Mechanical properties of W and W(C) thin films: Young’s modulus, fracture toughness and adhesion

1998 ◽  
Vol 332 (1-2) ◽  
pp. 195-201 ◽  
Author(s):  
Emmanuelle Harry ◽  
André Rouzaud ◽  
Michel Ignat ◽  
Pierre Juliet
Keyword(s):  
Thin Films ◽  
Mechanical Properties ◽  
Fracture Toughness ◽  
Young’S Modulus ◽  
Young's Modulus

scholarly journals Effects of CNT Addition on Mechanical Properties, Electric Conductivity and Oxidation Resistance of Al2O3-TiC Composite

2013 ◽  
Vol 761 ◽  
pp. 83-86
Author(s):  
Hideaki Sano ◽  
Junichi Morisaki ◽  
Guo Bin Zheng ◽  
Yasuo Uchiyama
Keyword(s):  
Mechanical Properties ◽  
Carbon Nanotubes ◽  
Fracture Toughness ◽  
Flexural Strength ◽  
Electric Conductivity ◽  
Young’S Modulus ◽  
Oxidation Resistance ◽  
Young's Modulus ◽  
Tic Particle

Effects of carbon nanotubes (CNT) addition on mechanical properties, electric conductivity and oxidation resistance of CNT/Al2O3-TiC composite were investigated. It was found that flexural strength, Young’s modulus and fracture toughness of the composites were improved by addition of more than 2 vol%-CNT. In the composites with more than 3 vol%-CNT, the oxidation resistance of the composite was degraded. In comparison with Al2O3-26vol%TiC sample as TiC particle-percolated sample, the Al2O3-12vol%TiC-3vol%CNT sample, which is not TiC particle-percolated sample, shows almost the same mechanical properties and electric conductivity, and also shows thinner oxidized region after oxidation at 1200°C due to less TiC in the composite.

Mechanical Properties of Transparent Polycrystalline Silicon Nitride

2006 ◽  
Vol 317-318 ◽  
pp. 305-308 ◽  
Author(s):  
Rak Joo Sung ◽  
Takafumi Kusunose ◽  
Tadachika Nakayama ◽  
Yoon Ho Kim ◽  
Tohru Sekino ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Silicon Nitride ◽  
Young’S Modulus ◽  
Fracture Strength ◽  
Polycrystalline Silicon ◽  
Volume Fraction ◽  
Young's Modulus ◽  
Β Phase ◽  
Α Phase

A novel transparent polycrystalline silicon nitride was fabricated by hot-press sintering with MgO and AlN as additives. The mixed powder with 3 wt.% MgO and 9 wt.% AlN was sintered at 1900oC for 1 hour under 30 MPa pressure in a nitrogen gas atmosphere. Transparent polycrystalline silicon nitride was successfully fabricated. The mechanical properties such as density, hardness, young’s modulus, fracture strength and fracture toughness were evaluated. The effect of α/β phase on the mechanical properties of transparent polycrystalline silicon nitride was investigated. The properties were changed depending on the amount of α/β phase. The hardness and Young's modulus increased with increasing the volume fraction of α-phase fraction as a reflection of the higher hardness of α-phase Si3N4. The fracture toughness and fracture strength decreased with decreasing the volume fraction of β-phase Si3N4.

Densification Behaviour and Mechanical Properties on MgO Doped Zirconia Toughened Alumina (ZTA) Prepared by Two-Stage Sintering

2021 ◽  
Vol 1030 ◽  
pp. 3-10
Author(s):  
Teow Hsien Loong ◽  
Ananthan Soosai ◽  
Suresh Muniandy
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Grain Size ◽  
Total Hip Arthroplasty ◽  
Young’S Modulus ◽  
Vickers Hardness ◽  
Young's Modulus ◽  
Two Stage ◽  
Positive Effect ◽  
Zirconia Toughened Alumina

The effect of doping small amounts of Magnesium Oxide ranging between 0 to 1 vol% on Zirconia Toughened Alumina (ZTA) composites which is one of main biomaterial used for production of total hip arthroplasty were investigated. The samples were produced via conventional two-stage sintering with T1 varies between 1450°C and 1550°C with heating rate of 20°C/min. The samples were then rapid cooled to T2 set at 1400°C with holding time of 12 hours. The microstructural and mechanical properties of the two-stage sintered ZTA are then investigated to determine the feasibility of MgO addition. Combination of two-stage sintering at T1 above 1500 and also small amount of MgO up to 0.5 vol% were shown to have positive effect on ZTA which exhibited improvement on its grain size, mechanical properties such as Vickers hardness, Young’s modulus and fracture toughness compared to undoped ZTA composites. The sample with 0.5 vol% MgO addition sintered at T1 of 1500°C and T2 1400°C was able to achieve Vickers hardness of 19.6 GPa, Young’s modulus of 408 GPa and fracture toughness of 6.8 MPam1/2 without significant grain growth compared to undoped ZTA composites.

