scholarly journals CHARACTERIZATION OF CARBOXYMETHYL CELLULOSE (CMC) FROM PALM MIDRIB

2018 ◽  
Vol 8 (1) ◽  
pp. 53-61
Author(s):  
Devi Silsia ◽  
Zulman Efendi ◽  
Febri Timotius
Keyword(s):  
Reaction Time ◽  
Water Content ◽  
Carboxymethyl Cellulose ◽  
Reaction Times ◽  
Cellulose Content ◽  
Randomized Design ◽  
Substitution Degree ◽  
Two Factors ◽  
Three Stages

Midrib is one of the palm plantation  waste that has not been utilized optimally. The high cellulose content of palm midrib is potentially converted to carboxymethyl cellulose. This study aims to determine the characteristics of carboxymethyl cellulose that produced from various concentrations of trichloroacetic acid and reaction times. This study used a complete randomized design (RAL) with two factors i.e tricloroacetic acid concentration (10%, 20% and 30%) and reaction time (3 hours and 4 hours). The synthesis of carboxymethyl cellulose in this study consists of three stages i.e alkalization, carboxymethylation and purification. The carboxymethyl cellulose obtained was characterized include degree of subsitution (DS), pH, viscosity, water content, and purity. The results showed that the best carboxymethyl cellulose was obtained from the use of 20% tricloroacetic acid and 3 hours reaction time. The characterrization result include substitution degree value of 0.76, pH of 8.32, water content of 7.1%, with a  viscosity of 7.8 cP,   and purity of 92.62%. 

scholarly journals Pemanfaatan Selulosa dari Rumput Gajah (Pennisetum purpureum) pada Sintesis Karboksimetil Selulosa (CMC)

KOVALEN ◽  
2021 ◽  
Vol 7 (2) ◽  
pp. 146-153
Author(s):  
Erwin Abdul Rahim ◽  
Grace Sita Turumi ◽  
Syaiful Bahri ◽  
Jusman ◽  
Syamsuddin
Keyword(s):  
Reaction Time ◽  
Carboxymethyl Cellulose ◽  
Trichloroacetic Acid ◽  
Pennisetum Purpureum ◽  
Main Ingredient ◽  
Independent Variables ◽  
Randomized Design ◽  
Substitution Degree ◽  
Completely Randomized Design ◽  
Two Independent Variables

Cellulose from Pennisetum purpureum has been used as the main ingredient in the synthesis of carboxymethyl cellulose (CMC). The purpose of CMC synthesis from the cellulose of Pennisetum purpureum is to obtain CMC compounds with the best degree of substitution (DS) value and the highest yield. The study was conducted using a completely randomized design with a factorial pattern consisting of two independent variables, namely the concentration of trichloroacetic acid (10%, 20%, and 30%) and reaction time (3 and 4 hours). The results showed that the CMC with the highest DS value (0.839) was obtained using 20% trichloroacetic acid with a reaction time of 3 hours. The highest CMC yield was 30.15% which was obtained using 30% trichloroacetic acid with a reaction time of 4 hours. Keywords: Pennisetum purpureum, carboxymethyl cellulose, substitution degree.

scholarly journals Karakteristik Fisik, Kimia, dan Fungsional Pati Ubi Banggai Asetat pada Berbagai Variasi Waktu Reaksi

2021 ◽  
Vol 40 (4) ◽  
pp. 340
Author(s):  
If'all If'all ◽  
Asriani Hasanuddin ◽  
Abdul Rahim ◽  
Syahraeni Kadir
Keyword(s):  
Reaction Time ◽  
Treatment Time ◽  
Reaction Times ◽  
Degree Of Substitution ◽  
Raw Material ◽  
Physical Chemical ◽  
Randomized Design ◽  
Substitution Degree ◽  
Completely Randomized Design ◽  
The One

Banggai yam plant (endemic in Banggai Kepulauan Regency) is a potential raw material in production of modified starch. The one of techniques to increase the value of starch is modification of starch by acetylation method. This study objectives to determine the physical, chemical and functional characteristics of Banggai acetate yam starch at various reaction times. The study used a Completely Randomized Design with treatment time reaction (T), namely T1: 30 min, T2: 35 min, T3: 40 min, T4: 45 min, T5: 50 min, T6: 55 min. This study was conducted to determine the characteristics of yam acetate starch, which includes percent acetyl, degree of substitution, water and oil holding capacity (WHC/OHC), flammability, solubility, moisture content, ash, fat, protein, starch and amylose starch. The results showed that the longer reaction time under certain conditions will increase the acetyl percent, degree of substitution, WHC, OHC, flareability, solubility but reduce levels of fat, water, ash, fat, protein, starch and amylose starch, yam acetate. In this study at the best reaction time is (50 min), gives the acetyl percent 8.658% and substitution degree of 0.356, the value of WHC, OHC, Swelling ratio and solubility of 32.21%, 30.21%, 1.98 g/g, and 19.17% respectively.

