scholarly journals Dentin Bond Integrity of Filled and Unfilled Resin Adhesive Enhanced with Silica Nanoparticles—An SEM, EDX, Micro-Raman, FTIR and Micro-Tensile Bond Strength Study

Polymers ◽  
2021 ◽  
Vol 13 (7) ◽  
pp. 1093
Author(s):  
Aasem M. Alhenaki ◽  
Esra A. Attar ◽  
Abdullah Alshahrani ◽  
Imran Farooq ◽  
Fahim Vohra ◽  
...  
Keyword(s):  
Raman Spectroscopy ◽  
Bond Strength ◽  
Silica Nanoparticles ◽  
Negative Control Group ◽  
Negative Control ◽  
Tensile Bond Strength ◽  
Control Group ◽  
Mean Values ◽  
Micro Raman Spectroscopy ◽  
Dentin Adhesive

The objective of this study was to synthesize and assess unfilled and filled (silica nanoparticles) dentin adhesive polymer. Methods encompassing scanning electron microscopy (SEM)—namely, energy dispersive X-ray spectroscopy (EDX), micro-tensile bond strength (µTBS) test, Fourier transform infrared (FTIR), and micro-Raman spectroscopy—were utilized to investigate Si particles’ shape and incorporation, dentin bond toughness, degree of conversion (DC), and adhesive–dentin interaction. The Si particles were incorporated in the experimental adhesive (EA) at 0, 5, 10, and 15 wt. % to yield Si-EA-0% (negative control group), Si-EA-5%, Si-EA-10%, and Si-EA-15% groups, respectively. Teeth were set to form bonded samples using adhesives in four groups for µTBS testing, with and without aging. Si particles were spherical shaped and resin tags having standard penetrations were detected on SEM micrographs. The EDX analysis confirmed the occurrence of Si in the adhesive groups (maximum in the Si-EA-15% group). Micro-Raman spectroscopy revealed the presence of characteristic peaks at 638, 802, and 1300 cm−1 for the Si particles. The µTBS test revealed the highest mean values for Si-EA-15% followed by Si-EA-10%. The greatest DC was appreciated for the control group trailed by the Si-EA-5% group. The addition of Si particles of 15 and 10 wt. % in dentin adhesive showed improved bond strength. The addition of 15 wt. % resulted in a bond strength that was superior to all other groups. The Si-EA-15% group demonstrated acceptable DC, suitable dentin interaction, and resin tag formation.

scholarly journals Effects of adhesive drying methods to reduce aerosol generation during resin bonding on enamel bond strength

2021 ◽  
Author(s):  
Muhammet Kerim Ayar ◽  
Onder Yesil
Keyword(s):  
Bond Strength ◽  
Negative Control Group ◽  
Negative Control ◽  
Control Group ◽  
Drying Methods ◽  
Adhesive Systems ◽  
Mean Values ◽  
Aerosol Generation ◽  
Air Stream ◽  
Cotton Pellet

ABSTRACTObjectiveIn order to reduce the amount of aerosol during the use of dental adhesives, which are widely used in minimally invasive procedures, the effects of air stream-free adhesive drying methods on the enamel bond strength of resin adhesive systems were evaluated.Materials and MethodsThe four adhesive drying techniques used were an air-stream, a micro-applicator, a cotton pellet and an absorbent paper. Adhesive systems were Single Bond Universal and Optibond All-in-one. The group in which the adhesive was not dried served as the negative control group. Enamel shear bond strength was performed with a universal tester with a crosshead speed of 1 mm/min (n=12). A two-way analysis of variance and the Tukey post-hoc test were used for analysis of the SBS data.ResultsFor both adhesives, drying the adhesive with cotton pellet or micro-applicator provided a SBS mean values similar to air-stream drying, while statistically significantly lower SBS mean values were observed in the negative control group and in the absorbent paper-dry group compared to the air-drying group.ConclusionsDrying the adhesive with micro-applicator and cotton pellets creates less aerosol and thus can be used in the COVID-19 pandemic as it provides enamel bonding strength similar to air drying.CLINICAL SIGNIFICANCETo provide safer dental care during COVID-19 pandemic, it is highly recommended to use non-aerosol-generating alternatives, instead of aerosolgenerating dental procedures. In this study, we found that the aerosol generation-free methods for adhesive-drying such as cotton pellet and micro applicator drying methods provide similar enamel bonding with conventional drying method. We think that our findings will contribute to the realization of safer adhesive dentistry practice, especially during the COVID-19 pandemic.

