scholarly journals Effect of Minocycline on the Durability of Dentin Bonding Produced with Etch-and-Rinse Adhesives

2016 ◽  
Vol 41 (5) ◽  
pp. 511-519 ◽  
Author(s):  
AD Loguercio ◽  
R Stanislawczuk ◽  
P Malaquias ◽  
MF Gutierrez ◽  
J Bauer ◽  
...  
Keyword(s):  
Nitrate Solution ◽  
Water Storage ◽  
Silver Nitrate Solution ◽  
Control Group ◽  
Single Bond ◽  
Water Control ◽  
X Ray ◽  
Etch And Rinse ◽  
Group 2 ◽  
Scanning Electron

SUMMARY Objectives: To evaluate the effect of minocycline and chlorhexidine pretreatment of acid-etched dentin on the longevity of resin-dentin bond strength (μTBS) and nanoleakage of two-step etch-and-rinse adhesives. Methods: Before application of Prime & Bond NT and Adper Single Bond 2 in occlusal dentin, the dentin surfaces were treated with 37% phosphoric acid, rinsed, air-dried, and rewetted with water (control group), 2% minocycline, or 2% chlorexidine digluconate. Composite buildups were constructed incrementally, and specimens were longitudinally sectioned to obtain bonded sticks (0.8 mm2) to be tested in tension (0.5 mm/min) immediately or after 24 months of water storage. For nanoleakage, two specimens of each tooth/period were immersed in the silver nitrate solution, photo-developed, and polished with SiC paper for analysis under energy-dispersive X-ray spectroscopy/scanning electron microscopy. Results: Reductions of the μTBS and increases in the nanoleakage were observed for both adhesives when the rewetting procedure was performed with water. Stable bonds were observed for the 2% minocycline and 2% chlorexidine digluconate groups after 24 months. Conclusions: The use of 2% minocycline as pretreatment of acid-etched dentin is one alternative to retard the degradation of resin-dentin interfaces over a 24-month period as well as 2% chlorexidine digluconate.

Three-Year Effects of Deproteinization on the In Vitro Durability of Resin/Dentin-Eroded Interfaces

2018 ◽  
Vol 43 (1) ◽  
pp. 60-70 ◽  
Author(s):  
FSF Siqueira ◽  
AFM Cardenas ◽  
GM Gomes ◽  
AC Chibinski ◽  
OMM Gomes ◽  
...  
Keyword(s):  
Nitrate Solution ◽  
Water Storage ◽  
Silver Nitrate Solution ◽  
Smear Layer ◽  
Dentin Surface ◽  
Etch And Rinse ◽  
Bonding Properties ◽  
Self Etch ◽  
Scanning Electron

SUMMARY Objective: To evaluate the effect of sodium hypochlorite on the immediate and three-year bonding properties of a resin-eroded dentin interface produced by one of two adhesive strategies. Methods and Materials: Forty-eight molars were randomly assigned to six experimental groups, according to the combination of the adhesive strategy (etch-and-rinse and self-etch) and the dentin surface (control groups without erosion, eroded dentin surface [ED], and eroded dentin surface + NaOCl 5.2% [ED + NaOCl]). After completing restoration, specimens were stored in water (37°C) for 24 hours and then sectioned into resin–dentin beams (0.8 mm2) to be tested under tension (0.5 mm/min) immediately thereafter or after three years of water storage. To assess nanoleakage (NL), specimens were immersed in silver nitrate solution and examined by scanning electron microscopy at both time points. The dentin-etching pattern was examined under a scanning electron microscope. Data were subjected to appropriate statistical analysis (α=0.05) Results: In both strategies, a more pronounced and significant reduction of the microtensile bond strength (μTBS) values was observed for the ED groups (p=0.0001) after three years. However, in the ED + NaOCl group, μTBS values were maintained after three years of water storage. Furthermore, application of NaOCl to eroded dentin significantly reduced the immediate NL values and also preserved these values after three years of water storage for both adhesive strategies (p>0.05). When considering the ED group, a superficial removal of the smear layer and enlarged lumen tubules in comparison to control were present. However, for ED + NaOCl, there was a total removal of the smear layer and significant numbers of collagen fibrils were exposed. Conclusion: The use of NaOCl may maintain the long-term stability of a resin-eroded dentin interface formed by etch-and-rinse and self-etch adhesives.