scholarly journals Pemanfaatan Jerami Padi (Oryza Sativa L.) Sebagai Bahan Baku Dalam Pembuatan CMC (Carboximetil Cellulose)

2021 ◽  
Vol 15 (2) ◽  
pp. 194
Author(s):  
RIZKA NURLAILA
Keyword(s):  
Oryza Sativa ◽  
Reaction Time ◽  
Rice Straw ◽  
Carboxymethyl Cellulose ◽  
Oryza Sativa L ◽  
Raw Material ◽  
Cellulose Content ◽  
Cosmetic Products ◽  
High Cellulose

Rice straw is a waste from rice plants that contains 37.71% cellulose, 21.99% hemicellulose, and 16.62% lignin. High cellulose content in rice straw can be used as raw material for the manufacture of Carboxymethyl Cellulose (CMC). CMC is a cellulose derivative widely used in food, pharmaceutical, detergent, textile and cosmetic products industries as a thickener, stabilizer of emulsions, or suspensions and bonding. This study aims to process rice straw waste into CMC with variations in sodium monochloroacetate of 5,6,7,8 and 9 grams. The method used in this research is by synthesis using 15% NaOH solvent, with a reaction time of 3.5 hours and 5 grams of rice straw. The results showed that the best CMC was obtained at a concentration of 9 grams of sodium monochloroacete with a yield characterization of 94%, pH 6, water content of 13.39%, degree of substitution (Ds) of 0.80, and viscosity of 1.265 cP.

scholarly journals PEMBUATAN Carboxymethyl cellulose (CMC) DARI PELEPAH NANAS (Ananas cosmosus Merr.)

KOVALEN ◽  
2019 ◽  
Vol 5 (2) ◽  
pp. 166-172
Author(s):  
Ripdayana Ripdayana ◽  
Ahmad Ridhay ◽  
Erwin Abdul Rahim
Keyword(s):  
Reaction Time ◽  
Carboxymethyl Cellulose ◽  
Design Method ◽  
Independent Variables ◽  
Randomized Design ◽  
Substitution Degree ◽  
Optimum Reaction ◽  
Completely Randomized Design ◽  
Two Independent Variables

A research about production of Carboxymethyl cellulose (CMC)  from pineapple midrib (Ananas cosmosus Merr.) has been conducted.  This research aims to determine the best cellulose ratio with sodium monochloro acetate and the best reaction time to the substitution  degree of carboxymethyl cellulose from pineapple midrib fibers.  This study used a Completely Randomized Design method with two independent variables,  i.e. variations in the weight of sodium monochloroacetate (2.5 grams, 3 grams, 3.5 grams, 4 grams, and 4.5 grams) and variations in reaction time (1 hour, 2 hours, 3 hours, 4 hours , and 5 hours), each treatment was done  duplo using 20 treatment units. The result of the study showed that the best ratio of sodium monochloroacetate to cellulose which produced carboxymethyl cellulose from pineapple midribs was 2.5: 2.5 with  substitution degree value of  1.93  and optimum reaction time which produced carboxymethyl cellulose from pineapple midribs was 1 hour with substitution degree of 2.38. Keywords: Carboxymethyl cellulose, Pineapple midrib

scholarly journals Karakteristik Kimia dan Organoleptik Flakes Kacang Hijau dengan Penambahan Bahan Pengisi dan Air

2016 ◽  
Vol 8 (1) ◽  
pp. 24-28
Author(s):  
Maya Indra Rasyid
Keyword(s):  
Water Absorption ◽  
Water Content ◽  
Mung Bean ◽  
Protein Levels ◽  
Absorption Ratio ◽  
Bean Flour ◽  
Organoleptic Characteristics ◽  
Randomized Design ◽  
Two Factors ◽  
Completely Randomized Design