scholarly journals Influence of Different Conditioning Treatments on The Bond Integrity of Root Dentin to rGO Infiltrated Dentin Adhesive. SEM, EDX, FTIR and MicroRaman Study

Polymers ◽  
2021 ◽  
Vol 13 (10) ◽  
pp. 1555
Author(s):  
Firas Alqarawi ◽  
Mazen Alkahtany ◽  
Khalid Almadi ◽  
Afnan Gassem ◽  
Faris Alshahrani ◽  
...  
Keyword(s):  
Raman Spectroscopy ◽  
Bond Strength ◽  
Strength Test ◽  
Control Group ◽  
Micro Raman Spectroscopy ◽  
Fiber Posts ◽  
Root Canal Disinfection ◽  
Reduced Graphene ◽  
Root Dentin ◽  
Push Out

The present study aimed to synthesize and equate the mechanical properties and dentin interaction of two adhesives; experimental adhesive (EA) and 5 wt.% reduced graphene oxide rGO) containing adhesive. Scanning electron microscopy (SEM)-Energy-dispersive X-ray spectroscopy (EDX), Micro-Raman spectroscopy, push-out bond strength test, and Fourier Transform Infrared (FTIR) spectroscopy were employed to study nano-bond strength, degree of conversion (DC), and adhesive-dentin interaction. The EA was prepared, and rGO particles were added to produce two adhesive groups, EA-rGO-0% (control) and rGO-5%. The canals of sixty roots were shaped and prepared, and fiber posts were cemented. The specimens were further alienated into groups based on the root canal disinfection technique, including 2.5% sodium hypochlorite (NaOCl), Photodynamic therapy (PDT), and ER-CR-YSGG laser (ECYL). The rGO nanoparticles were flake-shaped, and EDX confirmed the presence of carbon (C). Micro-Raman spectroscopy revealed distinct peaks for graphene. Push-out bond strength test demonstrated highest values for the EA-rGO-0% group after NaOCl and PDT conditioning whereas, rGO-5% showed higher values after ECYL conditioning. EA-rGO-0% presented greater DC than rGO-5% adhesive. The rGO-5% adhesive demonstrated comparable push-out bond strength and rheological properties to the controls. The rGO-5% demonstrated acceptable DC (although lower than control group), appropriate dentin interaction, and resin tag establishment.

Hepatoprotective Role of AV/LCP/18 In CCl4 Induced FLKS Syndrome in Commercial Broilerst

2016 ◽  
Vol 12 (2) ◽  
Author(s):  
P. M. Sonkusale ◽  
Pratik N. Inglepatil ◽  
Siddharth V. Jamadade
Keyword(s):  
Body Weight ◽  
Treatment Group ◽  
Protein Profile ◽  
Negative Control Group ◽  
Positive Control ◽  
Negative Control ◽  
Control Group ◽  
Broiler Chicks ◽  
Mean Values ◽  
Group B

A total of 75 day old broiler chicks were divided into three equal groups. Group A served as negative control. Group B (positive control) and C (treatment group) were intoxicated with oral administration of CCl4 @ 1 ml/kg body weight after every 3rd day during 15-28 days of age. Group C was given AV/LCP/18 @ 0.10 ml / chick / day in drinking water during 29th-42nd day of age. At the end of experiment, significantly (P is less than 0.01) higher mean body weight and lower FCR was observed in treatment group C as compared to positive control group B. Similarly, significantly (P is less than 0.05) decreased levels of SGOT, SGPT, cholesterol, triglycerides, creatinine and higher mean values of serum protein profile along with mild degenerative changes in liver and kidney of broilers in group C were observed as compared to group B indicating therapeutic efficacy of AV/LCP/18 in ameliorating the toxic effects or FLKS induced by CCl4 in commercial broilers

scholarly journals Comparative Study of the Bioactivity of Two Bioceramic Materials