scholarly journals Investigation of Nano-Mechanical and- Tribological Properties of Hydrogenated Diamond Like Carbon (DLC) Coatings

2016 ◽  
Vol 33 (6) ◽  
pp. 769-776 ◽  
Author(s):  
Y.-R. Jeng ◽  
S. Islam ◽  
K-T. Wu ◽  
A. Erdemir ◽  
O. Eryilmaz
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Friction Coefficient ◽  
Young’S Modulus ◽  
Tribological Properties ◽  
Young's Modulus ◽  
Chemical Vapour ◽  
Diamond Like Carbon ◽  
Dlc Coatings ◽  
Mechanical And Tribological Properties

AbstractHydrogenated diamond like Carbon (H-DLC) is a promising lubricious coating that attracted a great deal of interest in recent years mainly because of its outstanding tribological properties. In this study, the nano-mechanical and -tribological properties of a range of H-DLC films were investigated. Specifically, four kinds of H-DLC coatings were produced on Si substrates in pure acetylene, pure methane, 25% methane + 75% hydrogen, 50% methane + 50% hydrogen discharge plasmas using a plasma enhanced chemical vapour deposition (PECVD) system. Nano indentation was performed to measure the mechanical properties such as hardness and young's modulus and nanoscartching was performed to investigate the frictional behavior and wear mechanism of the H-DLC samples in open air. Moreover, Vickers indentation method was utilized to assess the fracture toughness of the samples. The results revealed that there is a strong correlation between the mechanical properties (hardness, young's modulus, fracture toughness) and the friction coefficient of DLC coatings and the source gas chemistry. Lower hydrogen to carbon ratio in source gas leads to higher hardness, young's modulus, fracture toughness and lower friction coefficient. Furthermore, lower wear volume of the coated materials was observed when the friction coefficient was lower. It was also confirmed that lower hydrogen content of the DLC coating leads to higher wear resistance under nanoscratch conditions.

Nanoindentation Measurements on Low-k Porous Silica Thin Films Spin Coated on Silicon Substrates

2003 ◽  
Vol 125 (4) ◽  
pp. 361-367 ◽  
Author(s):  
Xiaoqin Huang ◽  
Assimina A. Pelegri
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Mechanical Properties ◽  
Young’S Modulus ◽  
Microelectromechanical Systems ◽  
Young's Modulus ◽  
Porous Silica ◽  
Silicon Substrates ◽  
Silica Thin Films ◽  
Low K

MEMS (MicroElectroMechanical Systems) are composed of thin films and composite nanomaterials. Although the mechanical properties of their constituent materials play an important role in controlling their quality, reliability, and lifetime, they are often found to be different from their bulk counterparts. In this paper, low-k porous silica thin films spin coated on silicon substrates are studied. The roughness of spin-on coated porous silica films is analyzed with in-situ imaging and their mechanical properties are determined using nanoindentation. A Berkovich type nanoindenter, of a 142.3 deg total included angle, is used and continuous measurements of force and displacements are acquired. It is shown, that the measured results of hardness and Young’s modulus of these films depend on penetration depth. Furthermore, the film’s mechanical properties are influenced by the properties of the substrate, and the reproduction of the force versus displacement curves depends on the quality of the thin film. The hardness of the studied low-k spin coated silica thin film is measured as 0.35∼0.41 GPa and the Young’s modulus is determined as 2.74∼2.94 GPa.

Effect of Temperature and Holding Time on Zirconia Toughened Alumina (ZTA) Prepared by Two-Stage Sintering

2021 ◽  
Vol 1030 ◽  
pp. 11-18
Author(s):  
Teow Hsien Loong ◽  
Ananthan Soosai ◽  
Suresh Muniandy
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Young’S Modulus ◽  
Sintering Temperature ◽  
Young's Modulus ◽  
Holding Time ◽  
Effect Of Temperature ◽  
Two Stage ◽  
Pinning Effect ◽  
Zirconia Toughened Alumina

The microstructure and mechanical properties of Zirconia Toughened Alumina (ZTA) produced via two-stage sintering at various sintering temperature of T1 and T2 in addition to effect of various holding time were investigated. T1 temperature was set between the range of 1400°C to 1500°C with a heating rate of 20°C/min. The samples were then sintered at T2 ranging from 1350°C to 1400°C followed by various holding time between 2 hours to 12 hours. The sintered samples’ microstructural properties, bulk density, hardness (Vickers hardness), elastic modulus (Young’s modulus) and fracture toughness (K1C) were then determined. Compared to standard holding time of two-stage sintering which is 12 hours, results show that ZTA produced via two-stage sintering with shorter holding time of 4 hours with T1 set at 1500°C and T2 of 1450°C are capable of achieving full densification. In addition, the same sample were also able to achieve hardness up to 19 GPa, Young’s modulus of 390 GPa and fracture toughness of 6.1 MPam1/2. The improvement in mechanical properties can be mainly attributed to the absent of surface diffusion at T2 above 1400°C and also presence of Y-TZP which contributed to lower grain growth due to the pinning effect.

