Preparation and Features of Nano-ZrO2 / HA Coating on Surface of Titanium Materials in Dental-Implant

2011 ◽  
Vol 295-297 ◽  
pp. 491-495
Author(s):  
Xiao Feng Pang ◽  
Yong Huang ◽  
Xian Yu Cao
Keyword(s):  
Composite Coating ◽  
Dental Implant ◽  
Titanium Surface ◽  
Double Layers ◽  
Ionic Form ◽  
Zirconia Coating ◽  
Coating Materials ◽  
Zirconium Oxides ◽  
Ha Coating ◽  
Titanium Surfaces

The nano-hydroxyapatite/zirconia coating of double layers on surface of titanium allay materials have been prepared using electrochemical method. The features and structures of the composite coating materials are studied and analyzed by the Scanning electron microscope (SEM) and EDAX measurement. The results show that nano-HA/ZrO2 are densely and uniformly deposited on the surface of titanium allays in ionic form, a stable gradient composite coating, in which the nano-zirconium oxides (ZrO2) are homogeneously distributed between HA and titanium surfaces, are obtained. The tensile strength experiment exhibits that the adhesion or combined strength of the coating with the titanium surface is higher and about 17GPa, which manifests the nano-HA/ ZrO2 coating is successfully combined on the surface of the titanium allay materials. The biological experiments represent that this material can be used in repairing of bone and medical dental- implant of teeth.

scholarly journals Long-lasting renewable antibacterial porous polymeric coatings enable titanium biomaterials to prevent and treat peri-implant infection

2021 ◽  
Vol 12 (1) ◽  
Author(s):  
Shuyi Wu ◽  
Jianmeng Xu ◽  
Leiyan Zou ◽  
Shulu Luo ◽  
Run Yao ◽  
...  
Keyword(s):  
Dental Implant ◽  
Pathogenic Bacteria ◽  
Titanium Surface ◽  
Polymeric Coating ◽  
Antibacterial Efficacy ◽  
Polymeric Coatings ◽  
Implant Infection ◽  
Titanium Surfaces

AbstractPeri-implant infection is one of the biggest threats to the success of dental implant. Existing coatings on titanium surfaces exhibit rapid decrease in antibacterial efficacy, which is difficult to promisingly prevent peri-implant infection. Herein, we report an N-halamine polymeric coating on titanium surface that simultaneously has long-lasting renewable antibacterial efficacy with good stability and biocompatibility. Our coating is powerfully biocidal against both main pathogenic bacteria of peri-implant infection and complex bacteria from peri-implantitis patients. More importantly, its antibacterial efficacy can persist for a long term (e.g., 12~16 weeks) in vitro, in animal model, and even in human oral cavity, which generally covers the whole formation process of osseointegrated interface. Furthermore, after consumption, it can regain its antibacterial ability by facile rechlorination, highlighting a valuable concept of renewable antibacterial coating in dental implant. These findings indicate an appealing application prospect for prevention and treatment of peri-implant infection.

Preparation of Bioactive Hydroxyapatite on Pure Titanium

2009 ◽  
Vol 24 (1_suppl) ◽  
pp. 169-182 ◽  
Author(s):  
Wang Tianshi ◽  
Zhang Renji ◽  
Yan Yongnian
Keyword(s):  
Titanium Surface ◽  
Pure Titanium ◽  
Cell Counting ◽  
Cell Compatibility ◽  
Ha Coating ◽  
Micro Arc Oxidation ◽  
Surface Metal ◽  
Titanium Surfaces ◽  
Better Than ◽  
Complex Oxidation

In this study, a hydroxyapatite (HA) was coated on a pure titanium surface by means of a complex oxidation and hydrothermal treatment. First an anodic oxidation was done on the titanium plates, followed by micro-arc oxidation. The HA-coated specimens and pure titanium specimens were immersed in SLB for 1, 5, and 10 days, respectively, to study their electrochemical behavior. The corrosion currents of HA-coated specimens were less than pure titanium specimens. This indicated that HA coating prevented surface metal ions of the implant from dissolving, thereby, reducing the tissue toxicity. The cytotoxic effect on fibroblasts L929 cells was measured by cell counting after being seeded for 2, 4, 8, 12, and 24 h. The number of surface cell attachments on the HA-coated specimens was much greater than on pure titanium specimens. The morphology of the cells on the HA coating had normal shapes and spread well with some cells climbing onto surface pores while cells on the pure titanium were oval shaped. The results confirm that the cell compatibility on HA-coated ion titanium surfaces is much better than pure titanium.

scholarly journals UV Light-Generated Superhydrophilicity of a Titanium Surface Enhances the Transfer, Diffusion and Adsorption of Osteogenic Factors from a Collagen Sponge