2018 ◽  
Vol 21 (2) ◽  
pp. 73-81
Author(s):  
Margarita Trujillo-Hernández ◽  
Rebeca E. Flores-Ventura ◽  
Angélica Suárez-Porras MSc ◽  
Leandro García-González PhD ◽  
Julián Hernández-Torres PhD ◽  
...  
Keyword(s):  
Raman Spectroscopy ◽  
Calcium Phosphate ◽  
Negative Control Group ◽  
Positive Control ◽  
Negative Control ◽  
Control Group ◽  
Carbonated Apatite ◽  
Human Dentine ◽  
Group 2 ◽  
Group 1

Calcium silicate-based materials have been shown to be bioactive due to their ability to produce biologically compatible carbonated apatite. The objective of this study was to analyze the bioactivity of Biodentine ™ and MTA Repair HP® in contact with human dentine discs, which were sealed and divided randomly to form four groups: group 1 Biodentine™, group 2 MTA Repair HP®, positive control group MTA Angelus® and negative control group IRM®, which were incubated in PBS solution for 10 days, for a subsequent analysis by means of MEB-EDS and Raman spectroscopy. The three calcium-based materials analyzed in this study proved to be bioactive because upon contact with a phosphate-based solution they were triggered at the onset of amorphous calcium phosphate, as the precursor during the formation of carbonated apatite.

scholarly journals Effects of two different sealer material on fiber post bond strength in root canal

2016 ◽  
Vol 1 (1) ◽  
pp. 31
Author(s):  
Kurniawaty Kurniawaty ◽  
Christine A. Rovani ◽  
Juni J. Nugroho ◽  
Nurhayaty Natsir ◽  
Indrya K. Mattulada
Keyword(s):  
Bond Strength ◽  
Epoxy Resin ◽  
Root Canal ◽  
Testing Machine ◽  
Negative Control Group ◽  
Negative Control ◽  
Control Group ◽  
Fiber Post ◽  
Single Root ◽  
Gutta Percha

This study was aimed to determine the effect of epoxy resin-based and MTA-based sealer on fiber post bond strength in the root canal wall.Samples are mandibulary first premolar, with a single root canal. They are divided into three groups: negative control group which is a gutta percha obturation without sealer, gutta percha obturation with epoxy resin based sealer [AH Plus], and gutta percha obturation with MTA-based sealer [MTA Fillapex] groups. Samples were decoronated, prepared, obturated and then stored in the incubator at room temperature for one week, the post space were prepared for fiber post insertion. Samples were mounted in the PVC pipes before insertion. Samples were stored in the incubator for one day before bond strength testing. Universal testing machine was used with the speed of 0,5 mm/minutes. Data were collected and analysed using ANOVA.The result showed that the fiber post bond strength in the root canal obturated with epoxy resin-based sealer was higher [12.311 N/mm2] than MTA-based sealer [10.786 N/mm2], but that result was not statistically significant. Therefore, it was concluded that the root canal obturated with epoxy resin-based sealer did not yield a significant bond strength [p = 0.689] compared to MTA-based sealer [p> 0.05].

scholarly journals Effects of two different sealer material on fiber post bond strength in root canal

2016 ◽  
Vol 1 (1) ◽  
pp. 29
Author(s):  
Kurniawaty Kurniawaty ◽  
Christine A. Rovani ◽  
Juni Jekti Nugroho ◽  
Nurhayaty Natsir ◽  
Indrya K. Mattulada
Keyword(s):  
Bond Strength ◽  
Epoxy Resin ◽  
Root Canal ◽  
Testing Machine ◽  
Negative Control Group ◽  
Negative Control ◽  
Control Group ◽  
Fiber Post ◽  
Single Root ◽  
Gutta Percha

