MoS2. These results agreed with the results obtained using SEM analysis. For the optical properties of the nanoparticles, UV–Vis and PL were used. The shift of the peaks from the red shift (600 nm) to the blue shift (270–5 nm and 287–9 nm (UV–Vis)) confirmed that the nanoparticles were quantum-confined. The application of the MoX2 NPs in QDSSCs was performed, with MoSe2 presenting the greatest PCE of 7.86%, followed by MoTe2 (6.93%) and, lastly, by MoS2, with the PCE of 6.05%.


2021 ◽  
Vol 69 (2) ◽  
pp. 30-33
Author(s):  
Murugesan Sumithra ◽  
Gayathri Murugan

Natural fibres are one of the good alternative sources for replacing synthetic fibres and reinforcing polymer matrices because of their eco-friendly nature. The present study was undertaken to investigate the fibres extract from Elettaria Cardamomum plant. The extracted Elettaria Cardamomum fibre was treated with NaOH for softening. Natural cellulose fibres extracted from Elettaria Cardamomum stems (ECS) have been characterized for their chemical composition and physical properties.The chemical composition of Elettaria Cardamomumstems (ECS) fi bres is, cellulose 60.44%, lignin 25.25%, wax 0.53%, ash 5.45%. Regarding physical properties of the fibres, single fibre strength was evaluated and the result was compared with cotton fibre and linen fibre.


Author(s):  
Brian K H Mo ◽  
Akinori Ando ◽  
Ryohei Nakatsuji ◽  
Tomoyo Okuda ◽  
Yuki Takemoto ◽  
...  

Abstract ω3 polyunsaturated fatty acids are currently obtained mainly from fisheries, thus sustainable alternative sources such as oleaginous microorganisms are required. Here we describe the isolation, characterization, and application of three novel ω3 desaturases with ω3 polyunsaturated fatty acid-producing activity at ordinary temperatures (28 °C). First, we selected Pythium sulcatum and Plectospira myriandra after screening for oomycetes with high eicosapentaenoic acid/arachidonic acid ratios and isolated the genes psulω3 and pmd17, respectively, which encode ω3 desaturases. Subsequent characterization showed that PSULω3 exhibited ω3 desaturase activity on both C18 and C20 ω6 polyunsaturated fatty acids while PMD17 exhibited ω3 desaturase activity exclusively on C20 ω6 polyunsaturated fatty acids. Expression of psulω3 and pmd17 in the arachidonic acid-producer Mortierella alpina resulted in transformants that produced eicosapentaenoic acid/total fatty acid values of 38% and 40%, respectively, at ordinary temperatures. These ω3 desaturases should facilitate the construction of sustainable ω3 polyunsaturated fatty acid sources.


Foods ◽  
2021 ◽  
Vol 10 (8) ◽  
pp. 1949
Author(s):  
Ana Alvarez Arraibi ◽  
Ângela Liberal ◽  
Maria Inês Dias ◽  
Maria José Alves ◽  
Isabel C. F. R. Ferreira ◽  
...  

Currently, there is a general trend towards reutilizing industrial by-products that would otherwise be discarded or considered as waste, aiming to explore them as alternative sources of valuable compounds. The apple pomace remaining from cider and apple juice industries represents a high-potential source of bioactive compounds with putative application in food or pharmaceutical-related products. Accordingly, the work reported herein was conducted to characterize the phenolic compounds in apple pomace from Belgium and Spain, as well as to evaluate its chemical composition and particular types of bioactivity. As a proof of concept, a new hydrogel was prepared, incorporated with the bioactive compounds and pectin extracted from apple pomace, aiming to obtain the most organic formulation possible. Independently of the extracting agent, it became evident that using lyophilization as the drying step is a better choice than thermal processes as it yielded a richer phenolic profile (fifteen individual compounds), with 5-O-caffeoylquinic acid as the major compound (66 to 114 mg/100 g dw) in Belgian samples. In general, the hydroethanolic extracts showed the strongest antioxidant and antimicrobial (particularly against Propionibacterium acnes: MIC = 2.5 mg/mL) activities. This result, together with the lipid nature of human skin, led it to be chosen as the extract type to be incorporated in the hydrogel. In general, apple pomace stood out as a valuable source of bioactive compounds, especially polyphenols and pectin, with good potential to be incorporated in dermal formulations.


Author(s):  
Himadri RAJPUT ◽  
Anoop VERMA ◽  
Manpreet KAUR ◽  
Taranjeet KAUR ◽  
Amrit Pal TOOR

This work evaluates the scope of alternative sources of iron i.e. Foundry Sand (FS), Fly Ash (FA) and mixture of FS and FA in heterogeneous photo-Fenton process for the degradation and decolourization of the dye Reactive Black5 (RB5). SEM-EDS characterization of FS and FA confirmed the presence of iron and aluminium which are required for photo-Fenton. In case of FS as an iron source, results confirmed the degradation and decolourization efficiency of 90% in 70 min and 45 min respectively when the reaction parameters were H2O2 = 2.2 mm, FS dose = 0.5 g, ph 3. With FA 90% degradation was achieved within 30 min and 93% decolourization rate within 15 min. When a mixture of FS (0.1 gm) and FA (0.05 gm) is used as source of iron 99% degradation and decolourization of the dye was achieved under the reaction conditions where H2O2 = 2.2 mm, FA:FS = 1:2, ph 3.


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