Optimization of tribo-mechanical properties of boron carbide reinforced magnesium metal matrix composite

Author(s):  
Manickam Ravichandran ◽  
Gopathy Veerappan ◽  
Veeman Dhinakaran ◽  
Jitendra Kumar Katiyar

In this study, magnesium–boron carbide composites are developed through the powder metallurgy technique and investigated for their tribological properties using a pin-on-disc tribometer. The process parameters such as load, sliding distance, sliding velocity, and concentration (wt%) of boron carbide are optimized using Taguchi's L16 array. A lower wear rate of magnesium–boron carbide composite is obtained at optimized process parameters. Further, the analysis of variance result shows that the most dominating factor that affects the wear loss is load followed by concentration of boron carbide reinforcement. Moreover, the optimum parameters for the low wear rate of magnesium–boron carbide composites are obtained as 5 N, 6 wt% of boron carbide, 1200 m, and 3 m/s through signal-to-noise ratio analysis. Further, the mechanical properties of magnesium–boron carbide composites such as hardness and compressive strength are also analyzed. The result shows that the hardness and compressive strength of magnesium–boron carbide composites are improved with the inclusion of boron carbide reinforcement.

Author(s):  
Fathima Banu Raza ◽  
Anand Kumar

The o-rings in ball retained overdentures deteriorate with time and need replacement to restore the retentive quality. We evaluated retrospectively the mechanical properties of o-rings after 3 years in function in one and two-piece implant-supported overdentures. The o-rings were retrieved from one-piece (Myriad snap, Equinox-Straumann, 3.3 x 13mm) and two-piece (Neo Biotech, 3.3 x 13mm) implant-supported overdenture patients. A total of 16 pairs of matrices were tested for wear, type of damage and elasticity using Pin on Disc method, USB Digital Camera in 30x zoom and Universal Tensile Machine respectively. The statistical analysis for independent groups were done with the Mann-Whitney U test. Assessment of used O-rings showed 84% more wear in the two-piece system with an abrasive type of damage while 46% wear in the one-piece system with a compressive type of damage. The o-rings in one-piece system showed increase in elongation and maximum displacement to 2% and 7% respectively, while two-piece system showed decrease in elongation and maximum displacement by 13% and 6% respectively. In one-piece system, the loss of retention was more with slow wear rate and in two-piece system, the wear resistance of O-rings decreased due to increased stiffness. Further studies to evaluate the changes in O-ring with increased sample size and at interval 1 year will pave way for insight into the progressive changes in the mechanical properties of an O-ring.


Materials ◽  
2019 ◽  
Vol 12 (2) ◽  
pp. 313 ◽  
Author(s):  
Xiaoyang Wang ◽  
Hongqiang Ru

Cu–Fe-based friction materials with flake graphite, granulated carbon black, and high-strength graphite as lubricating phase were prepared by the powder metallurgy method. The effects of different types and mass fraction of lubricating phase on the microstructure, mechanical properties, and tribological properties were investigated. The results show that when the mass fraction of granulated carbon black is 5 wt%, it is easy to form a good interface with the matrix, but the interface is prone to pores and cracks when its mass fraction is 10 wt%. The bending strength and compressive strength properties of the composites increased with increasing in the mass fraction of granulated carbon black and reached the maximum of 40 MPa and 70 MPa at 5 wt% granulated carbon black, after which bending strength and compressive strength all decreased. The friction coefficient and the wear loss of the materials initially decreased as the mass fraction of granulated carbon black increased and obtained minimum of 0.436 and 0.145 mm when the mass fraction of granulated carbon black was 5 wt%, then ascended. Compared with the sample with 5 wt% high-strength graphite as lubricating phase, the sample with 5 wt% granulated carbon black as lubricating phase had better sintering performance, mechanical properties, and tribological properties.


2014 ◽  
Vol 20 (2) ◽  
pp. 233-240 ◽  
Author(s):  
Violeta Leskevicienė ◽  
Dalia Nizevicienė

Phosphoanhydrite was obtained by processing dihydrate phosphogypsum generated during phosphoric acid production at Joint Stock Company (JSC) Lifosa (Lithuania). The influence on the properties of phosphoanhydrite of the treament process? parameters was determined, including the conditions of phosphogypsum neutralisation in the lime suspension; temperature and duration of calcination of neutralized phosphogypsum to phosphoanhydrite; fineness of ground anhydrite; selection of additives activating the hydration of anhydrite and their amounts. Upon adding activators of anhydrite hydration, K2SO4 or Na2SO4, the data of XRD and IR spectral analysis show that the specimens after 1 day of phosphoanhydrite hydration with additives contain complex salts - syngenite upon using K2SO4 additive and glauberite in the case of Na2SO4 additive. These additives act as crystallization centers and accelerate hydration. It has been determined that the specimens of phosphoanhydrite calcined at a temperature of 900 ? C with 2 % K2SO4 additive have the best physical and mechanical properties. Already after 1 day of hardening the specimens acquired a compressive strength of 21.18 MPa, and after 28 days of hardening they had a compressive strength of 58.5 MPa (dry specimens).


