Influence of Direct Lamellarizing and Tempering on Microstructure and Properties of F550 Ship Plate Steel

2013 ◽  
Vol 773 ◽  
pp. 391-396
Author(s):  
Xiao Lin Li ◽  
Qing Wu Cai ◽  
Wei Yu
Keyword(s):  
Electron Microscope ◽  
Impact Energy ◽  
Bainitic Ferrite ◽  
Optical Microscope ◽  
Cleavage Crack ◽  
Plate Steel ◽  
Microstructure And Properties ◽  
Transmission Electron ◽  
Austenite Grains ◽  
The Impact

The effects of quenching at 820 °C 850 °C 940 °C and tempering at 600 °C on microstructure and properties of F550 ship plate steel were studied by optical microscope (OM), scanning electron microscope (SEM), transmission electron microscope (TEM) and other experimental methods. The results show that the highest value of the impact energy at-80 °C is 240 J when the steel is quenched at 850 °C and tempered at 600 °C. A full graumber of martensite-austenite (M-A) constituents which distribute in the shape of point-liner or gather among the grains, is larger compared with lamellarizing and tempering. Although the strength of the steel is higher, the value of the impact energy at-80 °C is lower and unstable. After intercritical quenching, the presence of minor ferrite and austenite grains refined could also be helpful to improve the low temperature toughness. Because polygonal ferrite (QF) is small and distributes uniformly between bainitic ferrite lathes acting as beneficial barriers to cleavage crack propagation.

Real-time cryo-deformation of polypropylene and impact-modified polypropylene in the transmission electron microscope

1993 ◽  
Vol 51 ◽  
pp. 892-893
Author(s):  
Robert C. Cieslinski ◽  
H. Craig Silvis ◽  
Daniel J. Murray
Keyword(s):  
Electron Microscope ◽  
Transmission Electron Microscope ◽  
Failure Mechanisms ◽  
Brittle Transition ◽  
Molded Part ◽  
Transmission Electron ◽  
Solvent Cast ◽  
The Impact ◽  
Annealed Copper ◽  
Dynamic Plane

An understanding of the mechanical behavior polymers in the ductile-brittle transition region will result in materials with improved properties. A technique has been developed that allows the realtime observation of dynamic plane stress failure mechanisms in the transmission electron microscope. With the addition of a cryo-tensile stage, this technique has been extented to -173°C, allowing the observation of deformation during the ductile-brittle transition.The technique makes use of an annealed copper cartridge in which a thin section of bulk polymer specimen is bonded and plastically deformed in tension in the TEM using a screw-driven tensile stage. In contrast to previous deformation studies on solvent-cast films, this technique can examine the frozen-in morphology of a molded part.The deformation behavior of polypropylene and polypropylene impact modified with EPDM (ethylene-propylene diene modified) and PE (polyethylene) rubbers were investigated as function of temperature and the molecular weight of the impact modifier.

Organoclay-reinforced polyethersulfone-modified epoxy-based hybrid nanocomposites

2011 ◽  
Vol 23 (7) ◽  
pp. 526-534 ◽  
Author(s):  
Yang Wang ◽  
Boming Zhang ◽  
Jinrui Ye
Keyword(s):  
Electron Microscopy ◽  
Fracture Toughness ◽  
Electron Microscope ◽  
Optical Microscope ◽  
Mechanical Analysis ◽  
Hybrid Nanocomposites ◽  
X Ray Diffraction ◽  
Transmission Electron ◽  
Modified Epoxy ◽  
Scanning Electron

Hybrid nanocomposites were successfully prepared by the incorporation of polyethersulfone (PES) and organoclay into epoxy resin. They had higher fracture toughness than the prepared PES/epoxy blend and organoclay/epoxy nanocomposites. The microstructures of the hybrid nanocomposites were studied. They were comprised of homogeneous PES/epoxy semi-interpenetrating network (semi-IPN) matrices and organoclay micro-agglomerates made up of tactoid-like regions composed of ordered exfoliated organoclay with various orientations. The former was confirmed with dynamic mechanical analysis, scanning electron microscopy and transmission electron microscopy, while the latter was successfully observed with X-ray diffraction measurements, optical microscope, scanning electron microscope and transmission electron microscope. The improvement of their fracture toughness was due to the synergistic toughening effect of the PES and the organoclay and related to their microstructures.

