scholarly journals Synthesis and characterization of innovative insulation materials

2018 ◽  
Vol 149 ◽  
pp. 01078
Author(s):  
Aggeliki Skaropoulou ◽  
Afroditi Ntziouni ◽  
Dimitris Kioupis ◽  
Sotiris Tsivilis ◽  
Glikeria Kakali

Insulation elements are distinguished in inorganic fibrous and organic foamed materials. Foamed insulation materials are of great acceptance and use, but their major disadvantage is their flammability. In case of fire, they tend to transmit the flame producing toxic gases. In this paper, the synthesis and characterization of innovative inorganic insulation materials with properties competitive to commercial is presented. Their synthesis involves the mixing of inorganic raw material and water with reinforcing agent or/and foaming agent leading to the formation of a gel. Depending on raw materials nature, the insulation material is produced by freeze drying or ambient drying techniques of the gel. The raw material used are chemically benign and abundantly available materials, or industrial by-products and the final products are non-toxic and, in some cases, non-flammable. Their density and thermal conductivity was measured and found 0.02-0.06 g/cm3 and 0.03-0.04 W/mK, respectively.

1970 ◽  
Vol 17 (2) ◽  
pp. 208-212 ◽  
Author(s):  
Jolanta VĖJELIENĖ ◽  
Albinas GAILIUS ◽  
Sigitas VĖJELIS ◽  
Saulius VAITKUS ◽  
Giedrius BALČIŪNAS

The development of new thermal insulation materials needs to evaluate properties and structure of raw material, technological factors that make influence on the thermal conductivity of material. One of the most promising raw materials for production of insulation material is straw. The use of natural fibres in insulation is closely linked to the ecological building sector, where selection of materials is based on factors including recyclable, renewable raw materials and low resource production techniques In current work results of research on structure and thermal conductivity of renewable resources for production thermal insulating materials are presented. Due to the high abundance of renewable resources and a good its structure as raw material for thermal insulation materials barley straw, reeds, cattails and bent grass stalks are used. Macro- and micro structure analysis of these substances is performed. Straw bales of these materials are used for determining thermal conductivity. It was found that the macrostructure has the greatest effect on thermal conductivity of materials. Thermal conductivity of material is determined by the formation of a bale due to the large amount of pores among the stalks of the plant, inside the stalk and inside the stalk wall.http://dx.doi.org/10.5755/j01.ms.17.2.494


Foods ◽  
2021 ◽  
Vol 10 (6) ◽  
pp. 1411
Author(s):  
José Luis P. Calle ◽  
Marta Ferreiro-González ◽  
Ana Ruiz-Rodríguez ◽  
Gerardo F. Barbero ◽  
José Á. Álvarez ◽  
...  

Sherry wine vinegar is a Spanish gourmet product under Protected Designation of Origin (PDO). Before a vinegar can be labeled as Sherry vinegar, the product must meet certain requirements as established by its PDO, which, in this case, means that it has been produced following the traditional solera and criadera ageing system. The quality of the vinegar is determined by many factors such as the raw material, the acetification process or the aging system. For this reason, mainly producers, but also consumers, would benefit from the employment of effective analytical tools that allow precisely determining the origin and quality of vinegar. In the present study, a total of 48 Sherry vinegar samples manufactured from three different starting wines (Palomino Fino, Moscatel, and Pedro Ximénez wine) were analyzed by Fourier-transform infrared (FT-IR) spectroscopy. The spectroscopic data were combined with unsupervised exploratory techniques such as hierarchical cluster analysis (HCA) and principal component analysis (PCA), as well as other nonparametric supervised techniques, namely, support vector machine (SVM) and random forest (RF), for the characterization of the samples. The HCA and PCA results present a clear grouping trend of the vinegar samples according to their raw materials. SVM in combination with leave-one-out cross-validation (LOOCV) successfully classified 100% of the samples, according to the type of wine used for their production. The RF method allowed selecting the most important variables to develop the characteristic fingerprint (“spectralprint”) of the vinegar samples according to their starting wine. Furthermore, the RF model reached 100% accuracy for both LOOCV and out-of-bag (OOB) sets.


2012 ◽  
Vol 262 ◽  
pp. 405-409
Author(s):  
Yang Liu ◽  
Shan Shan Li ◽  
Xin Yan Yang ◽  
Chong Xing Huang

A new-type foam composites were fabricated by baking method from a mixture of cassava starch. A central composite design was constructed using the software Statistics Analysis System 9.0 to evaluate the static compression stress of foamed material. The optimum dosages of adhesive, foaming agent, catalyst were 2.0g, 6.0g, 2.4g, respectively; reaction temperature 65°C; reaction time 16 hour.


2016 ◽  
Vol 697 ◽  
pp. 433-436
Author(s):  
Shi Chao Zhang ◽  
Yu Feng Chen ◽  
Wei Wu ◽  
Hao Ran Sun ◽  
Guang Hai Wang ◽  
...  

In this paper, fumed nano-silica as the main raw material, nano-silica insulation materials were prepared by the dry processing. Research on humidity-reinforcement of nano-Silica insulation materials has been carried out and analyzed. When hygroscopicity of samples reach to 23%, the compressive strength 1.65MPa is at twice the one without high humidity-reinforcement, while the thermal conductivities are almost the same. Then, the action mechanism of high humidity-reinforcement method was analyzed. In humidity-reinforcement method, as vapor enters, silica sol is formed in the gap between one aggregate particle and another, and various condensation polymerization occurred in the drying process, which lead to aggregates connection and compressive strength improvement.


