scholarly journals Antimicrobial Efficacy of Low Concentration PVP-Silver Nanoparticles Deposited on DBD Plasma-Treated Polyamide 6,6 Fabric

Coatings ◽  
2019 ◽  
Vol 9 (9) ◽  
pp. 581 ◽  
Author(s):  
Ana Isabel Ribeiro ◽  
Dilara Senturk ◽  
Késia Karina Silva ◽  
Martina Modic ◽  
Uros Cvelbar ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Low Cost ◽  
Antimicrobial Effect ◽  
Bactericidal Effect ◽  
Dbd Plasma ◽  
Low Concentration ◽  
Log Reduction ◽  
Spray Method ◽  
Antibacterial Textiles ◽  
Fabric Surface

In this study, a low concentration (10 μg·mL−1) of poly(N-vinylpyrrolidone) (PVP)-coated silver nanoparticles (AgNPs) were deposited by spray and exhaustion (30, 70 and 100 °C) methods onto untreated and dielectric barrier discharge (DBD) plasma-treated polyamide 6,6 (PA66) fabric. DBD plasma-treated samples showed higher AgNP deposition than untreated ones for all methods. After five washing cycles, only DBD plasma-treated samples displayed AgNPs on the fabric surface. The best-performing method was exhaustion at 30 °C, which exhibited less agglomeration and the best antibacterial efficacy against S. aureus (4 log reduction). For E. coli, the antimicrobial effect showed good results in all the exhaustion samples (5 log reduction). Considering the spray method, only the DBD plasma-treated samples showed some bacteriostatic activity for both strains, but the AgNP concentration was not enough to have a bactericidal effect. Our results suggest DBD plasma may be a low cost and chemical-free method for the preparation of antibacterial textiles, allowing for the immobilization of a very low—but effective—concentration of AgNPs.

scholarly journals Effect of Dispersion Solvent on the Deposition of PVP-Silver Nanoparticles onto DBD Plasma-Treated Polyamide 6,6 Fabric and Its Antimicrobial Efficiency

Nanomaterials ◽  
2020 ◽  
Vol 10 (4) ◽  
pp. 607
Author(s):  
Ana I. Ribeiro ◽  
Martina Modic ◽  
Uros Cvelbar ◽  
Gheorghe Dinescu ◽  
Bogdana Mitu ◽  
...  
Keyword(s):  
Antimicrobial Activity ◽  
Silver Nanoparticles ◽  
Photoelectron Spectroscopy ◽  
Antimicrobial Effect ◽  
Dbd Plasma ◽  
Surface Distribution ◽  
E Coli ◽  
Log Reduction ◽  
Spray Method ◽  
Exhaustion Method

Polyvinylpyrrolidone-coated silver nanoparticles (PVP-AgNPs) dispersed in ethanol, water and water/alginate were used to functionalize untreated and dielectric barrier discharge (DBD) plasma-treated polyamide 6,6 fabric (PA66). The PVP-AgNPs dispersions were deposited onto PA66 by spray and exhaustion methods. The exhaustion method showed a higher amount of deposited AgNPs. Water and water-alginate dispersions presented similar results. Ethanol amphiphilic character showed more affinity to AgNPs and PA66 fabric, allowing better uniform surface distribution of nanoparticles. Antimicrobial effect in E. coli showed good results in all the samples obtained by exhaustion method but using spray method only the DBD plasma treated samples displayed antimicrobial activity (log reduction of 5). Despite the better distribution achieved using ethanol as a solvent, water dispersion samples with DBD plasma treatment displayed better antimicrobial activity against S. aureus bacteria in both exhaustion (log reduction of 1.9) and spray (methods log reduction of 1.6) due to the different oxidation states of PA66 surface interacting with PVP-AgNPs, as demonstrated by X-ray Photoelectron Spectroscopy (XPS) analysis. Spray method using the water-suspended PVP-AgNPs onto DBD plasma-treated samples is much faster, less agglomerating and uses 10 times less PVP-AgNPs dispersion than the exhaustion method to obtain an antimicrobial effect in both S. aureus and E. coli.

