scholarly journals COMPRESSION OF ECAPED TITANIUM MICRO-PILLARS FOR TWO PRINCIPAL ORIENTATIONS

2020 ◽  
Vol 27 ◽  
pp. 1-5
Author(s):  
David Vokoun ◽  
Jan Maňák ◽  
Karel Tesař ◽  
Stanislav Habr
Keyword(s):  
Room Temperature ◽  
Focused Ion Beam ◽  
Mechanical Response ◽  
Thermomechanical Processing ◽  
Ion Beam ◽  
Orientation Dependence ◽  
Material Strength ◽  
Angular Pressing ◽  
Macro Scale ◽  
Micro Pillars

The thermomechanical processing by equal-channel angular pressing (ECAP) is used for certain metals and alloys in order to make their structure fine and to increase material strength. In the previous study done at our institute, grade 2 titanium was successfully processed using four consecutive route A passes via a 90 ° ECAP die with high backpressure at room temperature. Orientation dependence of compressive and tensile loading of ECAPed titanium samples was demonstrated at macro-scale. However, scarce attention has been paid so far to the mechanical behavior of ECAPed titanium samples at micro-scale. In the present study, compression experiments on titanium micropillars, fabricated using focused ion beam, are carried out for two main directions in respect to preceding ECAP pressing (insert and extrusion directions). The purpose of this study is to discuss the orientation dependence of mechanical response during compression of the as-ECAPed titanium micro-pillars.

Nanocomposite Polyurethane Foams Via POSS Blends

2002 ◽  
Vol 733 ◽  
Author(s):  
Brock McCabe ◽  
Steven Nutt ◽  
Brent Viers ◽  
Tim Haddad
Keyword(s):  
High Temperature ◽  
Sample Preparation ◽  
Room Temperature ◽  
Focused Ion Beam ◽  
Ion Beam ◽  
Polyurethane Foams ◽  
Development Projects ◽  
Polymer Systems ◽  
Polyurethane Resin ◽  
Military Development

AbstractPolyhedral Oligomeric Silsequioxane molecules have been incorporated into a commercial polyurethane formulation to produce nanocomposite polyurethane foam. This tiny POSS silica molecule has been used successfully to enhance the performance of polymer systems using co-polymerization and blend strategies. In our investigation, we chose a high-temperature MDI Polyurethane resin foam currently used in military development projects. For the nanofiller, or “blend”, Cp7T7(OH)3 POSS was chosen. Structural characterization was accomplished by TEM and SEM to determine POSS dispersion and cell morphology, respectively. Thermal behavior was investigated by TGA. Two methods of TEM sample preparation were employed, Focused Ion Beam and Ultramicrotomy (room temperature).

Compression of Single-Crystal Micropillars of the Γ Intermetallic Phase in the Fe-Zn System

2014 ◽  
Vol 922 ◽  
pp. 264-269 ◽  
Author(s):  
Masahiro Inomoto ◽  
Norihiko L. Okamoto ◽  
Haruyuki Inui
Keyword(s):  
Single Crystal ◽  
Deformation Behavior ◽  
Room Temperature ◽  
Focused Ion Beam ◽  
Ion Beam ◽  
Intermetallic Phase ◽  
Gamma Phase ◽  
Compression Tests ◽  
Slip Direction ◽  
Beam Method

The deformation behavior of the Γ (gamma) phase in the Fe-Zn system has been investigated via room-temperature compression tests of single-crystal micropillar specimens fabricated by the focused ion beam method. Trace analysis of slip lines indicates that {110} slip occurs for the specimens investigated in the present study. Although the slip direction has not been uniquely determined, the slip direction might be <111> in consideration of the crystal structure of the Γ phase (bcc).

