Effects of Cu on Microstructure, Mechanical Properties and Damping Capacity of As-Cast Mg-3%Ni Alloy

2012 ◽  
Vol 463-464 ◽  
pp. 52-57 ◽  
Author(s):  
Shu Qun Chen ◽  
Xuan Pu Dong ◽  
Xiao Qing Xiong ◽  
Rong Ma ◽  
Zi Tian Fan

The effects of Cu addition on microstructure, mechanical properties and damping capacity of Mg-3%Ni based alloy were investigated by using tensile tests, X-ray diffraction, scanning electron microscope and dynamic mechanical analyzer. The results show that Cu addition could reduce the size of -Mg dendrites and a new binary phase Mg2Cu can be identified, which mostly distributes among the inter-dendrites in the form of typical lamellar-like eutectic microstructure and improve the mechanical properties. In low strain amplitude, with the increase of Cu addition, the damping capacities of Cu contained alloys change little, while in high strain range, the internal friction values decrease gradually with the grain refinement and increasing content of eutectic phase.

2007 ◽  
Vol 546-549 ◽  
pp. 257-260 ◽  
Author(s):  
Zhen Yan Zhang ◽  
Li Ming Peng ◽  
Xiao Qin Zeng ◽  
Lin Du ◽  
Lan Ma ◽  
...  

Effects of extrusion on mechanical properties and damping capacity of Mg-1.8wt.%Cu -0.5wt.%Mn (MCM1805) alloy have been investigated. Tensile tests and dynamic mechanical analyzer were respectively used to measure tensile properties and damping capacity at room temperature of as-cast and as-extruded MCM1805 alloy. The microstructure was studied using optical microscope, X-ray diffraction and scanning electron microscope with an energy dispersive X-ray spectrometer. Granato-Lücke model was used to explain the influences of extrusion on damping capacity of MCM1805 alloy. The results showed that extrusion dramatically decreases the grain size but has little influence on phase composition and solute atoms concentration of MCM1805 alloy, and the grain refinement was the dominant reason for the obvious increase of tensile properties and decrease of internal friction of MCM1805 alloy.


2014 ◽  
Vol 988 ◽  
pp. 156-160
Author(s):  
Hong Wei Liu ◽  
Feng Wang ◽  
Bai Qing Xiong ◽  
Yong An Zhang ◽  
Zhi Hui Li ◽  
...  

The microstructure and mechanical properties of the Al-2.24Cu-1.42Mg-0.9Fe-0.9Ni alloy were studied using optical microscopy (OM), scanning electron microscopy (SEM), X-ray diffraction (XRD), and tensile tests. The results indicate that the microstructures of the as cast alloy involve α-Al matrix, Al/Al2CuMg eutectic structure, Al7Cu2Fe, Al7Cu4Ni and Al9FeNi compounds. The tensile test results indicate that the alloy at elevated temperature (200°C) displays superior tensile strength due to the presence of the thermally stable Al7Cu2Fe, Al7Cu4Ni and Al9FeNi compounds.


2010 ◽  
Vol 654-656 ◽  
pp. 2126-2129 ◽  
Author(s):  
Yuichi Nakahira ◽  
Tomonari Inamura ◽  
Hiroyasu Kanetaka ◽  
Shuichi Miyazaki ◽  
Hideki Hosoda

Effect of nitrogen (N) addition on mechanical properties of Ti-Cr-Sn alloy was investigated in this study. Ti-7mol%Cr-3mol%Sn was selected and less than 0.5wt% of N were systematically added. The alloys were characterized by optical microscopy, X-ray diffraction analysis and tensile tests at room temperature. The apparent phase was β (bcc) phase, whereas the presence of precipitates was confirmed in 0.5wt%N-added alloy only which did not exhibit sufficient cold workability. The grain size was not largely affected by N addition being less than 0.5wt%. Tensile tests revealed that less than 0.5wt%N addition improves the strength which is due to the solution hardening by interstitial N atoms.