2021 ◽  
Vol 22 (13) ◽  
pp. 6811
Author(s):  
Masako Tabuchi ◽  
Kosuke Hamajima ◽  
Miyuki Tanaka ◽  
Takeo Sekiya ◽  
Makoto Hirota ◽  
...  
Keyword(s):  
Dental Implant ◽  
Titanium Surface ◽  
Uv Light ◽  
Active Material ◽  
Pure Titanium ◽  
Weight Ratio ◽  
Collagen Sponge ◽  
Uv Treatment ◽  
Titanium Surfaces ◽  
Osteogenic Factors

It is a significant challenge for a titanium implant, which is a bio-inert material, to recruit osteogenic factors, such as osteoblasts, proteins and blood effectively when these are contained in a biomaterial. The objective of this study was to examine the effect of ultraviolet (UV)-treatment of titanium on surface wettability and the recruitment of osteogenic factors when they are contained in an atelocollagen sponge. UV treatment of a dental implant made of commercially pure titanium was performed with UV-light for 12 min immediately prior to the experiments. Superhydrophilicity on dental implant surfaces was generated with UV-treatment. The collagen sponge containing blood, osteoblasts, or albumin was directly placed on the dental implant. Untreated implants absorbed only a little blood from the collagen sponge, while the UV-treated implants absorbed blood rapidly and allowed it to spread widely, almost over the entire implant surface. Blood coverage was 3.5 times greater for the UV-treated implants (p < 0.001). Only 6% of the osteoblasts transferred from the collagen sponge to the untreated implants, whereas 16% of the osteoblasts transferred to the UV-treated implants (p < 0.001). In addition, a weight ratio between transferred albumin on the implant and measured albumin adsorbed on the implant was 17.3% in untreated implants and 38.5% in UV-treated implants (p < 0.05). These results indicated that UV treatment converts a titanium surface into a superhydrophilic and bio-active material, which could recruite osteogenic factors even when they were contained in a collagen sponge. The transfer and subsequent diffusion and adsorption efficacy of UV-treated titanium surfaces could be useful for bone formation when titanium surfaces and osteogenic factors are intervened with a biomaterial.

scholarly journals Graphene-Doped Poly (Methyl-Methacrylate) (Pmma) Implants: A Micro-CT and Histomorphometrical Study in Rabbits

2021 ◽  
Vol 22 (3) ◽  
pp. 1441
Author(s):  
Antonio Scarano ◽  
Tiziana Orsini ◽  
Fabio Di Carlo ◽  
Luca Valbonetti ◽  
Felice Lorusso
Keyword(s):  
Methyl Methacrylate ◽  
Dental Implant ◽  
Animal Studies ◽  
White Male ◽  
Biological Response ◽  
Medullary Canal ◽  
Poly Methyl Methacrylate ◽  
Titanium Surfaces ◽  
Dental Applications

Background—the graphene-doping procedure represents a useful procedure to improve the mechanical, physical and biological response of several Polymethyl methacrylate (PMMA)-derived polymers and biomaterials for dental applications. The aim of this study was to evaluate osseointegration of Graphene doped Poly(methyl methacrylate) (GD-PMMA) compared with PMMA as potential materials for dental implant devices. Methods—eighteen adult New Zealand white male rabbits with a mean weight of approx. 3000 g were used in this research. A total of eighteen implants of 3.5 mm diameter and 11 mm length in GD-PMMA and eighteen implants in PMMA were used. The implants were placed into the articular femoral knee joint. The animals were sacrificed after 15, 30 and 60 days and the specimens were evaluated by µCT and histomorphometry. Results—microscopically, all 36 implants, 18 in PMMA and 18 in DG-PMMA were well-integrated into the bone. The implants were in contact with cortical bone along the upper threads, while the lower threads were in contact with either newly formed bone or with marrow spaces. The histomorphometry and µCT evaluation showed that the GP-PMMA and PMMA implants were well osseointegrated and the bone was in direct contact with large portions of the implant surfaces, including the space in the medullary canal. Conclusions—in conclusion, the results suggest that GD-PMMA titanium surfaces enhance osseointegration in rabbit femurs. This encourages further research to obtain GD-PMMA with a greater radiopacity. Also, further in vitro and vivo animal studies are necessary to evaluate a potential clinical usage for dental implant applications.

Fabrication of a Composite Coating by Laser, Nanoparticles Self-Assembly and Electrodeposition

2021 ◽  
Vol 1032 ◽  
pp. 84-90
Author(s):  
Ou Chuan Lin ◽  
Ying Luo Zhou ◽  
Jing Li ◽  
Virgil Bunyan
Keyword(s):  
Composite Coating ◽  
Self Assembly ◽  
Surface Coating ◽  
Laser Processing ◽  
Substrate Surface ◽  
Substrate Material ◽  
Processing Method ◽  
Coating Materials ◽  
Different Characteristics ◽  
Micro Morphology