scholarly journals Permeability of Dental Adhesives – A SEM Assessment

2010 ◽  
Vol 04 (04) ◽  
pp. 429-439 ◽  
Author(s):  
Juliana Malacarne-Zanon ◽  
Safira M. de Andrade e Silva ◽  
Linda Wang ◽  
Mario F. de Goes ◽  
Adriano Luis Martins ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Nitrate Solution ◽  
Silver Nitrate Solution ◽  
Single Step ◽  
Dental Adhesives ◽  
Backscattered Electrons ◽  
Etch And Rinse ◽  
Carbon Coated ◽  
Scanning Electron

Objectives: To morphologically evaluate the permeability of different commercial dental adhesives using scanning electron microscopy.Methods: Seven adhesive systems were evaluated: one three-step system (Scotchbond Multi- Purpose - MP); one two-step self-etching primer system (Clearfil SE Bond – SE); three two-step etch-and-rinse systems (Single Bond 2 – SB; Excite – EX; One-Step – OS); and two single-step selfetching adhesives (Adper Prompt – AP; One-Up Bond F – OU). The mixture of primer and bond agents of the Clearfil SE Bond system (SE-PB) was also tested. The adhesives were poured into a brass mold (5.8 mm x 0.8 mm) and light-cured for 80 s at 650 mW/cm2. After a 24 h desiccation process, the specimens were immersed in a 50% ammoniac silver nitrate solution for tracer permeation. Afterwards, they were sectioned in ultra-fine slices, carbon-coated, and analyzed under backscattered electrons in a scanning electron microscopy.Results: MP and SE showed slight and superficial tracer permeation. In EX, SB, and OS, permeation extended beyond the inner superficies of the specimens. SE-PB did not mix well, and most of the tracer was precipitated into the primer agent. In AP and OU, “water-trees” were observed all over the specimens.Conclusions: Different materials showed distinct permeability in aqueous solution. The extent of tracer permeation varied according to the composition of each material and it was more evident in the more hydrophilic and solvated ones. (Eur J Dent 2010;4:429-439)

scholarly journals The New Complexes of Tris(2-Methoxy-5-Bromophenyl)Stibine with Silver Nitrate

2021 ◽  
Vol 13 (1) ◽  
pp. 21-30
Author(s):  
O.K. Sharutina ◽  
Keyword(s):  
Diffraction Analysis ◽  
Silver Nitrate ◽  
Silver Atom ◽  
Nitrate Solution ◽  
Silver Nitrate Solution ◽  
X Ray Diffraction ◽  
Space Group ◽  
X Ray ◽  
Crystallographic Characteristics ◽  
Group A

