Influence of morphology and chemical surface composition on electrical conductivity of SiC microspheres

2022 ◽  
Vol 715 ◽  
pp. 121942
Author(s):  
Ilona Pleșa ◽  
Simone Radl ◽  
Uwe Schichler ◽  
Franz Ramsauer ◽  
Werner Ladstätter ◽  
...  
Materials ◽  
2020 ◽  
Vol 13 (12) ◽  
pp. 2706
Author(s):  
Katarzyna Siwińska-Ciesielczyk ◽  
Beata Kurc ◽  
Dominika Rymarowicz ◽  
Adam Kubiak ◽  
Adam Piasecki ◽  
...  

Hydrothermal crystallization was used to synthesize an advanced hybrid system containing titania and molybdenum disulfide (with a TiO2:MoS2 molar ratio of 1:1). The way in which the conditions of hydrothermal treatment (180 and 200 °C) and thermal treatment (500 °C) affect the physicochemical properties of the products was determined. A physicochemical analysis of the fabricated materials included the determination of the microstructure and morphology (scanning and transmission electron microscopy—SEM and TEM), crystalline structure (X-ray diffraction method—XRD), chemical surface composition (energy dispersive X-ray spectroscopy—EDS) and parameters of the porous structure (low-temperature N2 sorption), as well as the chemical surface concentration (X-ray photoelectron spectroscop—XPS). It is well known that lithium-ion batteries (LIBs) represent a renewable energy source and a type of energy storage device. The increased demand for energy means that new materials with higher energy and power densities continue to be the subject of investigation. The objective of this research was to obtain a new electrode (anode) component characterized by high work efficiency and good electrochemical properties. The synthesized TiO2-MoS2 material exhibited much better electrochemical stability than pure MoS2 (commercial), but with a specific capacity ca. 630 mAh/g at a current density of 100 mA/g.


2016 ◽  
Vol 27 (6) ◽  
pp. 2324-2334 ◽  
Author(s):  
Martin Foerster ◽  
Thomas Gengenbach ◽  
Meng Wai Woo ◽  
Cordelia Selomulya

2006 ◽  
Vol 253 (3) ◽  
pp. 1506-1511 ◽  
Author(s):  
Dariusz Szmigiel ◽  
Krzysztof Domański ◽  
Piotr Prokaryn ◽  
Piotr Grabiec ◽  
Janusz W. Sobczak

1989 ◽  
Vol 167 ◽  
Author(s):  
T. Flottmann ◽  
A. Tulke ◽  
E. Esper ◽  
W. Lohmann

AbstractDecomposition of a palladium compound by ion irradiation has been used to catalyze electroless plating on polyimide. First, palladium-acetylacetonate or -acetate is spin-coated on a polyimide substrate. The thin resist film is then irradiated through a mask with He or Ar ions of 100 keV energy. After washing off the film parts which were not exposed to the ion beam, copper is deposited on the catalyzed polyimide substrate in an alkaline electroless plating bath. When using alkaline resistant polyimide, copper lines several microns thick can be plated. The chemical surface composition of the Pd-compounds after ion beam exposure has been investigated with ESCA. It has been found that the Pd is partially reduced. Pd-acetate is more effective to form catalytic sites than Pd-acetylacetonate.


2020 ◽  
Vol 22 (22) ◽  
pp. 12591-12604
Author(s):  
Carolina Ardila-Suárez ◽  
Daniel R. Molina V. ◽  
Halima Alem ◽  
Víctor G. Baldovino-Medrano ◽  
Gustavo E. Ramírez-Caballero

Ordered micro/macroporous MOF-808 materials with tunable porosity and similar chemical surface composition were synthesized through the modulator-induced defect-formation and surfactant self-assembly strategies.


Polymers ◽  
2020 ◽  
Vol 12 (6) ◽  
pp. 1423
Author(s):  
Chihaoui Belgacem ◽  
Quim Tarres ◽  
Francesc Xavier Espinach ◽  
Pere Mutjé ◽  
Sami Boufi ◽  
...  

In this work, date palm waste (DPW) stemming from the annual pruning of date palm was used as reinforcing filler in polypropylene (PP) matrix at 40% w/w. Three pre-treatment routes were performed for the DPW, namely (i) defibration, (ii) soft alkali treatment, and (iii) enzymatic treatment, to obtain date palm fibers (DPF) and to investigate the effect of each process on their chemical composition, which will ultimately affect the mechanical properties of the resulting composites. The enzymatic and alkali treatment, combined with maleated polypropylene (MAPP) as a coupling agent, resulted in a composite with higher strength and stiffness than the neat PP. The differences in the reinforcing effect were explained by the change in the morphology of DPF and their chemical surface composition according to the selected treatment of DPW. Enzymatic treatment maximized the tensile strength of the compound as a consequence of an improvement in the interfacial shear strength and the intrinsic resistance of the fibers.


1998 ◽  
Vol 53 (8) ◽  
pp. 679-683 ◽  
Author(s):  
Y. Waseda ◽  
S. Suzuki ◽  
K. Urbanb

Abstract This paper deals with the morphology and surface chemistry of faceted voids existing in singlequasicrystalline icosahedral Al70.5Pd21.0Mn8.5. By observation with a scanning electron microscope of surfaces obtained by cleavage of the quasicrystal, the habit planes of the dodecahedral voids were identified. The chemical surface composition of the void surface was determined by Auger electron spectroscopy after cleavage in ultra-high vacuum.


Coatings ◽  
2020 ◽  
Vol 10 (3) ◽  
pp. 234 ◽  
Author(s):  
Peter Rodič ◽  
Barbara Kapun ◽  
Matjaž Panjan ◽  
Ingrid Milošev

A combination of the chemical etching process in FeCl3 solution and chemical surface grafting by immersion in ethanol solution containing 1H,1H,2H,2H-perfluorodecyltriethoxysilane is a viable route to achieve a hierarchical surface topography and chemical bonding of silane molecules on an aluminium surface leading to (super)hydrophobic characteristics. Characterisation of untreated and treated aluminium surfaces was carried out using contact profilometry, optical tensiometry, scanning electron microscopy coupled with energy-dispersive spectroscopy and X-ray photoelectron spectroscopy to define the surface topography, wettability, morphology and surface composition. Additionally, the dynamic characteristics were evaluated to define bouncing and the self-cleaning effect. A thermal infrared camera was employed to evaluate anti-icing properties. The micro/nano-structured etched aluminium surface grafted with perfluoroalkyl silane film showed excellent superhydrophobicity and bounce dynamics in water droplet tests. The superhydrophobic aluminium surface exhibited the efficient self-cleaning ability of solid pollutants as well as improved anti-icing performance with melting delay.


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