Online measurements for quality in the metals industries: does automated inspection meet the need?

2004 ◽  
Vol 31 (1) ◽  
pp. 2-7
Author(s):  
Keyword(s):  
Automated Inspection ◽  
Online Measurements

The Investigation of Fluorine Induced Novel Probe Marker Discoloration

2018 ◽  
Author(s):  
W.F. Hsieh ◽  
Henry Lin ◽  
Vincent Chen ◽  
Irene Ou ◽  
Y.S. Lou
Keyword(s):  
Electric Field ◽  
Dark Field ◽  
Inspection System ◽  
Automated Inspection ◽  
Stress Tests ◽  
Auger Analysis ◽  
Corrosion Film ◽  
Scan Data ◽  
Thickness Variations ◽  
One Year

Abstract This paper describes the investigation of donut-shaped probe marker discolorations found on Al bondpads. Based on SEM/EDS, TEM/EELS, and Auger analysis, the corrosion product is a combination of aluminum, fluorine, and oxygen, implying that the discolorations are due to the presence of fluorine. Highly accelerated stress tests simulating one year of storage in air resulted in no new or worsening discolorations in the affected chips. In order to identify the exact cause of the fluorine-induced corrosion, the authors developed an automated inspection system that scans an entire wafer, recording and quantifying image contrast and brightness variations associated with discolorations. Dark field TEM images reveal thickness variations of up to 5 nm in the corrosion film, and EELS line scan data show the corresponding compositional distributions. The findings indicate that fluorine-containing gases used in upstream processes leave residues behind that are driven in to the Al bondpads by probe-tip forces and activated by the electric field generated during CP testing. The knowledge acquired has proven helpful in managing the problem.

Analysis of paper, print and press interaction from online measurements in a press room

2007 ◽  
Vol 22 (3) ◽  
pp. 383-387 ◽  
Author(s):  
Jörgen Ungh ◽  
Carl-Magnus Nilsson ◽  
Antanas Verikas
Keyword(s):  
Online Measurements ◽  
Press Room

scholarly journals Automated maintenance feasibility testing on the EU DEMO Automated Inspection and Maintenance Test Unit (AIM-TU)

2021 ◽  
Vol 170 ◽  
pp. 112517
Author(s):  
S. Jimenez ◽  
D. Bookless ◽  
R. Nath ◽  
W.J. Leong ◽  
J. Kotaniemi ◽  
...  
Keyword(s):  
Automated Inspection ◽  
Test Unit ◽  
Inspection And Maintenance ◽  
Feasibility Testing ◽  
The Eu

scholarly journals Automatic 1D 1H NMR Metabolite Quantification for Bioreactor Monitoring

Metabolites ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 157
Author(s):  
Roy Chih Chung Wang ◽  
David A. Campbell ◽  
James R. Green ◽  
Miroslava Čuperlović-Culf
Keyword(s):  
High Throughput ◽  
Nmr Metabolomics ◽  
Gene Therapies ◽  
Quantification Method ◽  
Minimal Sample ◽  
Enhanced Production ◽  
Bioreactor Monitoring ◽  
Online Measurements ◽  
Metabolite Quantification ◽  
Set Up

High-throughput metabolomics can be used to optimize cell growth for enhanced production or for monitoring cell health in bioreactors. It has applications in cell and gene therapies, vaccines, biologics, and bioprocessing. NMR metabolomics is a method that allows for fast and reliable experimentation, requires only minimal sample preparation, and can be set up to take online measurements of cell media for bioreactor monitoring. This type of application requires a fully automated metabolite quantification method that can be linked with high-throughput measurements. In this review, we discuss the quantifier requirements in this type of application, the existing methods for NMR metabolomics quantification, and the performance of three existing quantifiers in the context of NMR metabolomics for bioreactor monitoring.

scholarly journals Evaluation of Process Control Schemes for Sour Water Strippers in Petroleum Refining

Processes ◽  
2021 ◽  
Vol 9 (2) ◽  
pp. 363
Author(s):  
Chii-Dong Ho ◽  
Yih-Hang Chen ◽  
Chao-Min Chang ◽  
Hsuan Chang
Keyword(s):  
Feedback Control ◽  
Prediction Models ◽  
Feedforward Control ◽  
Absolute Error ◽  
Dynamic Responses ◽  
Control Schemes ◽  
Online Measurements ◽  
Measurement Delay ◽  
Water Feed ◽  
Sour Water

For the sour water strippers in petroleum refinery plants, three prediction models were developed first, including the estimators of sour water feed concentrations using convenient online measurements, the minimum reboiler duty and the corresponding internal temperature at a specific location (Tstage,29). Feedforward control schemes were developed based on these prediction models. Four categories of control schemes, including feedforward, feedback, feedback with external reset, and feedforward-feedback, were proposed and evaluated by the rigorous dynamic simulation model of the sour water stripper for their dynamic responses to the sour water feed stream disturbances. The comparison of control performance, in terms of the settling time, integrated absolute error (IAE) of the NH3 concentration of the stripped sour water and IAE of the specific reboiler duty, reveals that FFT (feedforward control of Tstage,29) and FBA-DT3 (feedback control with 3 min concentration measurement delay) are the best control schemes. The second-best control scheme is FBAT (cascade feedback control of concentration with temperature).