By mixing solutions of tris(2-methoxy-5-bromophenyl)antimony and silver nitrate in a methanol : acetonitrile mixture (1:1 vol.), nitrato-O,O'-(acetonitrile)[tris(2-methoxy-5-bromophenyl)antimony]silver complex with the general formula [(C6H3ОMe-2-Br-5)3SbAg(μ2-NO3)(Ме3CN)]2•2[(C6H3ОMe-2-Br-5)3SbAgNO3(Ме3CN)] (1) has been obtained. An addition of silver nitrate solution in the methanol : acetonitrile mixture to the tris(2-methoxy-5-bromophenyl)antimony dioxane solution has led to the formation of a small amount of dark crystals of the ionic complex [(2-MeО-5-Br-C6H3)3SbAg(H2O)Sb(C6H3Br-5-OMe-2)3]+[(2-MeО-5-Br-C6H3)3SbAg(m-NO3)3 AgSb(C6H3Br-5-OMe-2)3]-×3C4H8O2 (2). Complexes 1 and 2 have been characterized by IR spectroscopy, and their structures have been determined by X-ray diffraction analysis. The IR spectra of complexes 1 and 2 contain the bands characterizing the Sb-O, Sb-C, С≡N-, and NO3-group band vibrations. X-ray diffraction analysis of the complexes has been carried out on an automatic four-circle D8 Quest Bruker diffractometer (МоКα radiation, λ = 0.71073 Å, graphite monochromator) at 293 K. Crystallographic characteristics of 1: triclinic, P-1 space group, a = 9.32(3), b = 17.50(7), c = 17.97(5) Å, a = 97.56(14), β = 92.90(19), g = 99.45(19) grad., V = 2859(16) Å3, Z = 2, rcalc = 2.069 g/cm3, 2: monoclinic, С2/с space group, a = 17.417(14), b = 21.041(15), c = 32.01(2) Å, a = 90, β = 97.79(3), g = 90 grad., V = 11624(15) Å3, Z = 4, rcalc = 2.006 g/cm3. In the monomeric and dimeric molecules of crystal 1, nitrate ligands are chelating and bridging, respectively. In the cation of complex 2, the silver atom is bonded to two antimony ligands, the third coordination site is occupied by a water molecule. In the dimeric anion there are one antimony ligand and three bridging nitrate groups surrounding each silver atom.

scholarly journals Effect of Proteolytic Agents on Microleakage of Etch and Rinse Adhesive Systems

2017 ◽  
Vol 16 ◽  
pp. 1-11
Author(s):  
Shahin Kasraei ◽  
Ebrahim Yarmohammadi ◽  
Maryam Farhadian ◽  
Mona Malek
Keyword(s):  
Phosphoric Acid ◽  
Nd:Yag Laser ◽  
Control Group ◽  
Single Bond ◽  
Adhesive Systems ◽  
Class V ◽  
Dentin Surface ◽  
Composite Restorations ◽  
Etch And Rinse ◽  
Significant Difference

Objective: this study aimed to assess the effect of treatment of phosphoric acid etched dentin surface with 5% bromelain enzyme and Nd:YAG laser prior to the use of etch and rinse adhesive systems on microleakage margins of class V composite restorations. Materials and Methods: sixty sound premolar teeth were selected. Standard class V cavities were prepared in the buccal and lingual surfaces of each teeth. Preparation in that way 1 mm of the cavity was above and 1 mm of it was below the cementoenamel junction. The teeth were then randomly divided into three groups including 20 teeth(40cavities  in each gorup). Two ethanol base etch and rinse system (Adper Single Bond and OptiBond Solo) was applied in each group. In the control group, cavities were etched with 37% phosphoric acid. Adper Single Bond was applied to 20 and OptiBond Solo was applied to the remaining 20 cavities and they were restored with Z250 composite (n=40). The same procedures were performed in bromelain and Nd:YAG laser groups with the difference that prior to the application of adhesive, aqueous 5% bromelain was applied in bromelain group while Nd:YAG laser was irradiated in laser group. All teeth were thermocycled and their apices were sealed with sticky wax. The tooth surfaces were coated with nail varnish except for 1 mm around the restoration margins, and the teeth were then immersed in fuchsine and sectioned by a diamond disc into mesial and distal halves. Marginal microleakage at both sides was determined and scored under a stereomicroscope at x40 magnification. Then data were analyzed using the Kruskal Wallis and Mann Whitney tests (α=0.05). Results: according the result of Mann Whitney test, Cervical margins showed significantly higher microleakage than the occlusal margins (P=0.000) but no significant difference was noted in microleakage of occlusal (P=0.362) or gingival (P=0.147) margins among the three groups by Kruskal Wallis test. Conclusion: in conclusion, application of proteolytic agents(5% bromelain solution and Nd:YAG laser)  on acid-etched dentin surface prior to the application of adhesive has no significant effect on marginal microleakage of class V composite restorations. 