Effect of Heat Treatment on Microstructure and Properties of Cu-3Ti-1Al Alloy

2013 ◽  
Vol 749 ◽  
pp. 282-286
Author(s):  
Xian Hui Wang ◽  
Xiao Chun Sun ◽  
Xiao Hong Yang ◽  
Shu Hua Liang
Keyword(s):  
Heat Treatment ◽  
Solid Solution ◽  
Electrical Conductivity ◽  
Electron Microscope ◽  
Treatment Process ◽  
Intermetallic Phase ◽  
Strengthening Effect ◽  
Microstructure And Properties ◽  
Optimal Heat Treatment ◽  
Transmission Electron

The effect of heat treatment on the microstructure and properties of Cu-3Ti-1Al alloy was investigated. The microstructure was characterized by scanning electron microscope (SEM) and transmission electron microscope (TEM), and the hardness and electrical conductivity were tested as well. The results showed that the hardness and electrical conductivity of Cu-3Ti-1Al alloy increased significantly after solid solution and ageing treatment. The strengthening effect of Cu-3Ti-1Al alloy was attributed to the formation of intermetallic phase such as Ti3Al and fine precipitates of coherent β-Cu4Ti. With increase of the aging time and the temperature, the precipitates became coarse and incoherent with Cu matrix, and the discontinuous precipitate β started to grow from grain boundaries toward grain interior, which decreased hardness. As the formation of Ti3Al, β-Cu3Ti and β-Cu4Ti phase can efficiently reduce Ti concentration in Cu matrix. The electrical conductivity of Cu-3Ti-1Al alloy increases. In the range of experiments, the optimal heat treatment process for Cu-3Ti-1Al alloy is solid solution at 850°C for 4h and ageing 500°C for 2h, and the hardness and electrical conductivity are 227HV and 12.3%IACS, respectively.

scholarly journals Acceleration of Plasma Nitriding at 550 °C with Rare Earth on the Surface of 38CrMoAl Steel

Coatings ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 1122
Author(s):  
Dongjing Liu ◽  
Yuan You ◽  
Mufu Yan ◽  
Hongtao Chen ◽  
Rui Li ◽  
...  
Keyword(s):  
Rare Earth ◽  
Electron Microscope ◽  
Weight Gain ◽  
Plasma Nitriding ◽  
Nitrided Layer ◽  
Surface Hardness ◽  
Optical Microscope ◽  
Steel Microstructure ◽  
Transmission Electron ◽  
Modified Layer

In order to explore the effect of the addition of rare earth (RE) to a steel microstructure and the consequent performance of a nitrided layer, plasma nitriding was carried out on 38CrMoAl steel in an atmosphere of NH3 at 550 °C for 4, 8, and 12 h. The modified layers were characterized using an optical microscope (OM), a microhardness tester, X-ray diffraction (XRD), a scanning electron microscope (SEM), a transmission electron microscope (TEM), and an electrochemical workstation. After 12 h of nitriding without RE, the modified layer thickness was 355.90 μm, the weight gain was 3.75 mg/cm2, and the surface hardness was 882.5 HV0.05. After 12 h of RE nitriding, the thickness of the modified layer was 390.8 μm, the weight gain was 3.87 mg/cm2, and the surface hardness was 1027 HV0.05. Compared with nitriding without RE, the ε-Fe2-3N diffraction peak was enhanced in the RE nitriding layer. After 12 h of RE nitriding, La, LaFeO3, and a trace amount of Fe2O3 appeared. The corrosion rate of the modified layer was at its lowest (15.089 × 10−2 mm/a), as was the current density (1.282 × 10−5 A/cm2); therefore, the corrosion resistance improved.