2016 ◽  
Vol 682 ◽  
pp. 245-251 ◽  
Author(s):  
Grzegorz Włoch ◽  
Tomasz Skrzekut ◽  
Jakub Sobota ◽  
Antoni Woźnicki ◽  
Justyna Cisoń

Mixed and preliminarily consolidated powders of aluminium and nickel (90 mass % Al and 10 mass % Ni) were hot extruded. As results the rod, 8 mm in diameter, was obtained. As-extruded material was subjected to the microstructural investigations using scanning electron microscopy (SEM/EDS) and X-ray analysis (XRD). The differential scanning calorimetry (DSC) and thermo-mechanical analysis (TMA) were also performed. The mechanical properties of as extruded material were determined by the tensile test and Vickers hardness measurements. In order to evaluate the thermal stability of PM alloy, samples were annealed at the temperature of 475 and 550 °C. After annealing Vickers hardness measurements and tensile tests were carried out. The plastic consolidation of powders during extrusion was found to be very effective, because no pores or voids were observed in the examined material. The detailed microstructural investigations and XRD analyses did not reveal the presence of the intermetallic phases in the as-extruded material. During annealing, the Al3Ni intermetallic compound was formed as the result of chemical reaction between the alloy components. The hardness of the alloy after annealing at the temperature of 475°C was found to be comparable to the hardness in as-extruded state. Annealing of the material at the temperature of 550°C results in hardness decreasing by about 50%, as the consequence of porosity formation and Al3Ni cracking.


2018 ◽  
Vol 89 (9) ◽  
pp. 1770-1781 ◽  
Author(s):  
Huaizhong Xu ◽  
Benedict Bauer ◽  
Masaki Yamamoto ◽  
Hideki Yamane

A facile route was proposed to fabricate core–sheath microfibers, and the relationships among processing parameters, crystalline structures and the mechanical properties were investigated. The compression molded poly(3-hydroxybutyrate-co-3-hydroxyhexanoate) (PHBH)/poly(L-lactic acid) (PLLA) strip enhanced the spinnability of PHBH and the mechanical properties of PLLA as well. The core–sheath ratio of the fibers was determined by the prefab strip, while the PLLA sheath component did not completely cover the PHBH core component due to the weak interfacial tension between the melts of PHBH and PLLA. A rotational target was applied to collect aligned fibers, which were further drawn in a water bath. The tensile strength and the modulus of as-spun and drawn fibers increased with increasing the take-up velocities. When the take-up velocity was above 500 m/min, the jet became unstable and started to break up at the tip of the Taylor cone, decreasing the mechanical properties of the fibers. The drawing process facilitated the crystallization of PLLA and PHBH, and the tensile strength and the modulus increased linearly with the increasing the draw ratio. The crystal information displayed from wide-angle X-ray diffraction patterns and differential scanning calorimetry heating curves supported the results of the tensile tests.


2016 ◽  
Vol 704 ◽  
pp. 183-189
Author(s):  
Yong Jun Su ◽  
Yi Feng Zheng ◽  
De Liang Zhang ◽  
Fan Tao Kong

TiAl alloy with a composition of Ti-43Al-5V-4Nb-Y (at.%) was prepared by spark plasma sintering (SPS). The TiAl powders were sintered between 650°C and 1300°C for 5 min under different loads. With the increasing of the temperature, the diffusion of the elements can be observed. Full compaction is achieved in a short period of time and the overall processing duration does not exceed 30 min. A fully lamellar structure was seen in the TiAl alloy after heat treatment. The microstructures of the samples were determined by X-ray diffraction and scanning electron microscopy. Their mechanical properties were evaluated by tensile tests performed at room temperature