Biosynthesis of Silver Nanoparticles for Study of Their Antimicrobial Effect on Plasma-Treated Textiles

2022 ◽  
pp. 149-166
Author(s):  
Shazia Shukrullah ◽  
Muhammad Anwar ◽  
Muhammad Yasin Naz ◽  
Inzamam Ul Haq
Keyword(s):  
Silver Nanoparticles ◽  
Plasma Treatment ◽  
Antimicrobial Properties ◽  
Antimicrobial Effect ◽  
Dielectric Medium ◽  
Average Crystalline Size ◽  
Dielectric Barrier Discharges ◽  
Dbd Plasma ◽  
Fabric Surface ◽  
Barrier Discharges

Dielectric barrier discharges (DBD) are the configurations for the production of electrical discharges using a dielectric medium between the metallic electrodes. Plasma treatment produces negative radicals, which increase the adhesion of fabric for nanoparticles. The plasma treatment made the fabric surface rougher because of the etching effect. UV-vis spectra of the Plasmon resonance band observed at 253-400 nm. X-ray diffraction results showed that AgNPs has a cubical structure and the average crystalline size is 25 nm. SEM results determined that the morphology of the silver nanoparticles are flower shaped. The energy bandgap of AgNPs was observed at 2.59 eV. The silver nanoparticles were found to have enhanced antimicrobial properties and showed better zone of inhibition against isolated bacteria (Escherichia coli). DBD plasma treatment changed the chemical as well as physical properties of the cotton fabric. FTIR spectrum revealed that oxygen-containing groups, such as C-O, C=O, O-C-O, as well as O-C=O, increased on DBD treatment of cotton samples.

scholarly journals Electrospun Silver Coated Polyacrylonitrile Membranes for Water Filtration Applications

Membranes ◽  
2018 ◽  
Vol 8 (3) ◽  
pp. 59 ◽  
Author(s):  
Shalv Parekh ◽  
Rebecca David ◽  
Kranthi Bannuru ◽  
Lakshminarasimhan Krishnaswamy ◽  
Avinash Baji
Keyword(s):  
Silver Nanoparticles ◽  
Low Cost ◽  
Silver Ions ◽  
Antimicrobial Effect ◽  
Water Filtration ◽  
Porous Membranes ◽  
Oh Groups ◽  
Underdeveloped Countries ◽  
Latex Beads ◽  
Particulate Filtration

The scarcity of drinking water and the contamination of water sources in underdeveloped countries are serious problems that require immediate low-tech and low-cost solutions. In this study, we fabricated polyacrylonitrile (PAN) porous membranes coated with silver nanoparticles (AgNP) and demonstrated their use for water filtration and water treatment applications. The membranes were prepared by electrospinning a PAN solution and treating in a hydroxylamine (NH2OH) aqueous solution to form –C(NH2)N–OH groups that were used for functionalization (Ag+ ions) of the membrane. The coordinated silver ions were then converted to silver nanoparticles. The microstructure of the membrane, water permeability, antimicrobial effect (using Escherichia coli), and particulate filtration capabilities were studied. This study verified that the membrane demonstrated a 100% reduction for Gram-negative bacteria with an effective filtration rate of 8.0 mL/cm2 min. Furthermore, the membrane was able to eliminate 60% of latex beads as small as 50 nm and over 80% of the 2 µm beads via gravity filtration. This study demonstrated that PAN–AgNP membranes can be employed as antimicrobial membranes for the filtration of water in underdeveloped countries.

scholarly journals A Novel Coloration of Polyester Fabric through Green Silver Nanoparticles (G-AgNPs@PET)

Nanomaterials ◽  
2019 ◽  
Vol 9 (4) ◽  
pp. 569 ◽  
Author(s):  
K. Hasan ◽  
Md. Pervez ◽  
Md. Talukder ◽  
Mst. Sultana ◽  
Sakil Mahmud ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Low Cost ◽  
Antibacterial Properties ◽  
Polyester Fabric ◽  
Bacterial Reduction ◽  
Tem Analysis ◽  
Pet Fabric ◽  
Thermogravimetric Analyzer ◽  
Transmission Electron ◽  
Fabric Surface

This paper reports a novel route for the coloration of polyester fabric with green synthesized silver nanoparticles (G-AgNPs@PET) using chitosan as a natural eco-friendly reductant. The formation of AgNPs was confirmed by UV-visible spectroscopy. The morphologies and average particles size of G-AgNPs was investigated by transmission electron microscope (TEM) analysis. The uniform deposition of G-AgNPs on the PET fabric surface was confirmed with scanning electron microscopy (SEM) and Fourier transform infrared (FT-IR) spectroscopy. The thermal properties were investigated using a thermogravimetric analyzer (TGA). The coloration and fastness properties of fabric were found to be significantly improved, a result related to the surface plasmon resonance of G-AgNPs. The antibacterial properties of fabric were also found to be excellent as more than 80% bacterial reduction was noticed even after 10 washing cycles. Overall, the proposed coating process using green nanoparticles can contribute to low-cost production of sustainable textiles.

