Effective, Shortened Drying of Agar-Gelcasting Al2O3 Tube Through Immersing in Acetone

Author(s):  
Ramnaree Kaemkit ◽  
Supawan Vichaphund ◽  
Anukorn Phureungrat ◽  
Methee Promsawat ◽  
Suksawat Sirijarukul ◽  
...  

Abstract A liquid drying agent, i.e. acetone, was employed for allowing the faster drying of Al2O3 tubes fabricated by agar gelcasting than the conventional air drying. The mixture of Al2O3 slurry and agar solution was separately prepared and then mixed prior to molding out of a set of warmed glass tubes. After the mixture transformed into gelled tube, the gelled tube was demolded and then immersed in acetone at different periods of time from 0 to 50 h. The immersed periods of 50 h led to the acetone replacement for water being inside of the gelling tube by 74 wt.% and then shortened the drying period to be 25 min. On the other hand, the conventional air drying spent 420 min drying completely. After drying, the immersed tubes possessed spherical cross section; whereas, no immersed tubes showed the deformation of cross section. The shortened drying was in line with the smaller drying shrinkage (4.7%), broader pore-size distribution and higher porous microstructure, comparing to the conventional air drying. The mechanism of acetone replacement for water was attributed to the acetone-water concentration gradient creating their inter-diffusion.

Author(s):  
V. Mizuhira ◽  
Y. Futaesaku

Previously we reported that tannic acid is a very effective fixative for proteins including polypeptides. Especially, in the cross section of microtubules, thirteen submits in A-tubule and eleven in B-tubule could be observed very clearly. An elastic fiber could be demonstrated very clearly, as an electron opaque, homogeneous fiber. However, tannic acid did not penetrate into the deep portion of the tissue-block. So we tried Catechin. This shows almost the same chemical natures as that of proteins, as tannic acid. Moreover, we thought that catechin should have two active-reaction sites, one is phenol,and the other is catechole. Catechole site should react with osmium, to make Os- black. Phenol-site should react with peroxidase existing perhydroxide.


Author(s):  
J. P. Colson ◽  
D. H. Reneker

Polyoxymethylene (POM) crystals grow inside trioxane crystals which have been irradiated and heated to a temperature slightly below their melting point. Figure 1 shows a low magnification electron micrograph of a group of such POM crystals. Detailed examination at higher magnification showed that three distinct types of POM crystals grew in a typical sample. The three types of POM crystals were distinguished by the direction that the polymer chain axis in each crystal made with respect to the threefold axis of the trioxane crystal. These polyoxymethylene crystals were described previously.At low magnifications the three types of polymer crystals appeared as slender rods. One type had a hexagonal cross section and the other two types had rectangular cross sections, that is, they were ribbonlike.


2021 ◽  
Vol 11 (3) ◽  
pp. 1037
Author(s):  
Se-Jin Choi ◽  
Ji-Hwan Kim ◽  
Sung-Ho Bae ◽  
Tae-Gue Oh

In recent years, efforts to reduce greenhouse gas emissions have continued worldwide. In the construction industry, a large amount of CO2 is generated during the production of Portland cement, and various studies are being conducted to reduce the amount of cement and enable the use of cement substitutes. Ferronickel slag is a by-product generated by melting materials such as nickel ore and bituminous coal, which are used as raw materials to produce ferronickel at high temperatures. In this study, we investigated the fluidity, microhydration heat, compressive strength, drying shrinkage, and carbonation characteristics of a ternary cement mortar including ferronickel-slag powder and fly ash. According to the test results, the microhydration heat of the FA20FN00 sample was slightly higher than that of the FA00FN20 sample. The 28-day compressive strength of the FA20FN00 mix was approximately 39.6 MPa, which was higher than that of the other samples, whereas the compressive strength of the FA05FN15 mix including 15% of ferronickel-slag powder was approximately 11.6% lower than that of the FA20FN00 mix. The drying shrinkage of the FA20FN00 sample without ferronickel-slag powder was the highest after 56 days, whereas the FA00FN20 sample without fly ash showed the lowest shrinkage compared to the other mixes.


1993 ◽  
Vol 310 ◽  
Author(s):  
L.A. Wills ◽  
B.W. Wessels

AbstractThe defect structure of BaTiO3 thin films grown on (100) Si was examined using transient photocapacitance spectroscopy. The concentration, optical cross section and associated energy levels of both native and impurity defects in as-grown and annealed BaTiO3 films were evaluated. Deep level defects withpeak energies of Ev+1.8, Ev+2.4, Ev+2.7, Ev+3.0-3.1 and Ev+3.2-3.3 eV were observed in the as-grown films. Upon vacuum annealing, the concentration of the traps at Ev+3.0 and Ev+3.2 eV increased while the concentration of the traps at Ev+ 1.8 and Ev+2.4 eV decreased. The levels at Ev+3.0-3.1 and Ev+3.2-3.3 eV are attributed to oxygen vacancies. The other levels are tentatively ascribed to Fe and Fe related defects.