Nanocrystals acting as Coulomb islands operating at room temperature created using a focused ion-beam process

2001 ◽  
Vol 79 (1) ◽  
pp. 120-122 ◽  
Author(s):  
T. W. Kim ◽  
D. C. Choo ◽  
J. H. Shim ◽  
M. Jung ◽  
S. O. Kang ◽  
...  
Keyword(s):  
Room Temperature ◽  
Focused Ion Beam ◽  
Ion Beam

Characterisation of Fracture and HAC Resistance of an Individual Microstructural Constituent with Micro-Cantilever Testing

2016 ◽  
Vol 713 ◽  
pp. 66-69
Author(s):  
Walter Costin ◽  
Olivier Lavigne ◽  
Andrei G. Kotousov
Keyword(s):  
Focused Ion Beam ◽  
Ion Beam ◽  
Plastic Hinge ◽  
Crack Tip Opening Displacement ◽  
Opening Displacement ◽  
Ferrous Alloys ◽  
Microstructural Constituent ◽  
Macro Scale ◽  
Micro Cantilever ◽  
Hinge Model

This paper focuses on the application of miniaturized fracture tests to evaluate the fracture and hydrogen assisted cracking (HAC) resistance of a selected microstructural constituent (acicular ferrite, AF) which only occurs in microscopic material volumes. Site-specific Focused Ion Beam (FIB) micro-machining was used to fabricate sharply notched micro-cantilevers into a region fully constituting of AF. The micro-cantilevers were subsequently tested under uncharged and hydrogen charged conditions with a nanoindenter. The load displacement curves were recorded and analysed with a simplified plastic hinge model for the uncharged specimen, as AF demonstrated an essentially ductile behaviour. The simplified model assisted with FE simulations provided values of the critical plastic crack tip opening displacement (CTOD). A value of the conditional fracture toughness was thereby determined as 12.1 MPa m1/2. With LEFM, a threshold stress intensity factor, Kth, to initiate hydrogen crack propagation in AF was found to range between 1.56 MPa m1/2 and 4.36 MPa m1/2. All these values were significantly below the corresponding values reported for various ferrous alloys in standard macro-tests. This finding indicates that the fracture and HAC resistance at the micro-scale could be very different than at the macro-scale as not all fracture toughening mechanisms may be activated at this scale level.

A finite element model to study the effect of porosity location on the elastic modulus of a cantilever beam

2019 ◽  
Vol 43 (4) ◽  
pp. 443-453
Author(s):  
Stephen M. Handrigan ◽  
Sam Nakhla
Keyword(s):  
Finite Element ◽  
Elastic Modulus ◽  
Focused Ion Beam ◽  
Mechanical Response ◽  
Ion Beam ◽  
Three Dimensional ◽  
Beam Theory ◽  
Element Model ◽  
Fe Model ◽  
Three Dimensional Finite Element

An investigation to determine the effect of porosity concentration and location on elastic modulus is performed. Due to advancements in testing methods, the manufacturing and testing of microbeams to obtain mechanical response is possible through the use of focused ion beam technology. Meanwhile, rigorous analysis is required to enable accurate extraction of the elastic modulus from test data. First, a one-dimensional investigation with beam theory, Euler–Bernoulli and Timoshenko, was performed to estimate the modulus based on load-deflection curve. Second, a three-dimensional finite element (FE) model in Abaqus was developed to identify the effect of porosity concentration. Furthermore, the current work provided an accurate procedure to enable accurate extraction of the elastic modulus from load-deflection data. The use of macromodels such as beam theory and three-dimensional FE model enabled enhanced understanding of the effect of porosity on modulus.

scholarly journals Optimization of Pt-C Deposits by Cryo-FIBID: Substantial Growth Rate Increase and Quasi-Metallic Behaviour

Nanomaterials ◽  
2020 ◽  
Vol 10 (10) ◽  
pp. 1906 ◽  
Author(s):  
Alba Salvador-Porroche ◽  
Soraya Sangiao ◽  
Patrick Philipp ◽  
Pilar Cea ◽  
José María De Teresa
Keyword(s):  
Growth Rate ◽  
Electrical Resistivity ◽  
Room Temperature ◽  
Focused Ion Beam ◽  
Ion Irradiation ◽  
Ion Beam ◽  
Electrical Contacts ◽  
Condensation Temperature ◽  
Monte Carlo Code ◽  
Condensed Layer

