Multiple techniques of microstructural characterization of DEF: Case of study with high early strength Portland cement composites

2021 ◽  
Vol 311 ◽  
pp. 125341
Author(s):  
Kleber Franke Portella ◽  
Nicole Pagan Hasparyk ◽  
Mariana D'Orey Gaivão Portella Bragança ◽  
Jeferson Luís Bronholo ◽  
Bruna Gomes Dias ◽  
...  
2017 ◽  
Vol 866 ◽  
pp. 187-190
Author(s):  
Thossapon Jaihlong ◽  
Nittaya Jaitanong ◽  
Suparut Narksitipan

In present research, the cement-rice husk ash composites were prepared and characterized. The samples were added fiber optic and rice husk ash was used as replacement cementitious materials at 10, 20, 30 and 40 wt% of portland cement. The samples were demolded after 24 h casting and cured in saturated lime water for 3 days. After these periods, the samples were wrapped with plastics films for 7 and 28 days. Then, samples were dried in air for 24 h. The chemical compositin of portland cement and rice husk ash were characterized by using x-ray fluorence spectrometry (XRF). Additionally, dried samples were analysized phase compositions and crystalline structure by using x-ray diffraction (XRD) technique. The chemical element compositions and microstructure were detected by scanning electron microscopy (SEM), respectively. Moreover, The effect of rice husk ash in these cement composites were investigated in this research.


Author(s):  
Fernando Benedicto Mainier ◽  
Viktor Labuto Fragoso Sereno Ramos ◽  
Claudio Fernando Mahler

This study presents the results of the mechanical characterization of cement composites reinforced with short fibers of jute, sisal and curauá. Tests of direct tension in flexion and traction, after wetting and drying cycle (5 cycles) to determine the first crack were performed to determine the first crack, the tension and post-peak toughness and strengh of the composites. To ensure the the composite durability, the ordinary Portland cement matrix was modified by adding metakaolin, to consume the calcium hydroxide generated during Portland cement hydration. The composites were produced using short fibers of jute, sisal and curauá (50 mm) at levels of 2%, 4% and 6% of sisal and white curauá, and 3%, 6% and 9% to jute. The fibers of jute and white curauá employed in this study came from the Brazilian Amazon, while the sisal came from the Brazilian Northeast.This fibers have great economic importance in the producing region. Composites with high toughness, strength and multiple cracking processes under bending load were obtained when volume fractions equal to 3% of jute were used as reinforcement and when 6% of sisal and 4% of white curauá were used as reinforcement.


2013 ◽  
Vol 19 (5) ◽  
pp. 1222-1230 ◽  
Author(s):  
Mafalda Guedes ◽  
Luís Evangelista ◽  
Jorge de Brito ◽  
Alberto C. Ferro

AbstractSeveral authors have reported the workability, mechanical properties, and durability of concrete produced with construction waste replacing the natural aggregate. However, a systematic microstructural characterization of recycled aggregate concrete has not been reported. This work studies the use of fine recycled aggregate to replace fine natural aggregate in the production of concrete and reports the resulting microstructures. The used raw materials were natural aggregate, recycled aggregate obtained from a standard concrete, and Portland cement. The substitution extent was 0, 10, 50, and 100 vol%; hydration was stopped at 9, 24, and 96 h and 28 days. Microscopy was focused on the cement/aggregate interfacial transition zone, enlightening the effect of incorporating recycled aggregate on the formation and morphology of the different concrete hydration products. The results show that concretes with recycled aggregates exhibit typical microstructural features of the transition zone in normal strength concrete. Although overall porosity increases with increasing replacement, the interfacial bond is apparently stronger when recycled aggregates are used. An addition of 10 vol% results in a decrease in porosity at the interface with a corresponding increase of the material hardness. This provides an opportunity for development of increased strength Portland cement concretes using controlled amounts of concrete waste.


Author(s):  
M.A. Parker ◽  
K.E. Johnson ◽  
C. Hwang ◽  
A. Bermea

We have reported the dependence of the magnetic and recording properties of CoPtCr recording media on the thickness of the Cr underlayer. It was inferred from XRD data that grain-to-grain epitaxy of the Cr with the CoPtCr was responsible for the interaction observed between these layers. However, no cross-sectional TEM (XTEM) work was performed to confirm this inference. In this paper, we report the application of new techniques for preparing XTEM specimens from actual magnetic recording disks, and for layer-by-layer micro-diffraction with an electron probe elongated parallel to the surface of the deposited structure which elucidate the effect of the crystallographic structure of the Cr on that of the CoPtCr.XTEM specimens were prepared from magnetic recording disks by modifying a technique used to prepare semiconductor specimens. After 3mm disks were prepared per the standard XTEM procedure, these disks were then lapped using a tripod polishing device. A grid with a single 1mmx2mm hole was then glued with M-bond 610 to the polished side of the disk.


Author(s):  
A.K. Rai ◽  
A.K. Petford-Long ◽  
A. Ezis ◽  
D.W. Langer

Considerable amount of work has been done in studying the relationship between the contact resistance and the microstructure of the Au-Ge-Ni based ohmic contacts to n-GaAs. It has been found that the lower contact resistivity is due to the presence of Ge rich and Au free regions (good contact area) in contact with GaAs. Thus in order to obtain an ohmic contact with lower contact resistance one should obtain a uniformly alloyed region of good contact areas almost everywhere. This can possibly be accomplished by utilizing various alloying schemes. In this work microstructural characterization, employing TEM techniques, of the sequentially deposited Au-Ge-Ni based ohmic contact to the MODFET device is presented.The substrate used in the present work consists of 1 μm thick buffer layer of GaAs grown on a semi-insulating GaAs substrate followed by a 25 Å spacer layer of undoped AlGaAs.


Author(s):  
G. M. Micha ◽  
L. Zhang

RENi5 (RE: rare earth) based alloys have been extensively evaluated for use as an electrode material for nickel-metal hydride batteries. A variety of alloys have been developed from the prototype intermetallic compound LaNi5. The use of mischmetal as a source of rare earth combined with transition metal and Al substitutions for Ni has caused the evolution of the alloy from a binary compound to one containing eight or more elements. This study evaluated the microstructural features of a complex commercial RENi5 based alloy using scanning and transmission electron microscopy.The alloy was evaluated in the as-cast condition. Its chemistry in at. pct. determined by bulk techniques was 12.1 La, 3.2 Ce, 1.5 Pr, 4.9 Nd, 50.2 Ni, 10.4 Co, 5.3 Mn and 2.0 Al. The as-cast material was of low strength, very brittle and contained a multitude of internal cracks. TEM foils could only be prepared by first embedding pieces of the alloy in epoxy.


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