<p>This study was aimed to determine the effect of epoxy resin-based and MTA-based sealer on fiber post bond strength in the root canal wall.Samples are mandibulary first premolar, with a single root canal. They are divided into three groups: negative control group which is a gutta percha obturation without sealer, gutta percha obturation with epoxy resin based sealer [AH Plus], and gutta percha obturation with MTA-based sealer [MTA Fillapex] groups. Samples were decoronated, prepared, obturated and then stored in the incubator at room temperature for one week, the post space were prepared for fiber post insertion. Samples were mounted in the PVC pipes before insertion. Samples were stored in the incubator for one day before bond strength testing. Universal testing machine was used with the speed of 0,5 mm/minutes. Data were collected and analysed using ANOVA.The result showed that the fiber post bond strength in the root canal obturated with epoxy resin-based sealer was higher [12.311 N/mm<sup>2</sup>] than MTA-based sealer [10.786 N/mm<sup>2</sup>], but that result was not statistically significant. Therefore, it was concluded that the root canal obturated with epoxy resin-based sealer did not yield a significant bond strength [p = 0.689] compared to MTA-based sealer [p&gt; 0.05].</p>

scholarly journals Influence of ER-CR-YSGG Laser and Photodynamic Therapy on the Dentin Bond Integrity of Nano-Hydroxyapatite Containing Resin Dentin Adhesive: SEM-EDX, Micro-Raman, Micro-Tensile, and FTIR Evaluation

Polymers ◽  
2021 ◽  
Vol 13 (12) ◽  
pp. 1903
Author(s):  
Abdullah S. Aljamhan ◽  
Mohammad H. Alrefeai ◽  
Alhanouf Alhabdan ◽  
Sarah A. Alhusseini ◽  
Imran Farooq ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Raman Spectroscopy ◽  
Photodynamic Therapy ◽  
Bond Strength ◽  
X Ray ◽  
Micro Raman Spectroscopy ◽  
Calcium And Phosphorus ◽  
Scanning Electron ◽  
Dentin Adhesive

The study aimed to analyze the effect of the addition of nano-hydroxyapatite (nano-HA) particles on the mechanical properties of experimental adhesive (EA). Furthermore, dentin interaction of EA (without nano-HA) and EA with nano-HA (hereon referred to as HA-10%) were also investigated and equated. Methods consisting of scanning electron microscopy (SEM)–energy-dispersive X-ray spectroscopy (EDX), micro-Raman spectroscopy, micro-tensile bond strength (µTBS) test, and Fourier transform infrared (FTIR) spectroscopy were employed to study nano-HA particles shape, dentin bond strength, degree of conversion (DC), and adhesive–dentin interaction. Ninety teeth (N = 90) were collected, and pre-bonding, conditioning of dentin was performed utilizing phosphoric acid (H3PO4) etching, photodynamic therapy (PDT), and ER-CR-YSGG (ECY) laser. The teeth were set to form bonded specimens using two adhesives. Nano-HA particles were spherical-shaped, and EDX confirmed the presence of oxygen, calcium, and phosphorus. Micro-Raman spectroscopy revealed distinct phosphate and carbonate peaks for nano-HA. The µTBS test demonstrated highest values for HA-10% group on the H3PO4 conditioned dentin. The greatest DC was observed for the EA group. The addition of nano-HA-10 wt.% particles in dentin adhesive resulted in improved bond strength. The incorporation also demonstrated acceptable DC (although lower than EA group), suitable dentin interaction, and resin tag formation.

scholarly journals Tooth discoloration induced by calcium-silicate-based pulp-capping materials

2015 ◽  
Vol 09 (02) ◽  
pp. 165-170 ◽  
Author(s):  
Da-A Yun ◽  
Su-Jung Park ◽  
Seok-Ryun Lee ◽  
Kyung-San Min
Keyword(s):  
Calcium Silicate ◽  
Repeated Measures ◽  
Negative Control Group ◽  
Negative Control ◽  
Control Group ◽  
Blood Contamination ◽  
Mean Values ◽  
Pulp Capping ◽  
Tooth Discoloration

ABSTRACT Objectives: The aim of this study was to evaluate tooth discoloration induced by contact with various calcium silicate-based pulp capping materials in the presence or absence of blood in vitro. Materials and Methods: Eighty bovine samples were divided into six experimental groups and two control groups according to the type of material used (ProRoot [PR], Endocem [EC], or EndocemZr [ECZ]) and the presence or absence of contamination with blood. A spectrophotometer was used to calculate the color difference (ΔE) between the baseline measurement (after placement of materials) and measurements taken 1, 2, 4, and 8 weeks. The results were analyzed with repeated measures analysis of variance, Tukey's post-hoc tests and independent t-tests (P = 0.05). Results: The PR group and EC group showed significantly higher mean values of ΔE than the negative control group after 2 weeks (P < 0.05), whereas ECZ did not. There were larger ΔE values when there was contact with blood, especially in PR and EC group (P < 0.05). Conclusions: ECZ which contains zirconium oxide as a radiopacifier showed less discoloration irrespective of blood contamination compared to PR and EC.