scholarly journals Advanced Kinetic Modeling of Bio-co-polymer Poly(3-hydroxybutyrate-co-3-hydroxyvalerate) Production Using Fructose and Propionate as Carbon Sources

Processes ◽  
2021 ◽  
Vol 9 (8) ◽  
pp. 1260
Author(s):  
Stefanie Duvigneau ◽  
Robert Dürr ◽  
Jessica Behrens ◽  
Achim Kienle
Keyword(s):  
Kinetic Model ◽  
Kinetic Modeling ◽  
Feed Rate ◽  
Raw Materials ◽  
Carbon Sources ◽  
Exhaust Gas ◽  
Current Yield ◽  
Promising Alternative ◽  
Parameter Variations ◽  
Online Measurements

Biopolymers are a promising alternative to petroleum-based plastic raw materials. They are bio-based, non-toxic and degradable under environmental conditions. In addition to the homopolymer poly(3-hydroxybutyrate) (PHB), there are a number of co-polymers that have a broad range of applications and are easier to process in comparison to PHB. The most prominent representative from this group of bio-copolymers is poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV). In this article, we show a new kinetic model that describes the PHBV production from fructose and propionic acid in Cupriavidus necator (C. necator). The developed model is used to analyze the effects of process parameter variations such as the CO2 amount in the exhaust gas and the feed rate. The presented model is a valuable tool to improve the microbial PHBV production process. Due to the coupling of CO2 online measurements in the exhaust gas to the biomass production, the model has the potential to predict the composition and the current yield of PHBV in the ongoing process.

scholarly journals Variable Temperature Synthesis of Tunable Flame-Generated Carbon Nanoparticles

2021 ◽  
Vol 7 (2) ◽  
pp. 44
Author(s):  
Francesca Picca ◽  
Angela Di Pietro ◽  
Mario Commodo ◽  
Patrizia Minutolo ◽  
Andrea D’Anna
Keyword(s):  
Carbon Nanoparticles ◽  
Variable Temperature ◽  
Flame Temperature ◽  
Cost Effective ◽  
Synthesis Process ◽  
Electrical Mobility ◽  
Material Synthesis ◽  
Online Measurements ◽  
Degree Of Graphitization

In this study, flame-formed carbon nanoparticles of different nanostructures have been produced by changing the flame temperature. Raman spectroscopy has been used for the characterization of the carbon nanoparticles, while the particle size has been obtained by online measurements made by electrical mobility analysis. The results show that, in agreement with recent literature data, a large variety of carbon nanoparticles, with a different degree of graphitization, can be produced by changing the flame temperature. This methodology allows for the synthesis of very small carbon nanoparticles with a size of about 3-4 nm and with different graphitic orders. Under the perspective of the material synthesis process, the variable-temperature flame-synthesis of carbon nanoparticles appears as an attractive procedure for a cost-effective and easily scalable production of highly tunable carbon nanoparticles.

scholarly journals In-Plane Heatwave Thermography as Digital Inspection Technique for Fasteners in Aircraft Fuselage Panels

2020 ◽  
Vol 11 (1) ◽  
pp. 132
Author(s):  
Michael Stamm ◽  
Peter Krüger ◽  
Helge Pfeiffer ◽  
Bernd Köhler ◽  
Johan Reynaert ◽  
...  
Keyword(s):  
Inspection Time ◽  
Scanning Laser ◽  
Aviation Industry ◽  
Automated Inspection ◽  
Comparison Study ◽  
Laser Doppler Vibrometry ◽  
Inspection Method ◽  
Aircraft Fuselage ◽  
Temporal Tracking ◽  
Lock In

The inspection of fasteners in aluminium joints in the aviation industry is a time consuming and costly but mandatory task. Until today, the manual procedure with the bare eye does not allow the temporal tracking of a damaging behavior or the objective comparison between different inspections. A digital inspection method addresses both aspects while resulting in a significant inspection time reduction. The purpose of this work is to develop a digital and automated inspection method based on In-plane Heatwave Thermography and the analysis of the disturbances due to thermal irregularities in the plate-like structure. For this, a comparison study with Ultrasound Lock-in Thermography and Scanning Laser Doppler Vibrometry as well as a benchmarking of all three methods on one serviceable aircraft fuselage panel is performed. The presented data confirm the feasibility to detect and to qualify countersunk rivets and screws in aluminium aircraft fuselage panels with the discussed methods. The results suggest a fully automated inspection procedure which combines the different approaches and a study with more samples to establish thresholds indicating intact and damaged fasteners.

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