Effect of thermomechanical treatment and length-scales on spatial distribution of CNTs in Al matrix

Carbon ◽  
2022 ◽  
Author(s):  
Qibing Liu ◽  
Genlian Fan ◽  
Zhanqiu Tan ◽  
Farhad Saba ◽  
Qiang Guo ◽  
...  
2015 ◽  
Vol 89 ◽  
pp. 327-343 ◽  
Author(s):  
Lin Jiang ◽  
Haiming Wen ◽  
Hanry Yang ◽  
Tao Hu ◽  
Troy Topping ◽  
...  

2009 ◽  
Vol 80 (2) ◽  
Author(s):  
Puspen Mondal ◽  
Meghmalhar Manekar ◽  
A. K. Srivastava ◽  
S. B. Roy

2020 ◽  
Vol 15 (02) ◽  
pp. 83-98
Author(s):  
Juliana C. Wortman ◽  
Ting-Fang He ◽  
Anthony Rosario ◽  
Roger Wang ◽  
Daniel Schmolze ◽  
...  

Favorable outcomes have been associated with high densities of tumor infiltrating lymphocytes (TILs) such as cytotoxic ([Formula: see text]) T cells. However, the clinical significance of the spatial distribution of TILs is less well understood. We have developed novel statistical techniques to characterize the spatial distribution of TILs at various length scales. These include a box counting method that we call “occupancy” and novel applications of fractal dimensions. We apply these techniques to the spatial distribution of [Formula: see text] T cells in the tumor microenvironment of tissue resected from 35 triple negative breast cancer patients. We find that there is a distinct difference in the spatial distribution of [Formula: see text] T cells between good clinical outcome (no recurrence within at least 5 years of diagnosis) and poor clinical outcome (recurrence within 3 years of diagnosis). The statistical significance of the difference between good and poor outcome in the occupancy, fractal dimension (FD), and FD difference of [Formula: see text] T cells is comparable to that of the [Formula: see text] T cell density. Even when we randomly exclude some of the cells so that the images have the same cell density, we still find that the fractal dimension at short length scales is correlated with cancer recurrence, implying that the actual spatial distribution of [Formula: see text] cells, and not just the [Formula: see text] cell density, is associated with clinical outcome. The occupancy and FD difference indicate that the [Formula: see text] T cells are more spatially dispersed in good outcome and more aggregated in poor outcome. We discuss possible interpretations.


2013 ◽  
Vol 753 ◽  
pp. 37-41 ◽  
Author(s):  
Dorte Juul Jensen ◽  
Feng Xiang Lin ◽  
Yu Bin Zhang ◽  
Yong Hao Zhang

Effects of local variations in the deformation microstructure on subsequent recrystallization are discussed and illustrated by three examples. The three examples consider local variations on different length scales and are: 1. Effects of local variations in the deformation microstructure on the formation of protrusions on migrating boundaries. 2. Effects of an inhomogeneous spatial distribution of second phase particles on growth. 3. Effects of stored energy and orientation variations on recrystallization kinetics.


2009 ◽  
Vol 131 (10) ◽  
Author(s):  
M. Reza Rasaei ◽  
Muhammad Sahimi

To model fluid flow and energy transport in a large-scale porous medium, such as an oil or a geothermal reservoir, one must first develop the porous medium’s geological model (GM) that contains all the relevant data at all the important length scales. Such a model, represented by a computational grid, usually contains several million grid blocks. As a result, simulation of fluid flow and energy transport with the GM, particularly over large time scales (for example, a few years), is impractical. Thus, an important problem is upscaling of the GM. That is, starting from the GM, one attempts to generate an upscaled or coarsened computational grid with only a few thousands grid blocks, which describes fluid flow and transport in the medium as accurately as the GM. We describe a powerful upscaling method, which is based on the wavelet transformation of the spatial distribution of any static property of the porous medium, such as its permeability, or a dynamic property, such as the spatial distribution of the local fluid velocities in the medium. The method is a multiscale approach that takes into account the effect of the heterogeneities at all the length scales that can be incorporated in the GM. It generates a nonuniform computational grid with a low level of upscaling in the high permeability sectors but utilizes high levels of upscaling in the rest of the GM. After generating the upscaled computational grid, a critical step is to calculate the equivalent permeability of the upscaled blocks. In this paper, six permeability upscaling techniques are examined. The techniques are either analytical or numerical methods. The results of computer simulations of displacement of oil by water, obtained with each of the six methods, are then compared with those obtained by the GM.


