scholarly journals Effect of Heat Treatment on the Microstructure and Mechanical Properties of Selective Laser-Melted Ti64 and Ti-5Al-5Mo-5V-1Cr-1Fe

Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 534
Author(s):  
Hongjie Bai ◽  
Hao Deng ◽  
Longqing Chen ◽  
Xianbo Liu ◽  
Xiaorong Qin ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Fracture Toughness ◽  
Titanium Alloys ◽  
Post Process ◽  
Heat Treated ◽  
Process Heat ◽  
The One ◽  
Equilibrium Microstructure ◽  
Non Equilibrium

Additive manufacturing (AM) has shown the ability in processing titanium alloys. However, due to the unique thermal history in AM, the microstructure of AM-fabricated parts is metastable and non-equilibrium. This work was aiming to tailor the microstructure and to improve the mechanical properties of α+β Ti-6Al-4V alloy and metastable β Ti-5Al-5Mo-5V-1Cr-1Fe alloys by manipulating the post-process heat treatment. The results showed that Ti-6Al-4V exhibited a metastable α’ martensite microstructure in the as-fabricated condition, while a metastable β structure was formed in as-printed Ti-5Al-5Mo-5V-1Cr-1Fe. After post-process heat treatment, both lamellar and bimodal microstructures were obtained in Ti64 and Ti-5Al-5Mo-5V-1Cr-1Fe alloys. Especially, the Ti-6Al-4V alloy subjected to 950 °C annealing showed the lamellar structure with the highest fracture toughness of 90.8 ± 2.1 MPa.m1/2. The one cyclically heat-treated has excellent combined strength, ductility and fracture toughness attributed to the bimodal structure. In addition, similar observations of lamellar and bimodal microstructure appeared in the post-process heat-treated Ti-5Al-5Mo-5V-1Cr-1Fe alloy. This study demonstrated that heat treatment is an effective way to tackle the non-equilibrium microstructure and improve the mechanical properties of selective laser melting (SLM)-fabricated titanium alloys.

Heat Treatment Variability Effects on the Mechanical Properties of Beta Solution Treated Ti-6Al-4V

2010 ◽  
Vol 638-642 ◽  
pp. 401-406
Author(s):  
J.R. Calcaterra
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Fracture Toughness ◽  
Solution Heat Treatment ◽  
Thermomechanical Processing ◽  
Tensile Tests ◽  
Maximum Temperature ◽  
Work Piece ◽  
Fatigue Crack Growth Resistance ◽  
Heat Treated

Beta solution heat treatment is used to increase the fatigue crack growth resistance of Ti-6AL-4V. Unfortunately, the beta solution heat treatment is very sensitive to maximum temperature, time at temperature and cooling rate. In order to determine the effect of these parameters on mechanical properties, several different titanium billets and forgings were heat treated at various times and temperatures. The forgings had differing amounts of work, reflecting the potential for thermomechanical processing differences seen in a die forged component. Fracture toughness and tensile tests were conducted on the billets and forgings. In addition, sections of each work piece were excised and examined microscopically. The results from the study indicate there is a significant effect of heat treatment on thicker section components. In these cases, grains near the surface may grow large, while being barely transformed near the center. The change in microstructure has an effect on mechanical properties. Material with the larger grains tends to have worse ductility, while the fracture toughness properties of the material tend to decrease with grain size.

Mechanochemically synthesized NbC cermets: Part II. Mechanical properties

1999 ◽  
Vol 14 (11) ◽  
pp. 4285-4290 ◽  
Author(s):  
B. R. Murphy ◽  
T. H. Courtney
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Fracture Toughness ◽  
Mechanical Behavior ◽  
Fracture Behavior ◽  
Cu Content ◽  
Heat Treated

The mechanical behavior of mechanochemically synthesized NbC cermets was investigated. Material hardnesses range from a high of 19.6 GPa for as-synthesized cermets containing about 4 vol% of Fe to a low of about 4 GPa for heat-treated cermets containing about 34 vol% Cu. Higher hardness generally correlates with lower fracture toughness (about 2 MPa m1/2 for cermets containing the highest percentage of NbC) and vice versa. Highest fracture toughness (about 7.5 MPa m1/2) is found in NbC–18 vol% Fe cermets heat treated extensively following consolidation. Abnormally low fracture toughnesses are found in high-Cu-content cermets in which Cu segregation takes place during heat treatment. Current models of ceramic toughening can be applied to describe the fracture behavior of NbC–Fe cermets.

