scholarly journals The spheroidizing tendency and spheroidization mechanism of 75Cr1 steel

2018 ◽  
Vol 242 ◽  
pp. 01009
Author(s):  
Jiping Huo ◽  
Chong Zhou ◽  
Hua Wang
Keyword(s):  
Cold Rolling ◽  
Treatment Process ◽  
Ostwald Ripening ◽  
Cold Deformation ◽  
Annealing Process ◽  
Analysis Software ◽  
Isothermal Temperature ◽  
Optimum Heat ◽  
Optimum Heat Treatment ◽  
Ostwald Ripening Mechanism

Spheroidization annealing process was carried out on 75Cr1 steel after cold rolling. Using TEM, SEM and image analysis software Image-Pro Plus 6.0, the effects of cold rolling and spheroidization processes on microstructure and mechanical properties were analyzed. The result shows that the cold rolling leads to fragmentation of the cementite and formation of the defects, which induces faster lamellae break-up and accelerates the annealing process. With the increase of isothermal temperature and holding time, the dimension of the spheroidized carbides increase as driven by Ostwald ripening mechanism, whereas the hardness of the steel decreases. The prior cold rolling before annealing process causes the yield strength improve slightly, however shows little effect on the cold formability. The optimum heat treatment process is, holding the samples at 705oC for 6 hours with cold deformation ratio (ε) of 0.6.

Study on Microstructure and Property of Al-Si-Cu-Mg Casting Alloy during Solution and Aging Treatment

2014 ◽  
Vol 915-916 ◽  
pp. 650-653
Author(s):  
Li Jun Wei ◽  
Bo Long Li ◽  
Liu Yi Guan ◽  
Zuo Ren Nie
Keyword(s):  
Solid Solution ◽  
Artificial Aging ◽  
Treatment Process ◽  
Solution Treatment ◽  
Aging Treatment ◽  
Solution Time ◽  
Casting Alloy ◽  
The Matrix ◽  
Optimum Heat ◽  
Optimum Heat Treatment

The effect of the alloying elements Cu and Mg, the solution and artificial aging process on the microstructure and property were investigated. Solution treatment was carried out at 535 ± 5°C in different time for the Al-Si-Cu-Mg casting alloy, and the artificial aging was carried out at 160 ± 5°C and 175 ± 5°C and190 ± 5°C in different time. The microstructure has been investigated by Optical Microscopy, Scanning Electron Microscopy (SEM). We found that most of Cu and Mg element in the alloy gathered and formed multivariate composite phase at grain boundaries. With the increasing of solid solution time, the intermetallic phases will be dissolution into the matrix, and if the solid solution time is long enough, they will be distributed uniformly in alloy. With the increase of the aging temperature, the time for aging peak will be shorter, but the peak will be lower. Finally, we determine the optimum heat treatment process is 535°C × 12h + 175°C × 8h。

Failure Analysis and Study on Heat Treatment Process of Grate Bars Used in Sintering Trolley

2014 ◽  
Vol 1061-1062 ◽  
pp. 454-459
Author(s):  
An Min Li ◽  
Ding Ma ◽  
Qi Feng Zheng ◽  
Ruo Huai Chen ◽  
Qiang Li ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Treatment Process ◽  
Residual Austenite ◽  
Shrinkage Porosity ◽  
Heat Treatment Process ◽  
Fracture Characteristics ◽  
Heat Treated ◽  
Primary Means ◽  
Optimum Heat ◽  
Optimum Heat Treatment

The as-cast grate bar structure used in sintering trolley is primarily comprised of austenite and eutectic (eutectic austenite and eutectic carbide).The austenite is dendrite, while the carbides are reticular and chrysanthemum-like. The failed grate bar structure primarily consists of ferrite, carbide, martensite and residual austenite; cavity shrinkage and shrinkage porosity exist in the structure, and the fracture exhibits typical cleavage fracture characteristics. The primary means of failure are abrasion and fracture. The secondary carbides precipitated in the sample (quenching (1050°C+2.5h)+ tempering (390°C+2.5h)) and the other one (quenching (1050°C+2.5h)+ tempering (420°C+2.5h) ) are dispersed and refined. Compared with the as-cast one, their relative abrasion resistance performances respectively are 0.8645 and 0.8752.The values of hardness and impact toughness of the samples heat-treated are greater than those of the as-cast grate bar. The optimum heat treatment process is as follows: quenching (1050°C,2.5h) + tempering (390°C~420°C,2.5h)

scholarly journals Effect of Heat Treatments on Microstructural Evolution and Tensile Properties of 15Cr12MoVWN Ferritic/Martensitic Steel

Metals ◽  
2020 ◽  
Vol 10 (9) ◽  
pp. 1271
Author(s):  
Tingwei Ma ◽  
Xianchao Hao ◽  
Ping Wang
Keyword(s):  
Heat Treatment ◽  
Tensile Properties ◽  
Room Temperature ◽  
Treatment Process ◽  
Martensitic Steel ◽  
Heat Treatment Process ◽  
Lath Width ◽  
Optimum Heat ◽  
Martensitic Lath ◽  
Optimum Heat Treatment