Author(s):  
L. D. Jackel

Most production electron beam lithography systems can pattern minimum features a few tenths of a micron across. Linewidth in these systems is usually limited by the quality of the exposing beam and by electron scattering in the resist and substrate. By using a smaller spot along with exposure techniques that minimize scattering and its effects, laboratory e-beam lithography systems can now make features hundredths of a micron wide on standard substrate material. This talk will outline sane of these high- resolution e-beam lithography techniques.We first consider parameters of the exposure process that limit resolution in organic resists. For concreteness suppose that we have a “positive” resist in which exposing electrons break bonds in the resist molecules thus increasing the exposed resist's solubility in a developer. Ihe attainable resolution is obviously limited by the overall width of the exposing beam, but the spatial distribution of the beam intensity, the beam “profile” , also contributes to the resolution. Depending on the local electron dose, more or less resist bonds are broken resulting in slower or faster dissolution in the developer.


Author(s):  
Jayesh Bellare

Seeing is believing, but only after the sample preparation technique has received a systematic study and a full record is made of the treatment the sample gets.For microstructured liquids and suspensions, fast-freeze thermal fixation and cold-stage microscopy is perhaps the least artifact-laden technique. In the double-film specimen preparation technique, a layer of liquid sample is trapped between 100- and 400-mesh polymer (polyimide, PI) coated grids. Blotting against filter paper drains excess liquid and provides a thin specimen, which is fast-frozen by plunging into liquid nitrogen. This frozen sandwich (Fig. 1) is mounted in a cooling holder and viewed in TEM.Though extremely promising for visualization of liquid microstructures, this double-film technique suffers from a) ireproducibility and nonuniformity of sample thickness, b) low yield of imageable grid squares and c) nonuniform spatial distribution of particulates, which results in fewer being imaged.


Author(s):  
M.T. Jahn ◽  
J.C. Yang ◽  
C.M. Wan

4340 Ni-Cr-Mo alloy steel is widely used due to its good combination of strength and toughness. The mechanical property of 4340 steel can be improved by various thermal treatments. The influence of thermomechanical treatment (TMT) has been studied in a low carbon Ni-Cr-Mo steel having chemical composition closed to 4340 steel. TMT of 4340 steel is rarely examined up to now. In this study we obtain good improvement on the mechanical property of 4340 steel by TMT. The mechanism is explained in terms of TEM microstructures4340 (0.39C-1.81Ni-0.93Cr-0.26Mo) steel was austenitized at 950°C for 30 minutes. The TMTed specimen (T) was obtained by forging the specimen continuously as the temperature of the specimen was decreasing from 950°C to 600°C followed by oil quenching to room temperature. The thickness reduction ratio by forging is 40%. The conventional specimen (C) was obtained by quenching the specimen directly into room temperature oil after austenitized at 950°C for 30 minutes. All quenched specimens (T and C) were then tempered at 450, 500, 550, 600 or 650°C for four hours respectively.


Author(s):  
Auclair Gilles ◽  
Benoit Danièle

During these last 10 years, high performance correction procedures have been developed for classical EPMA, and it is nowadays possible to obtain accurate quantitative analysis even for soft X-ray radiations. It is also possible to perform EPMA by adapting this accurate quantitative procedures to unusual applications such as the measurement of the segregation on wide areas in as-cast and sheet steel products.The main objection for analysis of segregation in steel by means of a line-scan mode is that it requires a very heavy sampling plan to make sure that the most significant points are analyzed. Moreover only local chemical information is obtained whereas mechanical properties are also dependant on the volume fraction and the spatial distribution of highly segregated zones. For these reasons we have chosen to systematically acquire X-ray calibrated mappings which give pictures similar to optical micrographs. Although mapping requires lengthy acquisition time there is a corresponding increase in the information given by image anlysis.


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