scholarly journals Influence of Post Weld Heat Treatment on the Grain Size, and Mechanical Properties of the Alloy-800H Rotary Friction Weld Joints

Materials ◽  
2021 ◽  
Vol 14 (16) ◽  
pp. 4366
Author(s):  
Saqib Anwar ◽  
Ateekh Ur Rehman ◽  
Yusuf Usmani ◽  
Ali M. Al-Samhan
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Grain Size ◽  
Heat Affected Zone ◽  
Tensile Testing ◽  
Weld Zone ◽  
Alloy 800H ◽  
Weld Joints ◽  
Heat Treated ◽  
Friction Weld

This study evaluated the microstructure, grain size, and mechanical properties of the alloy 800H rotary friction welds in as-welded and post-weld heat-treated conditions. The standards for the alloy 800H not only specify the composition and mechanical properties but also the minimum grain sizes. This is because these alloys are mostly used in creep resisting applications. The dynamic recrystallization of the highly strained and plasticized material during friction welding resulted in the fine grain structure (20 ± 2 µm) in the weld zone. However, a small increase in grain size was observed in the heat-affected zone of the weldment with a slight decrease in hardness compared to the base metal. Post-weld solution heat treatment (PWHT) of the friction weld joints increased the grain size (42 ± 4 µm) in the weld zone. Both as-welded and post-weld solution heat-treated friction weld joints failed in the heat-affected zone during the room temperature tensile testing and showed a lower yield strength and ultimate tensile strength than the base metal. A fracture analysis of the failed tensile samples revealed ductile fracture features. However, in high-temperature tensile testing, post-weld solution heat-treated joints exhibited superior elongation and strength compared to the as-welded joints due to the increase in the grain size of the weld metal. It was demonstrated in this study that the minimum grain size requirement of the alloy 800H friction weld joints could be successfully met by PWHT with improved strength and elongation, especially at high temperatures.

Application of Tailored Heat Treated Blanks under Quasi Series Conditions

2007 ◽  
Vol 344 ◽  
pp. 383-390 ◽  
Author(s):  
Marion Merklein ◽  
Uwe Vogt
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Local Heat ◽  
Strength Distribution ◽  
Process Window ◽  
Short Term ◽  
Forming Process ◽  
Heat Treated ◽  
Set Up ◽  
The Impact

Tailored Heat Treated Blanks (THTB) are blanks that exhibit locally different strength specifically optimized for the succeeding forming process. The strength distribution is set by a local, short-term heat treatment modifying the mechanical properties of the material. Hence, THTB allow enhancing forming limits significantly leading to shorter and more robust manufacture process chains. In order to qualify the use of THTB under quasi series conditions, the interdependencies of the blank’s local heat treatment and the entire process chain of the car body manufacture have to be analyzed. In this respect, the impact of a short-term heat treatment on the mechanical properties of AA6181PX, a commonly used aluminum alloy in today’s car bodies, was studied. Also the influence of a short-term heat treatment on the coil lubricant, usually already applied by the material supplier, was given a closer look. Based on these experiments process restrictions for the application of THTB in an industrial automotive environment were derived and a process window for the THTB design was set up. In conclusion, strategies were defined how to enhance the found process boundaries leading to a more robust process window.

A Study of the Influence of Local Heat Treatment on the Structure of Welded Titanium Pipelines

2021 ◽  
Vol 410 ◽  
pp. 37-41
Author(s):  
Natalia A. Astafeva ◽  
Andrey A. Balanovskiy ◽  
Anna A. Pershina
Keyword(s):  
Heat Treatment ◽  
Residual Stresses ◽  
Titanium Alloys ◽  
Welded Joints ◽  
Treatment Method ◽  
Local Heat ◽  
Optical Metallography ◽  
Heat Treated ◽  
Weld Structure ◽  
Heat Treatment Method

The article analyzes the results of a study of the influence of zonal heat treatment on the structure of welded joints of pipeline elements made of titanium alloys Ti-3.5Al-1.5Mn. In the manufacture of such structures, the TIG welding method is used to join pipe elements, after which the heat treatment method can be used to relieve residual stresses. The experiments have confirmed the effectiveness of zonal heat treatment preceded by welding. It was revealed that for welded joints made of titanium alloys, heat treatment can stabilize the structure. In experiments conducted by the method of optical metallography, the structure of heat treated and untreated welded joints was investigated. The influence of heat treatment on the weld structure and heat-affected zone was identified.