The Focused Ion Beam Induced Deposition (FIBID) under cryogenic conditions (Cryo-FIBID) technique is based on obtaining a condensed layer of precursor molecules by cooling the substrate below the condensation temperature of the gaseous precursor material. This condensed layer is irradiated with ions according to a desired pattern and, subsequently, the substrate is heated above the precursor condensation temperature, revealing the deposits with the shape of the exposed pattern. In this contribution, the fast growth of Pt-C deposits by Cryo-FIBID is demonstrated. Here, we optimize various parameters of the process in order to obtain deposits with the lowest-possible electrical resistivity. Optimized ~30 nm-thick Pt-C deposits are obtained using ion irradiation area dose of 120 μC/cm2 at 30 kV. This finding represents a substantial increment in the growth rate when it is compared with deposits of the same thickness fabricated by standard FIBID at room temperature (40 times enhancement). The value of the electrical resistivity in optimized deposits (~4 × 104 µΩ cm) is suitable to perform electrical contacts to certain materials. As a proof of concept of the potential applications of this technology, a 100 µm × 100 µm pattern is carried out in only 43 s of ion exposure (area dose of 23 μC/cm2), to be compared with 2.5 h if grown by standard FIBID at room temperature. The ion trajectories and the deposit composition have been simulated using a binary-collision-approximation Monte Carlo code, providing a solid basis for the understanding of the experimental results.

3D-EBSD Studies of Deformation, Recrystallization and Phase Transformations

2012 ◽  
Vol 715-716 ◽  
pp. 41-50 ◽  
Author(s):  
Michael Ferry ◽  
Wan Qiang Xu ◽  
M. Zakaria Quadir ◽  
Nasima Afrin Zinnia ◽  
Kevin J. Laws ◽  
...  
Keyword(s):  
Focused Ion Beam ◽  
Thermomechanical Processing ◽  
Electron Backscatter Diffraction ◽  
Ion Beam ◽  
Void Formation ◽  
Data Generation ◽  
Serial Sectioning ◽  
Resolution Electron ◽  
Plastic Forming ◽  
Backscatter Diffraction

A focused ion beam (FIB) coupled with high resolution electron backscatter diffraction (EBSD) has emerged as a useful tool for generating crystallographic information in reasonably large volumes of microstructure. In principle, data generation is reasonably straightforward whereby the FIB is used as a high precision serial sectioning device for generating consecutive milled surfaces suitable for mapping by EBSD. The successive EBSD maps generated by serial sectioning are combined using various post-processing methods to generate crystallographic volumes of the microstructure. This paper provides an overview of the use of 3D-EBSD in the study of various phenomena associated with thermomechanical processing of both crystalline and semi-crystalline alloys and includes investigations on the crystallographic nature of microbands, void formation at particles, phase redistribution during plastic forming, and nucleation of recrystallization within various regions of the deformation microstructure.

Compression of Micro-pillars of a Long Period Stacking Ordered Phase in the Mg-Zn-Y system

2013 ◽  
Vol 1516 ◽  
pp. 151-156 ◽  
Author(s):  
Atsushi Inoue ◽  
Kyosuke Kishida ◽  
Haruyuki Inui ◽  
Koji Hagihara
Keyword(s):  
Basal Plane ◽  
Focused Ion Beam ◽  
Ion Beam ◽  
Deformation Bands ◽  
Axis Orientation ◽  
Lpso Phase ◽  
Long Period ◽  
Image Position ◽  
Micro Pillars ◽  
Loading Axis

ABSTRACTDeformation behavior of an 18R-type long period stacking ordered (LPSO) phase in the Mg-Zn-Y system was studied by micro-pillar compressions of single crystalline specimens prepared by focused ion beam (FIB) technique as a function of loading axis orientation and specimen dimensions. When the loading axis is inclined to the basal plane of the LPSO phase by 42°, basal slip of (0001)<11$\bar 2$0>-type is activated irrespective of the specimen dimensions. When the loading axis is parallel to the basal plane, the formation of thick deformation bands are observed for all specimens tested. Strong size-dependence of yield stress values is observed for both types of micro-pillar specimens with different loading axis orientations.

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