In this paper, a composite micromachining process is introduced. By adjusting the surface microstructure, a composite coating with two kinds of materials with different characteristics was fabricated. Carbon steel is used as the substrate material, and laser processing is used to obtain the micro morphology on the substrate surface. nanoSiC particles were selected as one of the coating materials, and the SiC coating was added through the process of micropore induced nanoparticles self-assembly. Ni was selected as another coating material and added by electrodeposition. This processing method can be used to prepare multifunctional surface coating, combining the characteristics of different materials. This work can provide an idea to create more excellent multifunctional surfaces.

scholarly journals Biological and antibacterial properties of the micro-nanostructured hydroxyapatite/chitosan coating on titanium

2019 ◽  
Vol 9 (1) ◽  
Author(s):  
Baoe Li ◽  
Xiaomei Xia ◽  
Miaoqi Guo ◽  
Yu Jiang ◽  
Yu Li ◽  
...  
Keyword(s):  
Composite Coating ◽  
Antibacterial Property ◽  
Antibacterial Properties ◽  
Dip Coating ◽  
Ha Coating ◽  
Coating Method ◽  
Micro Arc Oxidation ◽  
Promising Application ◽  
Sbf Solution ◽  
Dip Coating Method

Abstract Titanium (Ti) is the widely used implant material in clinic, however, failures still frequently occur due to its bioinertness and poor antibacterial property. To improve the biological and antibacterial properties of Ti implants, micro-nanostructured hydroxyapatite (HA) coating was prepared on Ti surface by micro-arc oxidation (MAO), and then the antibacterial agent of chitosan (CS) was loaded on the HA surface through dip-coating method. The results showed that the obtained HA/CS composite coating accelerated the formation of apatite layer in SBF solution, enhanced cell adhesion, spreading and proliferation, and it also inhibited the bacterial growth, showing improved biological and antibacterial properties. Although, with the increased CS amount, the coverage of HA coating would be enlarged, resulting in depressed biological property, however, the antibacterial property of the composite coating was enhanced, and the cytotoxicity about CS was not detected in this work. In conclusion, the HA/CS coating has promising application in orthopedics, dentistry and other biomedical devices.

Microcontact Printed Protein Micropatterns on Titanium Surface Characterized by Confocal Laser Scanning Microscopy

2012 ◽  
Vol 487 ◽  
pp. 730-734 ◽  
Author(s):  
Chang Jiang Pan ◽  
Yu Dong Nie ◽  
Yun Xiao Dong
Keyword(s):  
Laser Scanning ◽  
Photoelectron Spectrum ◽  
Titanium Surface ◽  
Microcontact Printing ◽  
Laser Scanning Microscopy ◽  
Confocal Laser ◽  
Water Contact ◽  
X Ray ◽  
Replication Errors ◽  
Titanium Surfaces

In this paper, two kinds of stamps (squares (a×a)) separated by spacing b, the values of a and b were varied from 2.5 µm to 50 µm), i.e. positive and negative stamps, were prepared. The stamps inked with the rhodamine-labeled bovine serum albumin (BSA) were then microcontacted with the aldehyde-functionalized titanium surfaces. Water contact angle and X-ray photoelectron spectrum (XPS) indicated that BSA can be covalently immobilized on aldehyde modified titanium surface by microcontact printing. The experimental results of CLSM showed that the patterns with resolution from 2.5 µm to 50 µm were obtained successfully. Both positive stamp and negative stamp were deformed when the value of a was less than or equal to 5 µm, which resulted in replication errors. Furthermore, the larger spacing (50 µm) resulted in stamp collapse when the value a of the positive stamp was less than or equal to 10 µm, leading to whole fluorescence on substrates.

Novel Method for Hydroxyapatite Coating by Hydrothermal Hot-Pressing via Double Layered Capsule

2006 ◽  
Vol 309-311 ◽  
pp. 647-650 ◽  
Author(s):  
Takamasa Onoki ◽  
Toshiyuki Hashida
Keyword(s):  
Coating Layer ◽  
Hydrothermal Condition ◽  
Confining Pressure ◽  
Ceramic Coatings ◽  
Coating Materials ◽  
Adhesion Properties ◽  
Pull Out ◽  
Ha Coating ◽  
Outer Capsule ◽  
Novel Method

A new hydrothermal method is proposed which enables us to prepare thin hydroxyapatite (HA) ceramic coatings on Ti substrates with a curved surface at low temperatures. The method uses double layered capsules in order to produce a suitable hydrothermal condition; the inner capsule encapsulates the coating materials and a Ti substrate, and the outer capsule is subjected to isostatic pressing under the hydrothermal condition. In this study, it is demonstrated that a pure HA ceramic layer with the thickness of 50 µm could be coated to a Ti cylindrical rod at the low temperature as low as 135°C under the confining pressure of 40 MPa. Pull-out tests were conducted to obtain an estimate for the adhesion properties of the HA coating prepared by the double layered capsule method. The shear strength obtained from the pull-out tests was in the range of 4.0-5.5 MPa. It was also shown that the crack propagation occurred within the HA coating layer, not along the HA/Ti interface in the pull-out tests.

Sign in / Sign up

Export Citation Format

Share Document