Effect of heat treatment on mechanical properties of 3D printed polylactic acid parts

2021 ◽  
Vol 63 (1) ◽  
pp. 73-78
Author(s):  
Pulkin Gupta ◽  
Sudha Kumari ◽  
Abhishek Gupta ◽  
Ankit Kumar Sinha ◽  
Prashant Jindal
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Polylactic Acid ◽  
Recrystallization Temperature ◽  
Fused Deposition Modelling ◽  
Fused Deposition ◽  
Dog Bone ◽  
Heat Treated ◽  
Maximum Decrease ◽  
3D Printed

Abstract Fused deposition modelling (FDM) is a layer-by-layer manufacturing process type of 3D-printing (3DP). Significant variation in the mechanical properties of 3D printed specimens is observed because of varied process parameters and interfacial bonding between consecutive layers. This study investigates the influence of heat treatment on the mechanical strength of FDM 3D printed Polylactic acid (PLA) parts with constant 3DP parameters and ambient conditions. To meet the objectives, 7 sets, each containing 5 dog-bone shaped samples, were fabricated from commercially available PLA filament. Each set was subjected to heat treatment at a particular temperature for 1 h and cooled in the furnace itself, while one set was left un-treated. The temperature for heat treatment (Th) varied from 30 °C to 130 °C with increments of 10 °C. The heat-treated samples were characterized under tensile loading of 400 N and mechanical properties like Young’s modulus (E), Strain % ( ε ) and Stiffness (k) were evaluated. On comparing the mechanical properties of heat-treated samples to un-treated samples, significant improvements were observed. Heat treatment also altered the geometries of the samples. Mechanical properties improved by 4.88 % to 10.26 % with the maximum being at Th of 110 °C and below recrystallization temperature (Tr) of 65 °C. Deformations also decreased significantly at higher temperatures above 100 °C, by a maximum of 36.06 %. The dimensions of samples showed a maximum decrease of 1.08 % in Tr range and a maximum decrease of 0.31 % in weight at the same temperature. This study aims to benefit the society by establishing suitable Th to recover the lost strength in PLA based FDM 3D printed parts.

Influence of Heat Treatment on Microstrudture and Mechanical Properties of AZ31B Magnesium Alloy Prepared by Solid-State Recycling

2012 ◽  
Vol 271-272 ◽  
pp. 17-20
Author(s):  
Shu Yan Wu ◽  
Ze Sheng Ji ◽  
Chun Ying Tian ◽  
Ming Zhong Wu
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Solid State ◽  
Magnesium Alloy ◽  
Static Recrystallization ◽  
Annealing Treatment ◽  
Az31b Magnesium Alloy ◽  
Heat Treated ◽  
Elongation To Failure ◽  
Strength And Ductility

This work is to study the influence of heat treatment on microstrudture and mechanical properties of AZ31B magnesium alloy prepared by solid -state recycling. AZ31B magnesium alloy chips were recycled by hot extruding. Three different heat treatments were conducted for recycled alloy. Mechanical properties and microstructure of the recycled specimen and heat treated specimen were investigated. 300°C×2h annealing specimen exhibits finer grain due to static recrystallization, and microstructure of 400°C×2h annealing specimen becomes more coarse. 300°C×2h annealing treatment improves obviously strength and ductility of recycled alloy. Ultimate tensile strength of alloy decreases and elongation to failure increases after 400°C×2h annealing. Grain size, dislocation density and bonding of chips have an effect on the elongation of recycled materials. 190°C×8h ageing has no influence on microstructure and mechanical properties of recycled alloy.

scholarly journals Electron Beam Melting of Ti-6Al-4V Lattice Structures; Correlation between Post Heat Treatment and Mechanical Properties

2021 ◽  
Author(s):  
Giuseppe Del Guercio ◽  
Manuela Galati ◽  
Abdollah Saboori
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Computer Aided Design ◽  
Mechanical Performance ◽  
Industrial Applications ◽  
Heat Treatments ◽  
Layer By Layer ◽  
Lattice Structures ◽  
Heat Treated ◽  
Aided Design