(Chemical and Organoleptic Characteristics of Mung Bean Flakes with The Addition of Fillers and Water) ABSTRACT. The objective of this research was to determine the chemical and organoleptic characteristics of mung bean flakes with the addition of fillers and water. The study was conducted using completely randomized design with two factors namely the addition of fillers and water. The results showed that the addition of fillers and water has significant (P≤0,01) effect on the water absorption ratio and protein levels of mung bean flakes. The best treatment was obtained by the mung bean flour without the addition of fillers with 150% of addition water with water absorption ratio of 204%, water content of 5,7%, protein of 22,01%, starch levels of 61,76%, organoleptic values of aroma of 2,61, color of 2,42, crispness of 2,72 and flavor of 2,83.

scholarly journals EFFECTS OF FERMENTATION DURATION ON PHYSICOCHEMICAL AND ORGANOLEPTIC CHARACTERISTICS OF THREE AGARWOODS (Aquilaria) LEAVES TEA

2021 ◽  
Vol 9 (2) ◽  
pp. 73-82
Author(s):  
Anisa Leksono ◽  
◽  
Erni Sofia Murtini ◽  
Keyword(s):  
Antioxidant Activity ◽  
Water Content ◽  
Plant Species ◽  
Black Tea ◽  
Total Phenol ◽  
Pharmacological Effects ◽  
Organoleptic Characteristics ◽  
Randomized Design ◽  
Two Factors ◽  
Completely Randomized Design

Aquilaria is one of the plant genus-producing agarwood. Aquilaria leaves have pharmacological effects which the potential to be processed into black tea. The aim of this study is to determine the effect of fermentation duration on physicochemical and organoleptic characteristics of Aquilaria leaves tea. This study employed a Completely Randomized Design with two factors; the plant species (A. crassna, A. malaccensis, and A. subintegra) and fermentation duration (0 minutes, 70 minutes, and 90 minutes). Parameters analyzed including water content, total phenol, and antioxidant activity. Organoleptic tests were performed on the color, taste, and aroma of the brewed tea. The results summarized that A. subintegra had the highest total phenol and antioxidant activity, but the taste of the tea was not favored. A. crassna fermented 70 minutes and A. malaccensis fermented 0 minutes were the most preferred, but both have lower total phenol and antioxidant activity than A. subintegra.

scholarly journals Potensi Produksi Asap Cair, Arang dan Tar dari Limbah Industri Pengolahan Kayu

2021 ◽  
Vol 10 (2) ◽  
pp. 100-105
Author(s):  
Alaik Z H Albaki ◽  
Ahmad S Purnama ◽  
Fajri Yulianto ◽  
Budy Rahmat ◽  
Vita Meylani
Keyword(s):  
Water Content ◽  
High Water ◽  
Wood Waste ◽  
High Water Content ◽  
Wood Processing ◽  
Liquid Smoke ◽  
Test Characteristics ◽  
Randomized Design ◽  
Pyrolysis Tar ◽  
Two Factors

The practice of burning and stockpiling to reduce wood waste from the wood processing industry is not in line with the demands of clean production, environmentally friendly and sustainable industries. Pyrolysis technology can be used to produce bioenergy from wood waste. The temperature and the time of the pyrolysis process, the water content of materials, and the content of different yields between types of wood waste affect the bioenergy products produced. This study was aimed at determining the effect of wood waste form and condition on the quality and quantity of liquid smoke, tar, and charcoal. A Completely Randomized Design with two factors of treatments, i.e., waste forms and the drying process, was applied in this research. The results showed that the condition and shape of the material affect the volume of liquid smoke and the weight of the charcoal produced. The condition of the material without drying with high water content and the shape of the chunks produce more liquid smoke with an average yield of 191.14 mL and 186.37 mL, while the charcoal produced is higher in the condition of the material with drying and shaved form at 125.83 g and 115.62 g. The results of the test characteristics of grade 1 and 2 distillation liquid smoke meet the Japanese liquid smoke quality standards with phenol levels in the range of 26.66-35.94 mg GAE/mL sample and acidity levels of 16.91-58.9%. Keywords: Char; liquid smoke; pyrolysis; tar; wood waste.   ABSTRAK Praktik pembakaran dan penimbunan untuk mereduksi limbah kayu dari industri pengolahan kayu tidak selaras dengan tuntutan produksi bersih, ramah lingkungan dan industri berkelanjutan. Teknologi pirolisis dapat digunakan untuk memproduksi bioenergi dari limbah kayu dengan suhu dan waktu proses pirolisis, kadar air bahan serta kandungan rendemen yang berbeda antar jenis limbah kayu mempengaruhi produk bioenergi yang dihasilkan. Penelitian ini bertujuan untuk mengetahui pengaruh bentuk dan kondisi limbah kayu terhadap kualitas dan kuantitas asap cair, ter dan arang. Metode penelitian yang dilakukan adalah Rancangan Acak Lengkap yang disusun secara faktorial dengan perlakuan bentuk limbah dan proses pengeringan. Hasil penelitian menunjukan bahwa kondisi dan bentuk bahan mempengaruhi volume asap cair dan bobot arang yang dihasilkan. Kondisi bahan tanpa pengeringan dengan kadar air tinggi dan bentuk bongkah menghasilkan asap cair lebih banyak dengan hasil rata-rata 191,14 mL dan 186,37 mL, sedangkan arang yang dihasilkan lebih tinggi pada kondisi bahan dengan pengeringan dan bentuk serut yaitu 125,83 g dan 115,62 g. Hasil uji karakteristik asap cair distilasi grade 1 dan 2 memenuhi standar mutu asap cair Jepang dengan kadar fenol berada pada kisaran 26,66-35,94 mg GAE/mL sampel dan kadar keasaman 16,91-58,9 %. Kata kunci: Arang; asap cair; limbah kayu; pirolisis; ter.