2014 ◽  
Vol 59 (1) ◽  
pp. 127-131 ◽  
Author(s):  
J. Bogucka

Abstract The influence of bonding temperature on microstructure and mechanical properties of AA5251 alloy sheets have been analyzed in the paper. The alloy was deformed with the method of accumulative roll bonding (ARB) in various temperature conditions i.e. at ambient temperature up to 5th cycle (ε = 4.0) and using pre-heating of sheet packs at 200°C and 300°C up to 10 cycles (ε = 8.0). The deformed material was subjected to structural observations using TEM, measurements of crystallographic texture with the technique of X-ray diffraction and tensile tests. It was established that the temperature of roll-bonding had a significant effect on the structure evolution and the observed changes of mechanical properties. High refinement of microstructure and optimum mechanical properties were obtained for the material processed at lower temperatures, i.e. at ambient temperature and pre-heating at 200°C. Recovery structure processes occurring during deformation were observed in the alloy bonded with pre-heating at 300°C and therefore mechanical properties were lower than for the alloy bonded at lower temperatures.


2014 ◽  
Vol 543-547 ◽  
pp. 3733-3736
Author(s):  
Rong Hua Zhang ◽  
Biao Wu ◽  
Xiao Ping Zheng

In this study, 8009 heat resistant aluminum alloy was synthesized by the spray atomization and deposition technique. The microstructure and mechanical properties of the alloy were studied using transmission electron microscopy, X-ray diffraction, and tensile tests. The secondary phases in the microstructure of the spray-deposited alloy were examined. The tensile test results indicate that the spray-deposited 8009 alloy both at room and elevated temperature displays superior tensile strength due to the presence of the thermally stable Al12(Fe,V)3Si particles.


2017 ◽  
Vol 16 (05n06) ◽  
pp. 1750012 ◽  
Author(s):  
Farhad Jahantigh ◽  
Mehdi Nazirzadeh

In this project, nanocomposite films were prepared with different Titanium dioxide (TiO2) percentages. Properties of polycarbonate (PC) and PC–TiO2nanocomposite films were studied by X-ray diffraction (XRD) analysis and Fourier transform infrared (FTIR) spectroscopy. The structure of samples was studied by XRD. The mechanical properties of PC–TiO2nanocomposite films were investigated by conducting tensile tests and hardness measurements. Thermal stability of the nanocomposites was studied by thermogravimetric analysis (TGA) method. The elastic modulus of the composite increased with increasing weight fraction of nanoparticles. The microhardness value increases with increasing TiO2nanoparticles. The results of tensile testing were in agreement with those of micro-hardness measurements. In addition, TGA curves showed that nanocomposite films have higher resistance to thermal degradation compared to polycarbonate. There are many reports related to the modification of polycarbonate films, but still a systematic study of them is required.


2006 ◽  
Vol 510-511 ◽  
pp. 214-217 ◽  
Author(s):  
Joong Hwan Jun ◽  
Bong Koo Park ◽  
Jeong Min Kim ◽  
Ki Tae Kim ◽  
Woon Jae Jung

Influences of Ca addition on microstructures and mechanical properties at room and elevated temperatures up to 300oC were investigated for ZE41 (Mg-4%Zn-1%Zn)-(0~1.0)%Ca permanent mould casting alloys, based on the results from X-ray diffractometry (XRD), scanning electron microscopy (SEM) with energy dispersive X-ray spectroscopy (EDS) and tensile tests. The microstructure of ZE41 alloy is characterized by dendritic α-(Mg) grains surrounded by Mg7Zn3-based eutectic network phase. The average size of α grains decreases continuously with an increase in Ca content. The Ca-containing ZE41 alloys have Mg7Zn3-(RE)-(Ca) eutectic phase, in which Ca is distributed inhomogeneously owing to its strong segregation power. It is noteworthy that tensile yield strength (YS) for the ZE41 alloy was enhanced with increasing Ca content at all temperatures up to 300oC, which demonstrates that Ca can play a beneficial role in improving its tensile strength at room and elevated temperatures. The ZE41 alloy with 0.5%Ca showed the highest ultimate tensile strength (UTS) at room temperature, but in the range of 175 to 300oC, the higher the Ca content, the greater the UTS. The improved tensile strength of the Ca-containing ZE41 alloy would be caused by the refined α grains and higher thermal stability of the Mg7Zn3-(RE)-(Ca) eutectic phase.


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