scholarly journals New Textile for Personal Protective Equipment—Plasma Chitosan/Silver Nanoparticles Nylon Fabric

Fibers ◽  
2021 ◽  
Vol 9 (1) ◽  
pp. 3
Author(s):  
Cláudia M. Botelho ◽  
Margarida M. Fernandes ◽  
Jefferson M. Souza ◽  
Nicolina Dias ◽  
Ana M. Sousa ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Antimicrobial Effect ◽  
Average Diameter ◽  
Face Mask ◽  
Nylon Fabric ◽  
Resonance Band ◽  
Washing Process ◽  
Mask Material ◽  
Fabric Surface ◽  
Fabric Structures

Fabric structures are prone to contamination with microorganisms, as their morphology and ability to retain moisture creates a proper environment for their growth. In this work, a novel, easily processed and cheap coating for a nylon fabric with antimicrobial characteristics was developed. After plasma treatment, made to render the fabric surface more reactive sites, the fabric was impregnated with chitosan and silver nanoparticles by simply dipping it into a mixture of different concentrations of both components. Silver nanoparticles were previously synthesized using the Lee–Meisel method, and their successful obtention was proven by UV–Vis, showing the presence of the surface plasmon resonance band at 410 nm. Nanoparticles with 25 nm average diameter observed by STEM were stable, mainly in the presence of chitosan, which acted as a surfactant for silver nanoparticles, avoiding their aggregation. The impregnated fabric possessed bactericidal activity higher for Gram-positive Staphylococcus aureus than for Gram-negative Pseudomonas aeruginosa bacteria for all combinations. The percentage of live S. aureus and P. aeruginosa CFU was reduced to less than 20% and 60%, respectively, when exposed to each of the coating combinations. The effect was more pronounced when both chitosan and silver were present in the coating, suggesting an effective synergy between these components. After a washing process, the antimicrobial effect was highly reduced, suggesting that the coating is unstable after washing, being almost completely removed from the fabric. Nevertheless, the new-coated fabric can be successfully used in single-use face masks. To our knowledge, the coating of nylon fabrics intended for face-mask material with both agents has never been reported.

scholarly journals Robust immobilization of anionic silver nanoparticles on cellulose filter paper toward a low-cost point-of-use water disinfection system with improved anti-biofouling properties

RSC Advances ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 4873-4882
Author(s):  
Gongyan Liu ◽  
Ruiquan Yu ◽  
Jing Jiang ◽  
Zhuang Ding ◽  
Jing Ma ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Filter Paper ◽  
Low Cost ◽  
Water Disinfection ◽  
Point Of Use ◽  
Cellulose Filter

Point-of-use water disinfection by GA@AgNPs-LA-FP.

scholarly journals Evidence in Practice of Tissue Healing with Latex Biomembrane: Integrative Review

2019 ◽  
Vol 2019 ◽  
pp. 1-17 ◽  
Author(s):  
Suélia de Siqueira Rodrigues Fleury Rosa ◽  
Mário Fabrício Fleury Rosa ◽  
Marcos Augusto Moutinho Fonseca ◽  
Glécia Virgolino da Silva Luz ◽  
Carlos Federico Domínguez Avila ◽  
...  
Keyword(s):  
Diabetes Mellitus ◽  
Wound Healing ◽  
Chronic Diseases ◽  
Low Cost ◽  
Rubber Tree ◽  
Antimicrobial Effect ◽  
Integrative Review ◽  
Complication Rates ◽  
Biocompatible Material ◽  
Tissue Healing

