scholarly journals Simulated and Experimental Investigation of the Mechanical Properties and Solubility of 3D-Printed Capsules for Self-Healing Cement Composites

Materials ◽  
2021 ◽  
Vol 14 (16) ◽  
pp. 4578
Author(s):  
Se-Jin Choi ◽  
Ji-Hwan Kim ◽  
Hyojin Jeong ◽  
Ja-Sung Lee ◽  
Tae-Uk Lim ◽  
...  

In the concrete industry, various R&D efforts have been devoted to self-healing technology, which can maintain the long-term performance of concrete structures, which is important in terms of sustainable development. Cracks in cement composites occur and propagate because of various internal and external factors, reducing the composite’s stability. Interest in “self-healing” materials that can repair cracks has led researchers to embed self-healing capsules in cement composites. Overcoming the limitations of polymer capsules produced by chemical manufacturing methods, three-dimensional (3D) printing can produce capsules quickly and accurately and offers advantages such as high material strength, low cost, and the ability to fabricate capsules with complex geometries. We performed structural analysis simulations, experimentally evaluated the mechanical properties and solubility of poly(lactic acid) (PLA) capsules, and examined the effect of the capsule wall thickness and printing direction on cement composites embedded with these capsules. Thicker capsules withstood larger bursting loads, and the capsule rupture characteristics varied with the printing angle. Thus, the capsule design parameters must be optimized for different environments. Although the embedded capsules slightly reduced the compressive strength of the cement composites, the benefit of the encapsulated self-healing agent is expected to overcome this disadvantage.

2018 ◽  
Vol 52 (25) ◽  
pp. 3429-3444 ◽  
Author(s):  
Ezequiel Buenrostro ◽  
Daniel Whisler

Three-dimensional fiber-reinforced foam cores may have improved mechanical properties under specific strain rates and fiber volumes. But its performance as a core in a composite sandwich structure has not been fully investigated. This study explored different manufacturing techniques for the three-dimensional fiber-reinforced foam core using existing literature as a guideline to provide a proof of concept for a low-cost and easily repeatable method comprised of readily available materials. The mechanical properties of the fiber-reinforced foam were determined using a three-point bend test and compared to unreinforced polyurethane foam. The foam was then used in a sandwich panel and subjected to dynamic loading by means of a gas gun (103 s−1). High-strain impact tests validated previously published studies by showing, qualitatively and quantitatively, an 18–20% reduction in the maximum force experienced by the fiber-reinforced core and its ability to dissipate the impact force in the foam core sandwich panel. The results show potential for this cost-effective manufacturing method to produce an improved composite foam core sandwich panel for applications where high-velocity impacts are probable. This has the potential to reduce manufacturing and operating costs while improving performance.


Materials ◽  
2018 ◽  
Vol 11 (10) ◽  
pp. 1893 ◽  
Author(s):  
Přemysl Menčík ◽  
Radek Přikryl ◽  
Ivana Stehnová ◽  
Veronika Melčová ◽  
Soňa Kontárová ◽  
...  

This paper explores the influence of selected commercial plasticizers structure, which are based on esters of citric acid, on mechanical and thermal properties of Poly(3-hydroxybutyrate)/Poly(lactic acid)/Plasticizer biodegradable blends. These plasticizers were first tested with respect to their miscibility with Poly(3-hydroxybutyrate)/Poly(lactic acid) (PHB/PLA) blends using a kneading machine. PHB/PLA/plasticizer blends in the weight ratio (wt %) of 60/25/15 were then prepared by single screw and corotating meshing twin screw extruders in the form of filament for further three-dimensional (3D) printing. Mechanical, thermal properties, and shape stability (warping effect) of 3D printed products can be improved just by the addition of appropriate plasticizer to polymeric blend. The goal was to create new types of eco-friendly PHB/PLA/plasticizers blends and to highly improve the poor mechanical properties of neat PHB/PLA blends (with majority of PHB) by adding appropriate plasticizer. Mechanical properties of plasticized blends were then determined by the tensile test of 3D printed test samples (dogbones), as well as filaments. Measured elongation at break rapidly enhanced from 21% for neat non-plasticized PHB/PLA blends (reference) to 328% for best plasticized blends in the form of filament, and from 5% (reference) to 187% for plasticized blends in the form of printed dogbones. The plasticizing effect on blends was confirmed by Modulated Differential Scanning Calorimetry. The study of morphology was performed by the Scanning Electron Microscopy. Significant problem of plasticized blends used to be also plasticizer migration, therefore the diffusion of plasticizers from the blends after 15 days of exposition to 110 °C in the drying oven was investigated as their measured weight loss. Almost all of the used plasticizers showed meaningful positive softening effects, but the diffusion of plasticizers at 110 °C exposition was quite extensive. The determination of the degree of disintegration of selected plasticized blend when exposed to a laboratory-scale composting environment was executed to roughly check the “biodegradability”.