Pretreated Lignocellulosic Waste Mediated Biosynthesis of Silver Nanoparticles Under Room Temperature

2016 ◽  
Vol 15 (05n06) ◽  
pp. 1660001 ◽  
Author(s):  
V. P. Manjamadha ◽  
Karuppan Muthukumar
Keyword(s):  
Silver Nanoparticles ◽  
Silver Nitrate ◽  
Room Temperature ◽  
Nitrate Solution ◽  
Silver Ions ◽  
Silver Nitrate Solution ◽  
Morphological Characterization ◽  
Alternative Source ◽  
X Ray ◽  
Antibacterial Performance

The current work elucidates the utilization of biowaste as a valuable reducing agent for the synthesis of silver nanoparticles. In this study, the wastewater generated during the alkaline pretreatment of lignocellulosic wastes (APLW) was used as a bioreductant to reduce silver nitrate under room temperature. Synthesis of stable silver nanoparticles (AgNPs) was achieved rapidly on addition of APLW into the silver nitrate solution (1[Formula: see text]mM). The morphological characterization of AgNPs was performed using field emission scanning electron microscopy (FESEM). The micrograph clearly depicted the presence of spherical AgNPs. The presence of elemental silver along with biomoilties was determined using energy dispersive X-ray spectroscopy (EDAX) analysis. The X-ray diffraction (XRD) study proved the crystalline form of stable AgNPs. The AgNPs exhibited excellent antibacterial performance against Gram negative organism. The immediate bioreduction of silver ions using APLW was well illustrated in the present study. Thus, APLW serve as an alternative source for reducing agents instead of utilizing valuable medicinal plants for nanoparticles synthesis.

scholarly journals PMMA Intraocular Lenses Changes after Treatment with Nd:Yag Laser: A Scanning Electron Microscopy and X-ray Spectrometry Study

2020 ◽  
Vol 10 (18) ◽  
pp. 6321
Author(s):  
Alessandro Meduri ◽  
Alice Antonella Severo ◽  
Antonio De Maria ◽  
Pietro Perroni ◽  
Giuseppe Acri ◽  
...  
Keyword(s):  
Nd:Yag Laser ◽  
Surface Group ◽  
Intraocular Lenses ◽  
X Ray ◽  
Wrinkled Surface ◽  
Group 3 ◽  
Group 2 ◽  
Normal Shape ◽  
Scanning Electron ◽  
Group 1

Neodymium:yttrium-aluminum-garnet (Nd:YAG) laser may cause intraocular lenses (IOLs) damages. Therefore, the effects of Nd:YAG laser on IOLs were evaluated. Twenty-four IOLs (copolymer of 2-hydroxyethylmethacrylate and 2-ethoxyethylmethacrylate) were used. For scanning electron microscope (SEM), twelve IOLs were divided into three groups: Group 1, controls; Group 2, IOLs treated with two laser spots (YC-1800 Nidek Nd:YAG laser set at 1.2 mJ); and Group 3, IOLs treated with six laser spots. All IOLs were critical point dried in CO2 and viewed in a Zeiss EVO LS10 SEM. For Energy Dispersive X-ray spectrometry (EDX), four IOLs of each group were examined with a Jeol JMC-6000 SEM. With SEM, Group 1 IOLs showed well-preserved size, shape and surface. Group 2 IOLs exhibited normal shape and margins, a peripheral furrow with irregular blebs, straight clefts and holes on the wrinkled surface. Group 3 IOLs were swollen and broken into two or three parts. With SEM and EDX, Group 1 and the undamaged surfaces of Groups 2 and 3 showed evident carbon and oxygen peaks, while, in the damaged areas, both atoms were significantly reduced. Nd:YAG laser induced evident changes in IOLs morphology and organic alterations in their chemistry: great care during posterior capsule opacification treatment is required.