scholarly journals PENGARUH LAMA PEMANASAN DAN KADAR AIR YANG BERBEDA TERHADAP NILAI GLUKOSA DAN TOTAL KARBOHIDRAT PADA POLLARD

2019 ◽  
Vol 17 (1) ◽  
pp. 69-75
Author(s):  
Ikhsan I. Akbar ◽  
Marry Christiyanto ◽  
Cahya Setya Utama
Keyword(s):  
Experimental Design ◽  
Water Content ◽  
Total Carbohydrate ◽  
Glucose Content ◽  
Total Carbohydrate Content ◽  
Randomized Design ◽  
Secondary Factor ◽  
Two Factors ◽  
Carbohydrate Contents ◽  
Heating Duration

This study aims to determine the effects of different heating duration and water content on glucose and total carbohydrate in pollard. The experimental design in this study used a complete randomized design with two factors, of which are heating duration as the primary factor (T1=15 minutes and T2=30 minutes) water contentas the secondary factor (A1=25%, A2=50%, and A3=75%) with 3 replications. On glucose content, the duration ofheat treatment showed significant effect (p<0,05), while difference in water content didnot. On total carbohydrate content, the different water contentshowed significant effect (p<0,05), whereas different heating duration did notshow any significant effect. The research concludes that heating duration and water affects significantly on glucose and total carbohydrate contents, respectively. It is recommended that further research by digestibility analysis is needed to support the result of this research.

scholarly journals Pengaruh Konsentrasi Ekstrak Umbi Bit (Beta vulgaris L.) dan Gelatin Terhadap Karakteristik Marshmallow

2018 ◽  
Vol 3 (4) ◽  
pp. 808-821
Author(s):  
Cut Betari Arhandhi ◽  
Yuliani Aisyah ◽  
Rasdiansyah Rasdiansyah
Keyword(s):  
Antioxidant Activity ◽  
Vitamin C ◽  
Water Content ◽  
Beta Vulgaris ◽  
Natural Dyes ◽  
Randomized Design ◽  
Two Factors ◽  
Completely Randomized Design ◽  
Tuber Extract ◽  
Color Texture