Polymers ◽  
2020 ◽  
Vol 12 (3) ◽  
pp. 651 ◽  
Author(s):  
David Moises Baca Lopez ◽  
Rafiq Ahmad

The application of single homogeneous materials produced through the fused deposition modelling (FDM) technology restricts the production of high-level multi-material components. The fabrication of a sandwich-structured specimen with different material combinations using conventional thermoplastics such as poly (lactic acid) (PLA), acrylonitrile butadiene styrene (ABS) and high impact polystyrene (HIPS) through the filament-based extrusion process can demonstrate an improvement on its properties. This paper aims to assess among these materials, the best material sandwich-structured arrangement design, to enhance the mechanical properties of a part and to compare the results with the homogeneous materials selected. The samples were subjected to tensile testing to identify the tensile strength, elongation at break and Young’s modulus of each material combination. The experimental results demonstrate that applying the PLA-ABS-PLA sandwich arrangement leads to the best mechanical properties between these materials. This study enables users to consider sandwich structure designs as an alternative to manufacturing multi-material components using conventional and low-cost materials. Future work will consider the flexural tests to identify the maximum stresses and bending forces under pressure.


2012 ◽  
Vol 2 (1) ◽  
Author(s):  
Jifeng Wang ◽  
Jorge Olortegui-Yume ◽  
Norbert Müller

AbstractA low cost, light weight, high performance composite material turbomachinery impeller with a uniquely designed blade patterns is analyzed. Such impellers can economically enable refrigeration plants to use water as a refrigerant (R718). A strength and dynamic characteristics analyses procedure is developed to assess the maximum stresses and natural frequencies of these wound composite axial impellers under operating loading conditions. Numerical simulation using FEM for two-dimensional and three-dimensional impellers was investigated. A commercially available software ANSYS is used for the finite element calculations. Analysis is done for different blade geometries and then suggestions are made for optimum design parameters. In order to avoid operating at resonance, which can make impellers suffer a significant reduction in the design life, the designer must calculate the natural frequency and modal shape of the impeller to analyze the dynamic characteristics. The results show that using composite Kevlar fiber/epoxy matrix enables the impeller to run at high tip speed and withstand the stresses, no critical speed will be matched during start-up and shut-down, and that mass imbalances of the impeller shall not pose a critical problem.


2016 ◽  
Vol 17 (3-4) ◽  
Author(s):  
Matti Kesti ◽  
Philipp Fisch ◽  
Marco Pensalfini ◽  
Edoardo Mazza ◽  
Marcy Zenobi-Wong

AbstractBiofabrication techniques including three-dimensional bioprinting could be used one day to fabricate living, patient-specific tissues and organs for use in regenerative medicine. Compared to traditional casting and molding methods, bioprinted structures can be much more complex, containing for example multiple materials and cell types in controlled spatial arrangement, engineered porosity, reinforcement structures and gradients in mechanical properties. With this complexity and increased function, however, comes the necessity to develop guidelines to standardize the bioprinting process, so printed grafts can safely enter the clinics. The bioink material must firstly fulfil requirements for biocompatibility and flow. Secondly, it is important to understand how process parameters affect the final mechanical properties of the printed graft. Using a gellan-alginate physically crosslinked bioink as an example, we show shear thinning and shear recovery properties which allow good printing resolution. Printed tensile specimens were used to systematically assess effect of line spacing, printing direction and crosslinking conditions. This standardized testing allowed direct comparison between this bioink and three commercially-available products. Bioprinting is a promising, yet complex fabrication method whose outcome is sensitive to a range of process parameters. This study provides the foundation for highly needed best practice guidelines for reproducible and safe bioprinted grafts.


2010 ◽  
Vol 133-134 ◽  
pp. 497-502 ◽  
Author(s):  
Alvaro Quinonez ◽  
Jennifer Zessin ◽  
Aissata Nutzel ◽  
John Ochsendorf

Experiments may be used to verify numerical and analytical results, but large-scale model testing is associated with high costs and lengthy set-up times. In contrast, small-scale model testing is inexpensive, non-invasive, and easy to replicate over several trials. This paper proposes a new method of masonry model generation using three-dimensional printing technology. Small-scale models are created as an assemblage of individual blocks representing the original structure’s geometry and stereotomy. Two model domes are tested to collapse due to outward support displacements, and experimental data from these tests is compared with analytical predictions. Results of these experiments provide a strong understanding of the mechanics of actual masonry structures and can be used to demonstrate the structural capacity of masonry structures with extensive cracking. Challenges for this work, such as imperfections in the model geometry and construction problems, are also addressed. This experimental method can provide a low-cost alternative for the collapse analysis of complex masonry structures, the safety of which depends primarily on stability rather than material strength.