Mechanical Properties of Poly 3C-SiC Thin Films According to Carrier Gas (H2) Concentration

2008 ◽  
Vol 600-603 ◽  
pp. 867-870
Author(s):  
Gwiy Sang Chung ◽  
Ki Bong Han
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Mechanical Properties ◽  
Surface Roughness ◽  
Atomic Force Microscope ◽  
Young’S Modulus ◽  
Young's Modulus ◽  
Carrier Gas ◽  
Nano Indentation ◽  
Atomic Force

This paper presents the mechanical properties of 3C-SiC thin film according to 0, 7, and 10 % carrier gas (H2) concentrations using Nano-Indentation. When carrier gas (H2) concentration was 10 %, it has been proved that the mechanical properties, Young’s Modulus and Hardness, of 3C-SiC are the best of them. In the case of 10 % carrier gas (H2) concentration, Young’s Modulus and Hardness were obtained as 367 GPa and 36 GPa, respectively. When the surface roughness according to carrier gas (H2) concentrations was investigated by AFM (atomic force microscope), when carrier gas (H2) concentration was 10 %, the roughness of 3C-SiC thin was 9.92 nm, which is also the best of them. Therefore, in order to apply poly 3C-SiC thin films to MEMS applications, carrier gas (H2) concentration’s rate should increase to obtain better mechanical properties and surface roughness.

Measurement of Mechanical Properties for Thin Film Using Visual Image Tracing Method

2007 ◽  
Vol 124-126 ◽  
pp. 1701-1704 ◽  
Author(s):  
Sang Joo Lee ◽  
Seung Woo Han ◽  
Jae Hyun Kim ◽  
Hak Joo Lee
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Mechanical Properties ◽  
Young’S Modulus ◽  
Measurement System ◽  
Strain Measurement ◽  
Poisson’S Ratio ◽  
Young's Modulus ◽  
Visual Image ◽  
Poisson's Ratio

It is quite difficult to accurately measure the mechanical properties of thin films. Currently, there are several methods (or application) available for measuring mechanical properties of thin films. Their properties, however, have been determined by indirect methods such as cantilever beam test and diaphragm bulge test. This paper reports the efforts to develop a direct strain measurement system for micro/nano scale thin film materials. The proposed solution is the Visual Image Tracing (VIT) strain measurement system coupled with a micro tensile testing unit, which consists of a piezoelectric actuator, load cell, microscope and CCD cameras. The advantage of this system is the ability to monitor the real time images of specimen during the test in order to determine its Young’s modulus and Poisson’s ratio at the same time. Stress-strain curve, Young’s modulus, yield strength and Poisson’s ratio of copper thin film measured using VIT system are presented.

Densification, Microstructure, and Behavior of Hydroxyapatite Ceramics Sintered by Using Spark Plasma Sintering

2008 ◽  
Vol 130 (3) ◽  
Author(s):  
Shufeng Li ◽  
Hiroshi Izui ◽  
Michiharu Okano
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Flexural Strength ◽  
Relative Density ◽  
Young’S Modulus ◽  
Spark Plasma Sintering ◽  
Young's Modulus ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Temperature And Pressure

This paper discusses the dependence of the mechanical properties and microstructure of sintered hydroxyapatite (HA) on the sintering temperature and pressure. A set of specimens was prepared from as-received HA powder and sintered by using a spark plasma sintering (SPS) process. The sintering pressures were set at 22.3MPa, 44.6MPa, and 66.9MPa, and sintering was performed in the temperature range from 800°Cto1000°C at each pressure. Mechanisms underlying the interrelated temperature-mechanical and pressure-mechanical properties of dense HA were investigated. The effects of temperature and pressure on the flexural strength, Young’s modulus, fracture toughness, relative density, activation energy, phase stability, and microstructure were assessed. The relative density and grain size increased with an increase in the temperature. The flexural strength and Young’s modulus increased with an increase in the temperature, giving maximum values of 131.5MPa and 75.6GPa, respectively, at a critical temperature of 950°C and 44.6MPa, and the fracture toughness was 1.4MPam1∕2 at 1000°C at 44.6MPa. Increasing the sintering pressure led to acceleration of the densification of HA.

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