Wound healing is a perfectly coordinated cascade of cellular, molecular, and biochemical events which interact in tissue reconstitution. Chronic diseases such as pressure ulcers (PU) and diabetes mellitus (DM) are considered risk factors for wound healing. Patients with such diseases often have higher sepsis, infection, and complication rates, since they have revascularization inhibition and low growth factor expression. Thus, latex biomembrane (LBM), a biocompatible material, derived from the latex of the rubber tree (Hevea brasiliensis) appears to create tendencies as an angiogenic-inducing tissue healing agent and as biomaterial, resulting from its structural qualities and its low cost when compared to conventional treatments. Therefore, this work aims at summarizing the results, experiments, and scientific findings that certify or recommend the use of LBM as a new technique to be applied effectively in the treatment of wounds. An integrative review was held in the BIREME, LILACS, Burns, MEDLINE, PubMed, and SciELO databases, from 2000 to 2016, using the following descriptors: “healing,” “diabetes mellitus,” “wounds,” and “latex membrane.” As a result, 600 experiments (out of 612) presented satisfactory results; however, 33% of the cases received explicit recommendations, 11% required more studies on the subjects, and 1% was denied. On the other hand, half of the studies did not expressly endorse its use, despite presenting satisfactory results. The LBM was characterized as a good therapeutic alternative in cases of wounds, including chronic diseases, such as diabetes mellitus and PU, due to its relevant potential for wound healing stimulation, acceleration of cell tissue mending and revascularization, or the reestablishment of angiogenic functions (creation of new blood vessels). The LBM was also confirmed to be safe as a biocompatible material whose structural qualities (elasticity, adaptability, impermeability, and possibility of suture), devoid of toxicity, allowed interaction between tissues and presented no hypersensitivity inducer and no antimicrobial effect.

scholarly journals Biosynthesis, Characterization, and Biological Activities of Procyanidin Capped Silver Nanoparticles

2020 ◽  
Vol 11 (3) ◽  
pp. 66
Author(s):  
Umar M. Badeggi ◽  
Jelili A. Badmus ◽  
Subelia S. Botha ◽  
Enas Ismail ◽  
Jeanine L. Marnewick ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Food Packaging ◽  
Antioxidant Activities ◽  
Biological Activities ◽  
Bacterial Species ◽  
Bactericidal Effect ◽  
Total Extract ◽  
Selected Area Electron Diffraction ◽  
Ic50 Values ◽  
Inhibitory Activities

In this study, procyanidin dimers and Leucosidea sericea total extract (LSTE) were employed in the synthesis of silver nanoparticles (AgNPs) and characterized by ultraviolet-visible (UV-Visible) spectroscopy, high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED), X-ray diffraction (XRD), and dynamic light scattering (DLS) techniques. AgNPs of about 2–7 nm were obtained. DLS and stability evaluations confirmed that the AgNPs/procyanidins conjugates were stable. The formed nanoparticles exhibited good inhibitory activities against the two enzymes studied. The IC50 values against the amylase enzyme were 14.92 ± 1.0, 13.24 ± 0.2, and 19.13 ± 0.8 µg/mL for AgNPs coordinated with LSTE, F1, and F2, respectively. The corresponding values for the glucosidase enzyme were 21.48 ± 0.9, 18.76 ± 1.0, and 8.75 ± 0.7 µg/mL. The antioxidant activities were comparable to those of the intact fractions. The AgNPs also demonstrated bacterial inhibitory activities against six bacterial species. While the minimum inhibitory concentrations (MIC) of F1-AgNPs against Pseudomonas aeruginosa and Staphylococcus aureus were 31.25 and 15.63 µg/mL respectively, those of LSTE-AgNPs and F2-AgNPs against these organisms were both 62.50 µg/mL. The F1-AgNPs demonstrated a better bactericidal effect and may be useful in food packaging. This research also showed the involvement of the procyanidins as reducing and capping agents in the formation of stable AgNPs with potential biological applications.

Size-controlled fabrication of silver nanoparticles using the Hedyotis puberula leaf extract: toxicity on mosquito vectors and impact on biological control agents

RSC Advances ◽  
2016 ◽  
Vol 6 (99) ◽  
pp. 96573-96583 ◽  
Author(s):  
Raja Mohamed Sait Thameem Azarudeen ◽  
Marimuthu Govindarajan ◽  
Abubucker Amsath ◽  
Shine Kadaikunnan ◽  
Naiyf S. Alharbi ◽  
...  
Keyword(s):  
Biological Control ◽  
Silver Nanoparticles ◽  
Leaf Extract ◽  
Low Cost ◽  
Aquatic Organisms ◽  
Capping Agent ◽  
Mosquito Vectors ◽  
Biological Control Agents ◽  
Size Controlled ◽  
Control Tool

As a low-cost and eco-friendly control tool, Ag nanoparticles were fabricated usingHedyotis puberulaaqueous extract as a reducing and capping agent and showed potent activity against malaria and arbovirus vectors with low biotoxicity against non-target aquatic organisms.

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