Abstrak. Umbi bit merupakan salah satu bahan pangan yang dapat digunakan sebagai pewarna alami pada pembuatan soft candy seperti rshmallow. Penelitian ini dilakukan dengan menggunakan Rancangan Acak Lengkap (RAL) dengan pola faktorial yang terdiri atas dua faktor. Faktor pertama yaitu konsentrasi ekstrak umbi bit (B) yang terdiri dari 3 taraf yaitu B1 = 5% B2 = 10% dan B3 = 15%. Faktor kedua adalah konsentrasi gelatin (G) yang terdiri dari 3 taraf yaitu G1 = 3% G2 = 5% dan G3 = 8%. Ulangan dilakukan sebanyak 3 kali sehingga diperoleh 27 satuan percobaan. Hasil penelitian menunjukkan bawa konsentrasi ekstrak umbi bit berpengaruh sangat nyata terhadap kadar air, vitamin C dan aktivitas antioksidan serta uji deskrpsi aroma, rasa, warna buram, tekstur, dan mouthfeel marshmallow umbi bit. Adapun konsentasi gelatin berengaruh nyata terhadap kadar vitamin C dan uji deskripsi tekstur marshmallow umbi bit. Marshmallow umbi bit memiliki kadar air yaitu sebesar 22,06%, kadar vitmin C 80,67 Mg dan aktivitas antioksidan sebesar 30%.Abstract: Beetroot is one of food that can be used as natural dyes in making of soft candy like marshmallows. This research was conducted using a Completely Randomized Design (CRD) with a factorial pattern consisting of two factors. The first factor is the concentration of beet tuber extract (B) which consists of 3 levels, namely B1 = 5% B2 = 10% and B3 = 15%. The second factor is the concentration of gelatin (G) which consists of 3 levels, namely G1 = 3% G2 = 5% and G3 = 8%. Tests were carried out 3 replications so that 27 trial units were obtained. The results showed that the concentration of coffee extract had a very significant effect on water content, vitamin C and antioxidant activity, as well as the description of aroma, flavor, opaque color, texture, and mouthfeel marshmallow tuber content. The concentration of gelatin significantly affected vitamin C levels and test description of marshmallow tuber tuber texture. Marshmallow beetroot has a water content of 22.06%, vitamin C content of 80.67 Mg and antioxidant activity of 30%.

scholarly journals Pengaruh Suhu dan Waktu Pengeringan terhadap Karakteristik Kimia serta Sensori Teh Daun Bambu Tabah (Gigantochloa nigrociliata BUSE-KURZ.)

2019 ◽  
Vol 8 (2) ◽  
pp. 249
Author(s):  
I Kadek Wirawan ◽  
Pande Ketut Diah Kencana ◽  
I Made Supartha Utama
Keyword(s):  
Water Content ◽  
Total Phenol ◽  
Effect Of Temperature ◽  
Tea Leaves ◽  
Total Acid ◽  
Drying Time ◽  
Drying Temperature ◽  
Randomized Design ◽  
Two Factors ◽  
Completely Randomized Design

Penelitian ini bertujuan untuk mengetahui pengaruh suhu dan waktu pengeringan terhadap karakteristik kimia dan sensorik teh daun bambu Tabah. Penelitian ini dirancang menggunakan Rancangan Acak Lengkap (RAL) dengan dua faktor, yaitu faktor suhu pengeringan (50o C dan 60o C) dan faktor waktu pengeringan (1 jam, 2 jam, dan 3 jam). Perlakuan diulang tiga kali untuk mendapatkan 18 unit percobaan. Parameter yang diamati adalah kadar air, pH, total asam, total fenol, dan organoleptik. Hasil penelitian menunjukkan bahwa interaksi suhu dan lama pengeringan daun teh bambu Tabah memiliki pengaruh berbeda nyata terhadap kadar air, pH, total asam, total fenol, warna, penerimaan keseluruhan, tetapi tidak memiliki pengaruh yang berbeda nyata terhadap aroma dan rasa, dengan perlakuan terbaik ini, kadar air, pH, asam total, fenol total, warna, aroma, rasa dan penerimaan keseluruhan ditemukan kadar air 6,881%, pH 6,6, total asam 0, 73%, total fenol 84,01mg / 100g, warna 4,33, aroma 4,40, rasa 3,93, dan penerimaan keseluruhan 4,07.   This study aimd to determine the effect of temperature and drying time on the chemical and sensory characteristics of Tabah bamboo leaf tea. This study was designed using a Completely Randomized Design (CRD) with two factors, namely the drying temperature factor (50oC and 60oC) and the drying time factor (1 hour, 2 hours, and 3 hours). The treatment was repeated three times to obtain 18 experimental units. The parameters observed were water content, pH, total acid, total phenol, color, aroma, taste, and overall acceptance tested organoleptically. The results showed that the interaction of temperature and duration of drying of Tabah bamboo tea leaves had significantly different effects on water content, pH, total acid, total phenol, color, overall reception, but did not have a significantly different effect on aroma and taste. with this combained best treatment, the water content, pH, total acid, total phenol, color, aroma, taste and overall acceptance were found water content 6,881 %, pH 6,6, total acid 0, 73%, total phenol 84,01mg / 100g,color 4,33, aroma 4.40, taste 3,93, and overall acceptance 4,07.

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