scholarly journals KOMBINASI PENAMBAHAN SHIELDING TIMBAL MESIN FLUOROSCOPY BAGASI DAN PENGATURAN JARAK PEKERJA TERHADAP SUMBER RADIASI MENURUNKAN PAPARAN RADIASI SINAR X DAN KELELAHAN MATA PADA PEKERJA SCREENING DI BANDARA INTERNASIONAL X

2018 ◽  
Vol 4 (1) ◽  
Author(s):  
Maghfirotul Iffah ◽  
I Putu Gede Adiatmika ◽  
I Wayan Bandem Adnyana ◽  
I Dewa Putu Sutjana ◽  
I Made Muliarta ◽  
...  
Keyword(s):  
Radiation Exposure ◽  
Radiation Source ◽  
Additional Treatment ◽  
Control Group ◽  
Control Group Design ◽  
X Ray ◽  
Post Test ◽  
Lead Shielding ◽  
Group 2 ◽  
Working Distance

Screening is ordinary process airport passanger was machine baggage. X-ray radiation gives impact to eye because eye sensitive of radiation. Many kinds of eye strain symptom got by screening worker such eye poignant. It is neressary to give  intervention to decrease the radiation exposure and eye strain for worker by increasing lead shielding on the fluoroscopy machine baggage and setting of worker distance toward the source of radiation.             Experimental research with pre-post test control group design. A sampel of 30 people were taken with a simple randomized method which was subdivided into group 1 as a control group without the additional treatment of lead shielding and working distance regulation of the radiation source, group 2 with the addition of a shielding and setting distance as far as 2 m. the study was conducted in August 2017. The variables evaluated were exposure to the received radiation of workes and the strain of the workers eyes.             The result of the research is a combination of  lead shielding on machine baggage fluoroscopy and setting of working distance to X ray source at X International Ariport significantly (p<0,05) in decreasing radiation exposure received by worker equal to 74,59% and worker eye strain 68,85% for a distance of 1,5 m and decreased radiation exposure to the workers as much as 93, 69% and the eye strain on the worker 89,79% at a distance of 2 m from the radiation source.             Concluded that the combination of increasing lead shielding and the setting of worker distance toward the source of radiation decrease thr radiation exposure and eye strain on the screening worker at X International airport.

scholarly journals REMINERALIZATION EFFECT OF POLYASPARTIC ACID IN THE POLYMER-INDUCED LIQUID PRECURSOR PROCESS ON THE INTRAFIBRILLAR DENTIN (SCANNING ELECTRON MICROSCOPE AND ENERGY DISPERSIVE X-RAY ANALYSIS)

2020 ◽  
pp. 45-48
Author(s):  
RIVANTI IRMADELA DEVINA ◽  
ADELINE CLARISSA ◽  
NILAKESUMA DJAUHARIE ◽  
KAMIZAR NAZAR ◽  
RATNA MEIDYAWATI
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Energy Dispersive ◽  
Control Group ◽  
Polyaspartic Acid ◽  
Liquid Precursor ◽  
X Ray ◽  
Demineralized Dentin ◽  
Scanning Electron

Objective: This study aims to analyze remineralization that occurred in demineralized dentin following polyaspartic acid (pAsp) in PILP immersion.Methods: Sixteen dentin block samples were immersed in demineralized solution. The samples were divided into controls (no pAsp immersion) orpAsp immersion for 3, 7, or 14 days (n’s=4). The samples were evaluated using a scanning electron microscope (SEM) to observe morphology andenergy-dispersive X-ray (EDX) to observe calcium and phosphate levels.Results: SEM revealed that pAsp immersion resulted in significantly higher dentin remineralization compared to the control group. However, therewere no significant differences among 3, 7, and 14 days of immersion. EDX revealed that remineralization occurred by the deposition of calcium andphosphate ions.Conclusion: Including pAsp in the PILP process produced rapid remineralization of demineralized dentin.