2011 ◽  
Vol 1 (1) ◽  
Author(s):  
Kim Frail

Siminovich, Lorena. I Like Vegetables: A Touch-and-Feel Board Book. Somerville: Candlewick Press, 2011. Print.“I Like Vegetables” is a dream come true for any nutritionally conscience parent, children’s librarian or teacher. The brightly hued collage illustrations are intriguingly textured with patterns and “touch & feel” inlays. Silky peas and rough-skinned carrots invite young readers to learn about vegetables. The layout is quite clever as it leverages contrast and comparison as a learning method. On one side of the page vegetables are depicted as they would appear growing in the garden while on the other side they are in the home being prepared for the dinner table. In addition, the nature side of the page illustrates the concept of opposites. For example, there are “tall” and “short” cornstalks. Orange carrot roots are “below” the ground, while the feathery green tops are “above”. The indoor side of the page features close-ups of vegetables against a wood-grain background that evokes a cutting board. Here children get a different perspective on the harvested veggies. We see shelled peas, open cornhusks and a cross-section of a pumpkin. The concluding series of images features an “empty” gardener’s basket next to a basket “full” of colourful vegetables on a blue and white gingham picnic tablecloth inlay.  This is primarily a picture book with only the names of the vegetables and the two opposing concepts appearing on each page. The typeset is Helvetica and is large and easy to read.  It is a sturdy board book and the inlays could not be easily ripped out or damaged. It is therefore a welcome addition to any toddler’s library. Other titles in the “I Like” series by Siminovich include: “I Like Toys “, “I Like Bugs” and “I Like Fruit”. “I Like Vegetables” is sure to engage children from ages 1-3. Highly recommended: 4 out of 4 stars Reviewer: Kim FrailKim is a Public Services Librarian at the H.T. Coutts Education Library at the University of Alberta. Children’s literature is a big part of her world at work and at home. She also enjoys gardening, renovating and keeping up with her two-year old. 


BioResources ◽  
2020 ◽  
Vol 15 (3) ◽  
pp. 6149-6164
Author(s):  
Alan Dickson ◽  
Bernard Dawson

An approach combining maps of wood morphology and digital image correlation was developed to investigate the drying of Eucalyptus nitens wood. Maps of morphological features (vessel and ray distribution) and cell cross-section dimensions were acquired by confocal laser scanning microscopy. Shrinkage maps were generated using digital image correlation. There were statistically significant correlations between shrinkage/collapse and wood morphology at two levels. Firstly, there were positional relationships, with for example, both radial and tangential shrinkage increasing with increasing distance from vessel elements. Secondly, there were dimensional relationships, such as, cells with large perimeters (relative to their wall thickness) on average showing greater shrinkage. Generally, the positional relationships dominated the dimensional relationships. Detailed analysis over large areas allows for a fuller analysis of the interrelationship between wood morphology and drying shrinkage and collapse.


1962 ◽  
Vol 14 (2) ◽  
pp. 193-205 ◽  
Author(s):  
Toshio Nagano

The kinetic apparatus, the acrosome and associated structures, and the manchette of the spermatid of the domestic chicken have been studied with the electron microscope. The basic structural features of the two centrioles do not change during spermiogenesis, but there is a change in orientation and length. The proximal centriole is situated in a groove at the edge of the nucleus and oriented normal to the long axis of the nucleus and at right angles to the elongate distal centriole. The tail filaments appear to originate from the distal centriole. The plasma membrane is invaginated along the tail filaments. A dense structure which appears at the deep reflection of the plasma membrane is identified as the ring. The fine structure of the ring has no resemblance to that of a centriole and there is no evidence that it is derived from or related to the centrioles. The tail of the spermatid contains nine peripheral pairs and one central pair of tubular filaments. The two members of each pair of peripheral filaments differ in density and in shape: one is dense and circular, and the other is light and semilunar in cross-section. The dense filaments have processes. A manchette consisting of fine tubules appears in the cytoplasm of the older spermatid along the nucleus, neck region, and proximal segment of the tail. The acrosome is spherical in young spermatids and becomes crescentic and, finally, U-shaped as spermiogenesis proceeds. A dense granule is observed in the cytoplasm between acrosome and nucleus. This granule later becomes a dense rod which is interpreted as the perforatorium.


2001 ◽  
Vol 9 (4) ◽  
pp. 17-17
Author(s):  
Ron Doole

Section thickness can be measured by placing beads of some kind on the top and bottom surfaces of the section. This is then a simple parallax problem.Imagine the specimen in cross section. If there are two particles, one vertically above the other they are separated by the film thickness T. Tilt the film through an angle A and in plan view the particles will separate by a distance D. This can also be extended to account for two particles not vertically above each other but I'll stick to the easy case for the explanation.Take two negatives one at zero tilt and one at tilt of A and measure the separation D. The thickness can be calculated by T=D/sinA.The direction of the tilt axis must be known for the measurements and it is easy to see that the larger the tiit angle and the more accurately the separation is measured, the more accurate the measurement will be. Tilt at both positive and negative angles to get a more accurate result.


2013 ◽  
Vol 572 ◽  
pp. 257-260
Author(s):  
Markus Straub ◽  
Shu Jun Zhang ◽  
Carsten Manz ◽  
Kevin Hapeshi

Purpose: This paper shows the effects of using Minomi on the provision of long items in the plant area. In details it will be evaluated if the Minomi principle is usable for the provision of long item material at the manufacturing area and what improvements can be achieved. Definitions of the term Minomi and the term long item: The term long item is used in the logistic sector for all materials that are longer than 2.5 meters, require individually packing and have a relatively small cross section [1,2]. The term Minomi has not been clearly defined. In practise, the term Minomi is often associated with a system that does not use boxes for the material provision [3]. Findings: Through the case studies, it has been found that additional advantages can be obtained by using Minomi for the provision of long items than the other existing methods.


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