2020 ◽  
Vol 38 (3A) ◽  
pp. 308-318
Author(s):  
Reem A. Mohammed

The material utilized for manufacturing artificial dentures should have high-grade mechanical properties in order to resist heavy forces inside the mouth. This study includes investigation of some of the mechanical properties (wear rate resistance, compression strength, and hardness) of the specimens prepared by (hand lay-up) method. The wear behavior experiments were performed on (a pin-on-disk tester) under various factors 5%, 8%, 11%, 14%, 17% weight fraction of orange peel, (10, 15, 20 N) load applied and (5, 10, 15 minutes) sliding time, and analysis these experimentally by using the Taguchi’s experimental design (L9) (MINITAB 16). Tests explicated that the specimens (polymethylmethacrylate - 17% orange peel) composites have the best wear rate resistance, compression strength and hardness shore D (0.040×10-5 cm3/N.mm, 142 MPa, 86 shore D) respectively than other specimens (polymethylmethacrylate - 5%, 8%, 11%, 14% wt. orange peel) and these specimens better than the specimens standard polymethylmethacrylate, which could be attributed to the homogeneous dispersion of orange peel particles in the polymethylmethacrylate resin matrix. The results (signal to noise ratio) showed the factors (17% weight fraction) orange peels, (20 N) load applied, and (5 min) sliding time gives the best wear rate resistance. The results of the analysis of variance showed the sliding time (C) is the essential factor effect on the wear rate resistance followed by (A) weight fraction of orange peels and (B) load applied were less affected on wear behavior rate.


Author(s):  
Sandeep Kumar Khatkar ◽  
Rajeev Verma ◽  
Suman Kant ◽  
Narendra Mohan Suri

This article statistically investigates the effect of various parameters such as material factors: silicon carbide (SiC) reinforcement, graphite (Gr) reinforcement and mechanical factors: normal load, sliding distance and speed on the sliding wear rate of vacuum stir cast self-lubricating AZ91D-SiC-Gr hybrid magnesium composites. The sliding wear tests have been performed on pin-on-disc tribometer at 10-50N loads, 1-3m/s sliding speed and 1000-2000m sliding distance. It has been examined that hybrid composites yielded improved wear resistance with reinforcement of SiC and solid lubricant graphite. ANOVA and signal-to-noise ratio investigation indicated that applied load was the most critical factor influencing the wear rate, followed by sliding distance. Further, the AZ91D/5SiC/5Gr hybrid composite has exhibited the best wear properties. From the SEM and EDS analysis of worn surfaces, delamination was confirmed as the dominant wear mechanism for AZ91D-SiC-Gr hybrid composites.


2018 ◽  
Vol 7 (4.5) ◽  
pp. 526
Author(s):  
Ch. V. M. Prasad ◽  
K. Mallikarjuna Rao

In the present work, Al380 Al alloy and B4C metal matrix composite was fabricated with different weight fractions (1%,2% and 3%) using compo-casting method. The wear properties of fabricated composite is tested by pin on disc apparatus. On different loads of 30N,60N and 90N the wear tests are performed. The mechanical properties of hardness and tensile strength are performed on brinell’s hardness apparatus and Ultimate tensile machine. The study of homogeneous distribution of B4C particles were examined by scanning electron microscope (SEM) in the composites. The result shows that the Al380 Al alloy reinforced with B4C particles, that composite improves the mechanical properties and wear rate. Increasing of wear rate with the increase in B4C particles in composites. Using Opti- cal microscope, the study of worn surfaces of pins were analyzed. 


2017 ◽  
Vol 69 (5) ◽  
pp. 715-722 ◽  
Author(s):  
Sanjay Mohan Sharma ◽  
Ankush Anand