scholarly journals Degradation of Methylene Blue Using Biologically Synthesized Silver Nanoparticles

2014 ◽  
Vol 2014 ◽  
pp. 1-8 ◽  
Author(s):  
M. Vanaja ◽  
K. Paulkumar ◽  
M. Baburaja ◽  
S. Rajeshkumar ◽  
G. Gnanajobitha ◽  
...  
Keyword(s):  
Methylene Blue ◽  
Silver Nanoparticles ◽  
Leaf Extract ◽  
Nitrate Solution ◽  
Reaction Medium ◽  
Silver Ions ◽  
Silver Nitrate Solution ◽  
X Ray ◽  
Synthesis Of Nanoparticles ◽  
Aqueous Leaf Extract

Nowadays plant mediated synthesis of nanoparticles has great interest and achievement due to its eco-benign and low time consuming properties. In this study silver nanoparticles were successfully synthesized by usingMorinda tinctorialeaf extract under different pH. The aqueous leaf extract was added to silver nitrate solution; the color of the reaction medium was changed from pale yellow to brown and that indicates reduction of silver ions to silver nanoparticles. Thus synthesized silver nanoparticles were characterized by UV-Vis spectrophotometer. Dispersity and morphology was characterized by scanning electron microscope (SEM); crystalline nature and purity of synthesized silver nanoparticles were revealed by X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDX). FTIR spectrum was examined to identify the effective functional molecules responsible for the reduction and stabilization of silver nanoparticles synthesized by leaf extract. The photocatalytic activity of the synthesized silver nanoparticles was examined by degradation of methylene blue under sunlight irradiation. Green synthesized silver nanoparticles were effectively degrading the dye nearly 95% at 72 h of exposure time.

scholarly journals Permeability of Modified Dentinal Surfaces

2021 ◽  
Vol 11 (4) ◽  
pp. 272-287
Author(s):  
Manar M Abu Nawareg ◽  
Ola I Fahmy ◽  
Gihan A Abdel Rahman
Keyword(s):  
Fluid Transport ◽  
Control Group ◽  
Single Bond ◽  
Control Groups ◽  
Surface Pretreatment ◽  
Dentin Permeability ◽  
Etch And Rinse ◽  
One Step ◽  
Self Etch ◽  
Long Storage

Objectives: The aim of this study was to investigate the sealing ability of three adhesives bonded to modified dentinal surfaces after short and long storage periods. Methods: Three adhesives were used in this study; two-step etch-and-rinse “Adper Single Bond 2”, two-step self-etch “AdheSE” and one-step self-etch “G-Bond” adhesives. Modifications of the dentinal surface was performed by application of adhesives after oxalate application, application of adhesive after oxalate application to sodium hypochlorite (NaOCl)-deproteinized dentinal surface, compared to control groups (application of adhesive without any surface pretreatment). Dentinal sealing was investigated by measuring dentin permeability, using a fluid transport apparatus, after two storage periods; 24 hours and 2 months. Results: After 24 hours, the control group bonded with “Adper Single Bond 2” without any surface treatment had the highest permeability (25.3%) followed by “G-Bond” (16.2%) and finally “AdheSE” (11%). Significant reductions in permeability values were observed on application of oxalate in conjunction with both “Adper Single Bond 2” and “AdheSE” (11.7% and 2.6% respectively). Further significant reductions in permeability values of those two adhesives were noted when the combined NaOCl and oxalate pretreatments were used (5.7% and 0.8% respectively). Permeability means for all groups increased after storage for 2 months. Conclusions: Dentin surface deproteinization plus oxalate application produced the best dentin sealing for two step adhesives. Key words: Etch-and-rinse adhesives, self-etching adhesives, oxalate-desensitizing agent, NaOCl-deproteinizing agent, dentin permeability.

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