In this study, the phase transformation temperature of 15Cr12MoVWN ferritic/martensitic steel was determined by differential scanning calorimetry to provide a theoretical basis for the design of a heat treatment process. An orthogonal design experiment was performed to investigate the relationship between microstructure and heat treatment parameters, i.e., normalizing temperature, cooling method and tempering temperature by evaluating the room-temperature and elevated-temperature tensile properties, and the optimum heat treatment parameters were determined. It is shown that the optimized heat treatment process was composed of normalizing at 1050 °C followed by air cooling to room temperature and tempering at 700 °C. Under the optimum heat treatment condition, the room-temperature tensile properties were 1014 MPa (UTS), 810.5 MPa (YS) and 18.8% (elongation), while the values are 577.5 MPa (UTS), 469 MPa (YS) and 39.8% (elongation) tested at 550 °C. The microstructural examination shows that the strengthening contributions from microstructural factors were the martensitic lath width, dislocations, M23C6, MX and grain boundaries of prior austenite grain (PAG) in a descending order. The main factors influencing the tensile strength of 15Cr12MoVWN steel were the martensitic lath width and dislocations.

scholarly journals Hardness and Conductivity of Die Forged ZYK530 Magnesium Alloy

2021 ◽  
Author(s):  
Fenghong CAO ◽  
Yaohui XU ◽  
Chang CHEN ◽  
Zhaohui QIN ◽  
Chi DENG
Keyword(s):  
Heat Treatment ◽  
Electrical Conductivity ◽  
Treatment Process ◽  
Mg Alloy ◽  
Heat Treatment Process ◽  
Optimum Heat ◽  
The Relationship ◽  
Optimum Heat Treatment ◽  
Good Agreement ◽  
Peak Value

The relationship among the microstructure, hardness and electrical conductivity of the as-forged ZYK530 Mg alloy after heat treatment was analyzed and studied using a microscope, X-Ray Diffractometer, eddy current conductivity meter, and Vickers microhardness tester, to explore optimum heat treatment process of ZYK530 Mg alloy. The results show that: with the prolongation of holding time, the electrical conductivity and microhardness show the same change trend, both of which show an oscillatory upward trend, and then decrease in an oscillatory downward trend after reaching the  peak value. There is a linear positive correlation between the conductivity and the hardness, and the fitting results of the conductivity and hardness are in good agreement with the measured results; combined with the actual production, when the heat-treatment is 480 ℃ × 8 h + 220 ℃ × 3 h, the highest hardness is 79.2 HV, the electroconductivity is 36.2%IACS, and the comprehensive performance is the best, which is the best heat treatment process.

Crystallization of Amorphous Sputtered NiTi Shape-Memory Alloy Films

1995 ◽  
Vol 398 ◽  
Author(s):  
F.F. Gong ◽  
H.M. Shen ◽  
Y.N. Wang
Keyword(s):  
Shape Memory ◽  
Annealing Temperature ◽  
Optimum Shape ◽  
Niti Shape Memory Alloy ◽  
X Ray Diffraction ◽  
Initial Stage ◽  
Average Grain Size ◽  
Optimum Heat ◽  
Diffraction Patterns ◽  
Optimum Heat Treatment

ABSTRACTThe crystallization of amorphous sputtered NiTi films was investigated for selected heat treatments. From x-ray diffraction patterns, when the films were annealed below the crystallization temperature, the intensity of the broad maximum centered at 2θ = 43.5° increased with increasing the annealing temperature and time. When the films were annealed at 550°C for 0.5hr, parent B2 phase and Ni4Ti3 precipitates appeared. For annealing temperature above 700°C, the films showed embrittlement and volatilization. Therefore the optimum heat treatment for the optimum shape memory effect is found. The average grain size increased slowly in the initial stage of annealing but remained almost unchanged when the films were annealed for more than 1hr. This is because the grain boundary grooving caused by the titanium at a certain temperature volatilization seriously hinder the grain growth.

scholarly journals Texture Evolution and Control of 2524 Aluminum Alloy and Its Effect on Fatigue Crack Propagation Behavior

2021 ◽  
Vol 11 (12) ◽  
pp. 5550
Author(s):  
Yuqiang Chen ◽  
Chuang Xiong ◽  
Wenhui Liu ◽  
Suping Pan ◽  
Yufeng Song ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Aluminum Alloy ◽  
Fatigue Crack ◽  
Cold Rolling ◽  
Texture Evolution ◽  
Cold Deformation ◽  
Solution Treatment ◽  
Second Phase ◽  
Fatigue Crack Growth Resistance ◽  
Volume Fractions