scholarly journals Effect of Varying Working Distances between Sandblasting Device and Composite Substrate Surface on the Repair Bond Strength

Materials ◽  
2021 ◽  
Vol 14 (7) ◽  
pp. 1621
Author(s):  
Phoebe Burrer ◽  
Amanda Costermani ◽  
Matej Par ◽  
Thomas Attin ◽  
Tobias T. Tauböck
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Substrate Surface ◽  
Negative Control Group ◽  
Positive Control ◽  
Negative Control ◽  
Positive Control Group ◽  
Control Group ◽  
Composite Substrate ◽  
Mechanical Surface

This study investigates the effect of defined working distances between the tip of a sandblasting device and a resin composite surface on the composite–composite repair bond strength. Resin composite specimens (Ceram.x Spectra ST (HV); Dentsply Sirona, Konstanz, Germany) were aged by thermal cycling (5000 cycles, 5–55 °C) and one week of water storage. Mechanical surface conditioning of the substrate surfaces was performed by sandblasting with aluminum oxide particles (50 µm, 3 bar, 10 s) from varying working distances of 1, 5, 10, and 15 mm. Specimens were then silanized and restored by application of an adhesive system and repair composite material (Ceram.x Spectra ST (HV)). In the negative control group, no mechanical surface pretreatment or silanization was performed. Directly applied inherent increments served as the positive control group (n = 8). After thermal cycling of all groups, microtensile repair bond strength was assessed, and surfaces were additionally characterized using scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDX). The negative control group reached the significantly lowest microtensile bond strength of all groups. No significant differences in repair bond strength were observed within the groups with varying sandblasting distances. Composite surfaces sandblasted from a distance of 1 mm or 5 mm showed no difference in repair bond strength compared to the positive control group, whereas distances of 10 or 15 mm revealed significantly higher repair bond strengths than the inherent incremental bond strength (positive control group). In conclusion, all sandblasted test groups achieved similar or higher repair bond strength than the inherent incremental bond strength, indicating that irrespective of the employed working distance between the sandblasting device and the composite substrate surface, repair restorations can be successfully performed.

Effect of HylocereusPolyrhizus Rind Extract Toward Interleukin-1β, Vascular Endothelial Growth Factor Expression, Endometriosis Implant Area

2017 ◽  
Vol 9 (08) ◽  
Author(s):  
YanuarEka P. ◽  
Hendy Hendarto ◽  
Widjiati .
Keyword(s):  
Vascular Endothelial Growth Factor ◽  
Growth Factor ◽  
Treatment Group ◽  
Negative Control Group ◽  
Negative Control ◽  
Control Group ◽  
Vascular Endothelial ◽  
Mice Model ◽  
Endothelial Growth Factor ◽  
Fruit Rind

Retrograde menstruation lead to I Kappa B Kinase (IKK) fosforilation in peritoneum macrophage and cause secretion of proinflammatory cytokine interleukin1β then stimulate endometriosis cell to produce Vascular Endothelial Growth Factor which lead to increasing of endometriosis lession seen as endometriosis implant area. Cytokine secretion was inhibited through prevention of NF-κB activation by dragon red fruit rind extract (Hylocereuspolyrhizus). The aim of this reserach is to know the effect of dragon red fuit rind extract with 0,25; 0,5; and 1 mg/g bodyweight dosage toward IL-1β, VEGF expression and implant area in endometriosis mice model. The design of this experiment was randomized post test only control group design.Endometrios mice model were made in 14 days and split into two group, positive control group and treatment group after two week negative control group and postive control group were given Na-CMC 0,5% solution consequetively, and treatment group were given dragon red fruit extract with different dosage. Signification number for IL-1β is p>0,05, signification number for VEGF is p>0,05, and implant area signification number is p>0,05. Administration of dragon red fruit rind extract can decrease IL-1β, VEGF, and implant area.

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