2021 ◽  
Vol 22 (22) ◽  
pp. 12347
Author(s):  
Ashlee F. Harris ◽  
Jerome Lacombe ◽  
Frederic Zenhausern

The decellularization of plant-based biomaterials to generate tissue-engineered substitutes or in vitro cellular models has significantly increased in recent years. These vegetal tissues can be sourced from plant leaves and stems or fruits and vegetables, making them a low-cost, accessible, and sustainable resource from which to generate three-dimensional scaffolds. Each construct is distinct, representing a wide range of architectural and mechanical properties as well as innate vasculature networks. Based on the rapid rise in interest, this review aims to detail the current state of the art and presents the future challenges and perspectives of these unique biomaterials. First, we consider the different existing decellularization techniques, including chemical, detergent-free, enzymatic, and supercritical fluid approaches that are used to generate such scaffolds and examine how these protocols can be selected based on plant cellularity. We next examine strategies for cell seeding onto the plant-derived constructs and the importance of the different functionalization methods used to assist in cell adhesion and promote cell viability. Finally, we discuss how their structural features, such as inherent vasculature, porosity, morphology, and mechanical properties (i.e., stiffness, elasticity, etc.) position plant-based scaffolds as a unique biomaterial and drive their use for specific downstream applications. The main challenges in the field are presented throughout the discussion, and future directions are proposed to help improve the development and use of vegetal constructs in biomedical research.


Materials ◽  
2021 ◽  
Vol 14 (16) ◽  
pp. 4677
Author(s):  
Taeuk Lim ◽  
Hao Cheng ◽  
Wonil Song ◽  
Jasung Lee ◽  
Sunghoon Kim ◽  
...  

Three-dimensional (3D) printer-based self-healing capsules, embedded in cement composites, were proposed to heal cracks, as they allow for various structural designs of capsules, repeatable fabrication, and strength analysis. Out of many 3D printing methods, such as fusion deposition modeling (FDM), powder layer fusion, and PolyJet printing, FDM was used to design, analyze, and produce new self-healing capsules, which are widely used due to their high-speed, low-cost, and precise manufacturing. However, the PLA extruded in the FDM had low adhesion energy between stacked layers, which caused a degradation of the performance of the self-healing capsule, because it had different strengths depending on the angle between the stacked layers and the applied load within the concrete structure. Therefore, in this paper, specimens were produced, in accordance with ASTM specifications, using the FDM PLA method, and mechanical properties were obtained through tensile, shear, and compression tests. Additionally, the isotropic fracture characteristics of the four types of capsules were analyzed through finite element method analysis. Subsequently, the 3D-printed capsules were produced, and the fracture strength was analyzed in the x, y and z directions of the applied load through a compression test. As a result, the newly proposed capsule design was verified to have an isotropic fracture strength value of 1400% in all directions compared to conventional spherical thin film capsules


2021 ◽  
Author(s):  
Dmitry Vysochinskiy ◽  
Naureen Akhtar ◽  
Tord Nordmo ◽  
Mathias Rabjerg Strand ◽  
Adrian Vyssios ◽  
...  

The additive manufacturing has initially gained popularity for production of non-loadbearing parts and components or in the fields where the material strength and ductility are less important such as modelling and rapid prototyping. But as the technology develops, availability of metal additive manufacturing naturally dictates the desire to use the produced components in load-bearing parts. This requires not-only a thorough documentation on the mechanical properties but also additional and independent research to learn the expected level of variation of the mechanical properties and what factors affect them. The presented paper investigates strength, ductility, hardness, and microstructure of the AlSi10Mg alloy produced by the selective laser melting (SLM). The mechanical properties were determined through a series of uniaxial tension tests and supplementary hardness tests and rationalized with the microstructure evolution with regard to printing direction and heat treatment. The paper also addresses the effect of surface roughness on the mechanical properties of the material, by comparing the machined and net shape tension samples. As expected, the as-manufactured AlSi10Mg-alloy appears to be a semi-brittle alloy, but its microstructure can be altered, and ductility increased by a proper heat-treatment. The effect of surface layer removal on the measured mechanical properties is of particular interest.


2019 ◽  
Vol 14 ◽  
pp. 155892501989525 ◽  
Author(s):  
Pia Meyer ◽  
Christoph Döpke ◽  
Andrea Ehrmann

Three-dimensional printing belongs to the emerging technologies of our time. Still being relatively time-consuming and suffering from low mechanical properties, three-dimensional printing can be combined with other production technologies to overcome these problems. Three-dimensional printing on textile fabrics, for example, allows for creating large areas with sufficient lateral mechanical properties in a reasonable time on which three-dimensional printed parts give additional functionalities or laterally selective mechanical rigidity and so on. To create three-dimensional printed personalized knee joint support bandages, however, the adhesion between textile fabric and polymeric parts needs to be further increased. Here, we report on the influence of a polymer coating on different textile fabrics on the adhesion of three-dimensional printed elements from hard and soft poly(lactic acid). Surprisingly, the coating increases the adhesion significantly for the hard poly(lactic acid), while the soft poly(lactic acid) sticks better on some materials without additional coating. Maximum separation forces are measured for linen which can be attributed to the relatively long linen fibers with uneven surface, increasing the fiber–fiber friction inside the fabric and the adhesion to the polymer.


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