Foods ◽  
2018 ◽  
Vol 7 (12) ◽  
pp. 203 ◽  
Author(s):  
Friederike Gutöhrlein ◽  
Stephan Drusch ◽  
Sebastian Schalow

In order to evaluate by-products from food processing as alternative raw materials for pectin extraction, their amount of galacturonic acid (GalA) has to be analysed as a marker for pectin content. In the present study, significant differences in GalA release using different digestion methods are shown for pea hulls, as an example of by-products with a high content of cellulose. Complete digestion of the fibre matrix was assumed for Saeman hydrolysis as a reference protocol. Significantly lower GalA release was achieved by a treatment with trifluoracetic acid (TFA). An alternative treatment with ethylenediaminetetraacetic acid (EDTA) at pH 11 followed by an enzymatic digestion at pH 4.5 using a combination of polygalacturonase (Vegazyme M) and cellulase (Celluclast 1.5L) resulted in a similar release of GalA compared to Seaman hydolysis. Pea hull samples, analysed by this alternative protocol, showed on average a GalA content of 11.2%. Therefore, pea hulls may serve as new raw material for pectin extraction.


Author(s):  
Martins Andzs ◽  
Voldemars Skrupskis

Obtaining of a new ecological heat insulation material from always renewable raw material in nature, wood and hemp, derived from wood and hemp fibre remains left from the production process. The study was carried out to find hemp wood parts (shives), fiber, and material first possible compositions together with wood fibres, to produce heat insulation materials. The use of the heat insulation material would be meant for dwelling and recreation houses. In the present research the main characteristics of these materials are determined: moisture content, density, water absorption, as well as the coefficient of heat transmission.


2013 ◽  
Vol 662 ◽  
pp. 331-334
Author(s):  
Huan Qi Zhao ◽  
Guo Zhong Li

Cement-based lightweight insulation materials were made. Cement and fly ash are main raw materials. The self-developed composite excitation agent and foaming agent are used. The method of foaming is the physical foaming. The inflection of fiber dosage on the performance of lightweight insulation materials was researched. Its influencing mechanism was discussed. Experiments show that foaming lightweight insulation materials were made with 1.22MPa bending strength, 2.95MPa compressive strength and the 0.072W/mk coefficient of thermal conductivity when the fiber mixing content is 1.2%.


2021 ◽  
Vol 23 (05) ◽  
pp. 787-790
Author(s):  
Abhijit M ◽  
◽  
Suresh Kumar. B. V ◽  

Cowlesite is a Calcium Aluminum silicate CaAl2Si3O106H2O which formed under the hydrothermal conditions of low temperature (1800C) and pressure (1.013250bar). Cowlesite minerals are known for their peculiar occurrence. Synthesis of Cowlesite mineral was carried by suitable stoichiometric composition. Hydrothermal synthesized Cowlesite mineral was characterized by XRD, SEM, and EDAX. It crystallized in the orthorhombic system and a lattice parameter a=23.22Å, b=30.58Å, c=25.01Å, Volume of Unit cell=17758.79Å3, α=β=γ=900. EDAX results show the elemental concentration of raw material which was used.


2019 ◽  
pp. 658-687 ◽  
Author(s):  
R. V. Ralegaonkar ◽  
M. V. Madurwar ◽  
V. V. Sakhare

Due to ever increasing demand for the conventional construction materials as well as an increase in agro-industrial by-products it is essential to reuse these materials. As a smart city solution this chapter briefs an overview for the application of alternate raw materials as a principal source for the development of sustainable construction materials. The potential application of the discussed raw materials is elaborated as cementitious material, the aggregates as well as alternative reinforcement material. To understand the process of application, sustainable masonry product development is discussed in detail. In order to evaluate the feasibility of the raw material, the necessary physico-chemical test evaluation methods are also briefed. The developed end product performance evaluation is also discussed by desired tests as recommended by standards. The chapter concludes with a positive note that reuse of agro-industrial by-products is a feasible solution for the smart city development.


Coatings ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1091
Author(s):  
Alexandra Inberg ◽  
Dana Ashkenazi ◽  
Yishai Feldman ◽  
Omri Dvir ◽  
Deborah Cvikel

Fragments of decorated floor tiles were retrieved from the Akko Tower shipwreck, Israel. Most tiles were made of bright brown fired clay with a white glaze decorated with colored stenciled motifs (Type A); and others consisted of a red-brown fired clay body, coated with a brown pigment covered with transparent brown glaze (Type B). This study aimed to characterize the two tile types; to reveal information concerning the manufacturing process; and to determine the origin of their raw material. A multidisciplinary approach was used, including light microscopy, SEM-EDS, electron probe microanalysis with wavelength-dispersive X-ray spectroscopy (EPMA-WDS), XRD, Raman spectroscopy, and time-of-flight secondary ion mass spectrometry (TOF-SIMS) analyses. The characterization of both tile types demonstrated the use of different raw materials. The Type A tiles were covered with tin-opacified majolica glaze and colored with various mixtures of pigments. The blue color was due to pigment rich in cobalt; the yellow color was due to Naples yellow and lead-tin yellow I minerals; and the green, orange, and brown colors were all prepared by mixing the Naples yellow pigment with different minerals. These majolica glaze tiles were probably manufactured in Sicily. The brown coating of the Type B tiles was due to pigment rich in lead and iron minerals. These tiles were produced with different manufacturing processes, and apparently made in France.


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