The influences of cold rolling and subsequent heat treatment on the microstructure evolution of 2524 alloy were investigated using an orientation distribution function (ODF) and electron back-scattered diffraction (EBSD). A preparation method of 2524-T3 aluminum alloy with a strong Brass texture was developed, and its effect on the fatigue properties of the alloy was investigated using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The results show that with the increase in cold rolling deformation from 0% to 80%, the volume fractions of Brass, copper, and S textures in the 2524-T3 alloy also increase, especially in the case of Brass and S textures. However, the volume fractions of cube and Goss textures are reduced significantly, especially for cube textures, which are decreased by 57.4%. Reducing coarse second-phase particles (CSPs) is conducive to the formation of a strong deformation texture during cold rolling. A 10% deformation at each rolling pass, followed by a step annealing, helps the preservation of a Brass texture even after solution treatment at 500 °C for 0.5 h, while a large cold deformation followed by high-temperature annealing helps the formation of a strong cube texture. The Brass texture can enhance the strength while decreasing the fatigue crack growth resistance of this alloy.

scholarly journals Development of cyclosporine-loaded nanoemulsion for topical treatment of psoriasis

2019 ◽  
Vol 10 (SPL1) ◽  
Author(s):  
Siti Hajar Musa ◽  
Norazlinaliza Salim ◽  
Norashikin Shamsudin ◽  
Mahiran Basri ◽  
Hamid Reza Fard Masoumi
Keyword(s):  
Topical Treatment ◽  
Oral Delivery ◽  
Ostwald Ripening ◽  
Normal Skin ◽  
Severe Case ◽  
Transepidermal Water Loss ◽  
Water Soluble ◽  
Colloidal System ◽  
Thaw Cycle ◽  
Ostwald Ripening Mechanism

Psoriasis is an autoimmune disease in which the symptoms are obviously appeared on the patient's body with thick, red/ salmon colour and dry patches. Clinically, topical treatment has been the first-line treatment for psoriasis, whether or not the systemic and phototherapy is required. Currently, cyclosporine is one of the standard oral medications used for moderate to a severe case of psoriasis. However, through oral delivery, it cannot be used for a long period and causes bad effects. Thus, a new delivery system of cyclosporine is in need to be developed to overcome its toxic effects by skipping the first pass body metabolism. A nanoemulsion colloidal system, as the main carrier for big, non-water-soluble cyclosporine, is believed could help in the delivery of activities through the stratum corneum of the skin layer. Nanoemulsion system, which mainly consists of oil phase (a mixture of virgin coconut oil, nutmeg oil, and cyclosporine), aqueous phase, and surfactant, was successfully being developed by using Mixture Experimental Design optimization tool with droplet size range between 110-160 nm. Stability studies were carried out with respect to; pH, storage at different temperatures, coalescence and Ostwald ripening mechanism, free-thaw cycle, and FTIR analysis. From the obtained results, this newly-developed nanoemulsion containing cyclosporine was proven to be stable and successfully maintained its physicochemical characteristics even after 3 months of storage at 4°C and 25°C temperature. Ostwald ripening mechanism contributed to the instability of the system at 45°C of storage. Introduction of standard cyclosporine, blank nanoemulsion, and nanoemulsion containing cyclosporine to the HaCaT cells in the treatment of MTT assay study has confirmed the safety of the nanoemulsion. Permeation study of the newly-developed nanoemulsion containing cyclosporine showed it was best fitted the Korsmeyer-Peppas kinetic model. In addition, the transepidermal water loss and hydration studies proved the efficacy of cyclosporine-loaded nanoemulsion in increasing the water storage of the volunteers’ normal skin after 3h of application.  

Effect of Rolling Deformation on Corrosion Behaviour of AISI 304L in 3% NaCl Solution

2021 ◽  
Vol 406 ◽  
pp. 375-384
Author(s):  
Lazhar Yahia ◽  
Elamine Nouicer ◽  
Fatima Zohra Benlahreche
Keyword(s):  
Cold Rolling ◽  
Corrosion Behaviour ◽  
Cold Deformation ◽  
Austenitic Stainless Steels ◽  
Rolling Process ◽  
Mechanical Resistance ◽  
304L Stainless Steel ◽  
Aisi 304L ◽  
Pitting Potential ◽  
Rolling Deformation

It is well known that the mechanical resistance of austenitic stainless steels can be increased considerably by cold rolling process.¶ The cold rolling effect on corrosion resistance of AISI 304L stainless steel in 3% Sodium Chloride solution was investigated by potentiodynamic polarisation and by Scanning Electronic Microscopy (SEM). The pitting corrosion in this environment is related to the rate of cold deformation. The cold rolling induces important changes in the microstructure and involves phase transformation (γ→a'). The AISI 304L developes martensitic structure after 16% cold working. The potentiodynamic results show a moderate variation of the passivity zone, a remarkable decrease in the pitting potential and a free potential. The results also show an increase in the current density. However, it seems that the critical deformation rate appears to start at approximately 50% of the rolling deformation where the passivation current is minimal. After the polarisation tests, metastable pits are observed using SEM and the most probable initiation causes are discussed

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