Abstract Additive Manufacturing processes are considered advanced manufacturing methods. It would be possible to produce complex shape components from a Computer-Aided Design model in a layer-by-layer manner. Lattice structures as one of the complex geometries could attract lots of attention for both medical and industrial applications. In these structures, besides cell size and cell type, the microstructure of lattice structures can play a key role in these structures' mechanical performance. On the other hand, heat treatment has a significant influence on the mechanical properties of the material. Therefore, in this work, the effect of the heat treatments on the microstructure and mechanical behaviour of Ti-6Al-4V lattice structures manufactured by EBM was analyzed. The main mechanical properties were compared with the Ashby and Gibson model. It is very interesting to notice that a more homogeneous failure mode was found for the heat-treated samples. The structures' relative density was the main factor influencing their mechanical performance of the heat-treated samples. It is also found that the heat treatments were able to preserve the stiffness and the compressive strength of the lattice structures. Besides, an increment of both the elongation at failure and the absorbed energy was obtained after the heat treatments. Microstructure analysis of the heat-treated samples confirms the increment of ductility of the heat-treated samples with respect to the as-built one.

scholarly journals PROPERTIES OF PARTICLEBOARD PANELS MADE OF SUGARCANE PARTICLES WITH AND WITHOUT HEAT TREATMENT

2019 ◽  
Vol 43 (5) ◽  
Author(s):  
Emerson Gomes Milagres ◽  
Raiana Augusta Grandal Savino Barbosa ◽  
Karine Fernandes Caiafa ◽  
Gabriel Soares Lopes Gomes ◽  
Tatiana Aurora Condezo Castro ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Sugarcane Bagasse ◽  
Linear Expansion ◽  
Basic Density ◽  
Water Vapor Adsorption ◽  
Thickness Swelling ◽  
Specific Mass ◽  
Heat Treated ◽  
Significant Difference

ABSTRACT The objective of this work was to determine the properties of particleboard panels made of “in natura” sugarcane bagasse particles, heated at 250 °C for 5 minutes. Various particle proportions were utilized to produce the panels and their properties were compared with that of a panel made of Pinus sp. The panels were produced with 8% tannin formaldehyde adhesive, and 0.5% paraffin emulsion, being pressed at 32 kgf.cm-2 for 10 minutes at 180 ° C. It was determined the basic density of the “in natura” and heat-treated particles, their chemical composition, as well as the compression ratio necessary to obtain panels with density equal to 0.75 g.cm-3. The basic density of the panels, hygroscopic equilibrium humidity, thickness swelling, linear expansion, water vapor adsorption, modulus of elasticity and rupture, perpendicular traction, screw pullout, and Janka hardness were determined. The basic densities of Pinus particles and sugarcane bagasse without and with heat treatment were 0.46, 0.27 and 0.30 g.cm-3, respectively. The average specific mass of the panels was 0.74 g.cm-3 with no significant difference between them. Generally, panels made of sugarcane particles were less hygroscopic and dimensionally more stable than panels made of Pinus particles. However, the perpendicular tensile strength, screw pullout and Janka hardness of these panels were higher than for the Pinus panels. The heat treatment of sugarcane bagasse particles resulted in better mechanical properties of perpendicular traction and Janka hardness. In general, the panels are within the limits set by ANSI A208.1. It is therefore possible to replace panels made of Pinus particles for the ones made of sugarcane bagasse, provided that at least 25% of the particles are heat treated for 5 minutes at 250 ° C.

Characterization of Microstructure and Mechanical Properties of 6060 Aluminum Alloy Processed by ECAP

2018 ◽  
Vol 275 ◽  
pp. 81-88
Author(s):  
Monika Karoń ◽  
Marcin Adamiak
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Plastic Deformation ◽  
Aluminum Alloy ◽  
Internal Stresses ◽  
Refined Grains ◽  
Angular Pressing ◽  
Heat Treated ◽  
Evolution Of Microstructure

The purpose of this paper is to present the microstructure and mechanical behavior of 6060 aluminum alloy after intense plastic deformation. Equal Channel Angular Pressing (ECAP) was used as a method of severe plastic deformation. Before ECAP part of the samples were heat treated to remove internal stresses in the commercially available aluminium alloy. The evolution of microstructure and tensile strength were tested after 1, 3, 6 and 9 ECAP passes in annealed and non annealed states. It was found that intensely plastically deformed refined grains were present in the tested samples and exhibited increased mechanical properties. Differences were noted between samples without and after heat treatment

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