Purpose This paper aims to investigate the effect of CaF2 (calcium fluoride) addition as a solid lubricant on the friction and wear behaviour of sintered Fe-Cu-C materials under different loads. Design/methodology/approach In this study, the effects of CaF2 added in varying weight percentages on the friction-wear properties of Fe-2Cu-0.8C alloys are investigated. Five Fe-2Cu-0.8C-based compositions comprising CaF2 in 0, 3, 6, 9 and 12 Wt.% were prepared using the single-stage compaction and sintering technique. Friction coefficient, wear loss, hardness and compressive strength of the specimens were measured. The worn-out surfaces were analysed using a scanning electron microscope. Friction and wear tests were carried out on pin-on-disc machine under dry sliding conditions at room temperature. Findings The alloy with 3 Wt.% CaF2 was found to be useful in improving wear and friction properties, whereas higher contents of CaF2 resulted in increased wear and friction. Apart from enhanced tribological properties, a slight decrease in the compressive strength was also observed in the 3-Wt.%-CaF2-added sample. Adhesion and abrasion were the prominent wear types observed during this study. Originality/value A new self-lubricating composite is developed where CaF2 is used as a solid lubricant in a Fe-Cu-C-based matrix. CaF2, being a high-temperature lubricant, is tried and tested for friction and wear at room temperature, and the results show that the addition of CaF2 in Fe-Cu-C improved its friction and wear properties. Thus, the developed material can be used for antifriction applications.


2018 ◽  
Vol 7 (1) ◽  
pp. 48-60 ◽  
Author(s):  
Shashi Prakash Dwivedi ◽  
Satpal Sharma ◽  
Raghvendra Kumar Mishra

AbstractThe effect of waste carbonized eggshell and silicon carbide (SiC) wt.% on the dry sliding wear behavior of AA2014 alloy green composites produced by electromagnetic stir casting method was investigated. The percentage of waste carbonized eggshell particles and SiC particles varied from 2.5% to 12.5%. The tribological behavior of AA2014/waste carbonized eggshell/SiC hybrid green metal matrix composites (MMCs) was investigated on a pin-on-disc apparatus. The weight percentages of waste carbonized eggshell and of SiC, normal load, and sliding speed and distance were taken as input process parameters, and wear rate was taken as a response. Response surface methodology was used to plan and analyze the experiment. Minimum wear rate was found to be 8.89×10−5mm3/m with desirability one at optimum parameters of 1.75 m/s (sliding velocity), 6.5 (carbonized eggshell wt.%), 34.24 N (normal load), 1219.63 m (sliding distance), and 11 wt.% (SiC wt.%). In the confirmation experiment, the experimental wear rate of the hybrid green MMC at optimum parameters was found to be 9.5×10−5. Results showed that the experimental wear rate and density of the hybrid green MMC were reduced by about 36.66% and 0.35%, respectively, compared with the matrix.


2013 ◽  
Vol 2013 ◽  
pp. 1-8 ◽  
Author(s):  
M. Sudheer ◽  
N. Karthik Madhyastha ◽  
M. Kewin Amanna ◽  
B. Jonthan ◽  
K. Mayur Jayaprakash

The present work reveals the effect of the addition of commercial MoS2 (10 wt%) particles on mechanical and two-body abrasive wear behavior of epoxy with/without glass fiber mat reinforcement. The composites were fabricated using casting and simple hand lay-up techniques followed by compression molding. The mechanical properties such as density, hardness, tensile, and flexural properties were determined as per ASTM standards. The abrasive wear testing was carried out using pin-on-disc wear tester for different loads and abrading distances at constant speed of 1 m/s. A significant reduction in wear loss and specific wear rate was noticed after the incorporation of MoS2 filler allowing less wear of matrix during abrasion which in turn facilitated lower fiber damage. However the incorporation of MoS2 particles had a detrimental effect on most of the mechanical properties of the composites. The worn surface features were investigated through scanning electron microscopy (SEM) in order to investigate the wear mechanisms.


Author(s):  
YP Vaishnu ◽  
K Bindu Kumar ◽  
S Rani

The development of deposition of different metal processes established on electrodeposition of nickel, different alloy and composite coatings on different surfaces has attested an upsurge in interest among researchers. In latter years, these coatings have exhibited promising corrosion and wear resistance properties. Also, huge number of modern developments became most critical from macro to nano level applications. It is well known that one may shape the microstructure and the phase present in the material to recover the mechanical properties of highly pure materials, specifically metals. Co-deposition of fine particles inside a metal matrix to generate composite coatings has treated as a practical strategy to acquire enhanced mechanical properties like wear resistance, corrosion resistance and lubrication. In this work, CuO/Ni composite coatings are processed on the small cylindrical pin by electro brush plating to evaluate the wear and corrosion resistance. To examine the effects about the different parameters of processes on wear loss of CuO/Ni composite coating, L16(44) orthogonal experiment is designed and conducted with four process parameters (voltage, concentration of nanoCuO particles in g/l, temperature and thickness) which are selected as factors. Design of experiment is employed to resolve the effects of process parameters on the wear loss of composite coatings. It is concluded that concentration of CuO nanoparticle and voltage are the most significant factors for the wear loss.


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