Microstructure of the Acid Welding Slag

2012 ◽  
Vol 249-250 ◽  
pp. 914-917
Author(s):  
Yuan Bin Zhang ◽  
Kai Zhang
Keyword(s):  
Electron Microscope ◽  
Amorphous Matrix ◽  
Low Carbon Steel ◽  
Optical Microscope ◽  
Crystal Phase ◽  
Low Carbon ◽  
Extrusion Press ◽  
Transmission Electron ◽  
Welding Slag ◽  
Welding Electrode

Several E4303 type welding electrodes with different coating compositions were designed and manufactured using TL-25 welding electrode extrusion press. Welding slags of these electrodes were collected after welding on the low carbon steel, then the microstructure and the phase constitutes of the slags were investigated by optical microscope,scan electron microscope (SEM), electron probe microanalyzer (EPMA), Transmission electron microscope (TEM) and X-ray diffraction (XRD). It was indicated that the slags were mainly composed of amorphous matrix and Fe2MnTi3O10 crystal phase. Fe, Mn and Ti were the main elements to form the crystal phase, while Si, Al and Ca were mostly distributed in the amorphous matrix. The formation of the crystal phase in the slag could be controlled by adjusting the amount and the proportion of Fe, Mn and Ti in the welding rod coating.

Effect of Mg/Si Ratio on Hardening Behavior, Microstructure and Properties of Al-Mg-Si Alloys

2022 ◽  
Vol 905 ◽  
pp. 56-60
Author(s):  
Ya Ya Zheng ◽  
Tao Long ◽  
Bing Li
Keyword(s):  
Mechanical Properties ◽  
Electron Microscope ◽  
Transmission Electron Microscope ◽  
Intergranular Corrosion ◽  
Corrosion Test ◽  
Electrochemical Test ◽  
Microstructure And Properties ◽  
Hardening Behavior ◽  
Transmission Electron ◽  
Precipitation Behaviour

The effects of Mg/Si ratio on precipitation behaviour and properties of Al-Mg-Si alloys were studied by using electrochemical test, corrosion test and transmission electron microscope (TEM). The results show that with the increases of Mg/Si ratio from 0.9 to 1.1, the density of the β" decreases, and the mechanical properties decrease. When the ratio of Mg/Si increases from 1.0 to 1.1, the density y of β" does not increase significantly, but the continuous degree of the MgSi phase decreases significantly. The source of cracks originate from MgSi phase, which reduces the mechanical properties. When the Mg/Si ratio is 0.9, the alloy is in an over-Si state, which results in serious intergranular corrosion (IGC).

A Study of Membrane Impact on Spatial Resolution of Liquid In Situ Transmission Electron Microscope

2020 ◽  
Vol 26 (1) ◽  
pp. 126-133
Author(s):  
Ming Li ◽  
Ruth Knibbe
Keyword(s):  
Electron Microscope ◽  
Spatial Resolution ◽  
Transmission Electron Microscope ◽  
Signal To Noise Ratio ◽  
Chromatic Aberration ◽  
Membrane Thickness ◽  
Additional Material ◽  
Transmission Electron ◽  
The Impact

AbstractMicrochip technology with electron transparent membranes is a key component for in situ liquid transmission electron microscope (TEM) characterization. The membranes can significantly influence the TEM imaging spatial resolution, not only due to introducing additional material layers but also due to the associated bulging. The membrane bulging is largely defined by the membrane materials, thickness, and short dimension. The impact of the membrane on the spatial resolution, especially the extent of its bulging, was systematically investigated through the impact on the signal-to-noise ratio, chromatic aberration, and beam broadening. The optimization of the membrane parameters is the key component when designing the in situ TEM liquid cell. The optimal membrane thickness of 50 nm was found which balances the impact of membrane bulging and membrane thickness. Beyond this, the short membrane window dimension and the chip nominal spacing should be minimized. However, these two parameters have practical limitations in regards to chip handling.

The Effects of Mechanical Properties on Fatigue Behavior of ECAPed AA7075

2016 ◽  
Vol 35 (3) ◽  
pp. 225-234 ◽  
Author(s):  
Hasan Kaya ◽  
Mehmet Uçar
Keyword(s):  
Electron Microscope ◽  
Fatigue Life ◽  
Fatigue Behavior ◽  
Optical Microscope ◽  
Fatigue Tests ◽  
Angular Pressing ◽  
Four Point Bending ◽  
Selected Area Electron Diffraction ◽  
Transmission Electron ◽  
Hardness Values

AbstractIn this study, the effects of equal channel angular pressing (ECAP) on high-cycle fatigue and fatigue surface morphology of AA7075 have been investigated at a constant temperature (483 K) and the “C” route for four passes at ECAP process. ECAPed and as-received specimens were tested by four-point bending fatigue device. Fatigue tests were carried out by using 100, 120 and 140 MPa strength values. ECAPed specimens were characterized for each pass with optical microscope (OM), scanning electron microscope (SEM), energy-dispersive spectroscope (EDS), transmission electron microscope (TEM), selected area electron diffraction (SAED) and hardness measurements. Fracture surfaces of the specimens were also characterized with SEM. The results show that the highest hardness values (137 HV) and the best fatigue life (5.4 × 107for 100 MPa) were measured in ECAPed four-pass sample. For this reason hardness values and fatigue life were increased with increasing number of severe plastic deformation (SPD) process.

Metallographic Investigation on the Effect of Cryogenic Temperature on Steel Weldments

2014 ◽  
Vol 629 ◽  
pp. 456-460 ◽  
Author(s):  
S. Rasool Mohideen ◽  
Ahmad Zaidi Ahmad Mujahid ◽  
Abdullah Shohaimi ◽  
S. Ravi
Keyword(s):  
Mechanical Properties ◽  
Electron Microscope ◽  
Transmission Electron Microscope ◽  
Low Temperatures ◽  
Cryogenic Temperature ◽  
Liquid Nitrogen Temperature ◽  
Optical Microscope ◽  
Low Alloy Steel ◽  
Transmission Electron ◽  
Properties Of Materials

Materials are subjected to low temperatures either intentionally as in the case of cryogenic fuels or non-intentionally as in the case of aerospace environment and are observed to undergo changes in their properties. Microstructural changes are the premier indications of changes in the properties of materials. This paper investigates the effect of cryogenic temperature on the microstructure of low alloy steel weldments. The weldments were subjected to liquid nitrogen temperature of 77K and the microstructures were analyzed using optical microscope and transmission electron Microscope. A distinct change in the microstructure was observed which would reason out the changes in the mechanical properties of weldments.

Study on Precipitation Behavior of High Strength Steel Plate Strengthened Complexly by Titanium and Molybdenum

2011 ◽  
Vol 217-218 ◽  
pp. 812-818
Author(s):  
Hong Bin Wang ◽  
Sheng Li Li ◽  
Li Li ◽  
Peng Cheng Ma
Keyword(s):  
Electron Microscope ◽  
Steel Plate ◽  
High Strength ◽  
Optical Microscope ◽  
Steel Plates ◽  
Transmission Electron ◽  
Cold Rolled ◽  
Hot Rolled ◽  
Hot Rolled Steel ◽  
Energy Disperse Spectroscopy

The precipitation behaviors of hot rolling and cold rolled annealing steel plates strengthened complexly by titanium and molybdenum were studied in the paper. The microstructures and precipitate phases were analyzed using optical microscope (OM), scanning electron microscope (SEM), transmission electron microscope (TEM) with energy disperse spectroscopy (EDS). The results showed that the coarsening square TiN phase and the fine roundness (Ti,Mo)C phase were precipitated mostly in the hot rolled steel plate. As the finishing temperature decreased and coiling holding time increased, the quantity of fine precipitates increased. And also the fine round precipitates increased, dispersion expanded and shape of the phase being uniformed as the annealing temperature increased. Therefore, the strengthen effects can be improved effectively by a reasonable control toward titanium and molybdenum precipitation behaviors.

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