The Effect of Stoichiometry and Degree of Order on Mechanical Properties of Ni3Fe Intermetallics

2013 ◽  
Vol 747-748 ◽  
pp. 19-24 ◽  
Author(s):  
Ye Xin Chen ◽  
Hai Yan Qian ◽  
Tao Chen

The effects of Fe stoichiometry and degree of order on mechanical properties of intermetallics Ni3Fe were investigated. The experimental results showed that the phase composition and the grain size of Ni3Fe alloy was independent on Fe stoichiometry. The Ni3Fe alloy with the normal stoichiometry had the lowest elongation in the ordered and disordered alloys. The tensile strength of Ni3Fe alloy depended on Fe stoichiometry of alloy. The effect of Fe stoichiometry on the mechanical properties of the ordered alloy was larger than that of disordered alloy. There were more point defects in lattice when the alloy stoichiometry deviating from the normal stoichiometry in the Ni3Fe alloy. The changes of the concentration of the point defects and degree of order altered the deformation behavior of the Ni3Fe alloy.

2020 ◽  
Vol 17 (6) ◽  
pp. 831-836
Author(s):  
M. Vykunta Rao ◽  
Srinivasa Rao P. ◽  
B. Surendra Babu

Purpose Vibratory weld conditioning parameters have a great influence on the improvement of mechanical properties of weld connections. The purpose of this paper is to understand the influence of vibratory weld conditioning on the mechanical and microstructural characterization of aluminum 5052 alloy weldments. An attempt is made to understand the effect of the vibratory tungsten inert gas (TIG) welding process parameters on the hardness, ultimate tensile strength and microstructure of Al 5052-H32 alloy weldments. Design/methodology/approach Aluminum 5052 H32 specimens are welded at different combinations of vibromotor voltage inputs and time of vibrations. Voltage input is varied from 50 to 230 V at an interval of 10 V. At each voltage input to the vibromotor, there are three levels of time of vibration, i.e. 80, 90 and 100 s. The vibratory TIG-welded specimens are tested for their mechanical and microstructural properties. Findings The results indicate that the mechanical properties of aluminum alloy weld connections improved by increasing voltage input up to 160 V. Also, it has been observed that by increasing vibromotor voltage input beyond 160 V, mechanical properties were reduced significantly. It is also found that vibration time has less influence on the mechanical properties of weld connections. Improvement in hardness and ultimate tensile strength of vibratory welded joints is 16 and 14%, respectively, when compared without vibration, i.e. normal weld conditions. Average grain size is measured as per ASTM E 112–96. Average grain size is in the case of 0, 120, 160 and 230 is 20.709, 17.99, 16.57 and 20.8086 µm, respectively. Originality/value Novel vibratory TIG welded joints are prepared. Mechanical and micro-structural properties are tested.


Materials ◽  
2021 ◽  
Vol 14 (14) ◽  
pp. 3969
Author(s):  
Shirui Zhang ◽  
Shili Qiu ◽  
Pengfei Kou ◽  
Shaojun Li ◽  
Ping Li ◽  
...  

Granite exhibits obvious meso-geometric heterogeneity. To study the influence of grain size and preferred grain orientation on the damage evolution and mechanical properties of granite, as well as to reveal the inner link between grain size‚ preferred orientation, uniaxial tensile strength (UTS) and damage evolution, a series of Brazilian splitting tests were carried out based on the combined finite-discrete element method (FDEM), grain-based model (GBM) and inverse Monte Carlo (IMC) algorithm. The main conclusions are as follows: (1) Mineral grain significantly influences the crack propagation paths, and the GBM can capture the location of fracture section more accurately than the conventional model. (2) Shear cracks occur near the loading area, while tensile and tensile-shear mixed cracks occur far from the loading area. The applied stress must overcome the tensile strength of the grain interface contacts. (3) The UTS and the ratio of the number of intergrain tensile cracks to the number of intragrain tensile cracks are negatively related to the grain size. (4) With the increase of the preferred grain orientation, the UTS presents a “V-shaped” characteristic distribution. (5) During the whole process of splitting simulation, shear microcracks play the dominant role in energy release; particularly, they occur in later stage. This novel framework, which can reveal the control mechanism of brittle rock heterogeneity on continuous-discontinuous trans-scale fracture process and microscopic rock behaviour, provides an effective technology and numerical analysis method for characterizing rock meso-structure. Accordingly, the research results can provide a useful reference for the prediction of heterogeneous rock mechanical properties and the stability control of engineering rock masses.


2013 ◽  
Vol 749 ◽  
pp. 407-413
Author(s):  
Hong Xu ◽  
Xin Zhang ◽  
Ji Ping Ren ◽  
Min Peng ◽  
Shi Yang ◽  
...  

The mechanical properties and corrosion performances of the ZL101 alloy modified by the composite master alloy were investigated. The results showed that the master alloy had not only obvious effect of grain refinement, but also a significant role in refining dendrite grain of ZL101 alloy. The grain size decreased dramatically from 150μm to 62μm when the addition of composite master alloy is up to 0.5%(mass fraction) and the temperature is 720 for 30 minutes,. Its tensile strength and elongation increased by 27% and 42% respectively. The grain refinement of ZL101 alloy decreased its corrosion performance. The morphology of Si changed into globular from needle modified by NaF, instead of AlTiB.


2010 ◽  
Vol 667-669 ◽  
pp. 253-258
Author(s):  
Wei Ping Hu ◽  
Si Yuan Zhang ◽  
Xiao Yu He ◽  
Zhen Yang Liu ◽  
Rolf Berghammer ◽  
...  

An aged Al-5Zn-1.6Mg alloy with fine η' precipitates was grain refined to ~100 nm grain size by severe plastic deformation (SPD). Microstructure evolution during SPD and mechanical behaviour after SPD of the alloy were characterized by electron microscopy and tensile, compression as well as nanoindentation tests. The influence of η' precipitates on microstructure and mechanical properties of ultrafine grained Al-Zn-Mg alloy is discussed with respect to their effect on dislocation configurations and deformation mechanisms during processing of the alloy.


2021 ◽  
Vol 21 (9) ◽  
pp. 4897-4901
Author(s):  
Hyo-Sang Yoo ◽  
Yong-Ho Kim ◽  
Hyeon-Taek Son

In this study, changes in the microstructure, mechanical properties, and electrical conductivity of cast and extruded Al–Zn–Cu–Mg based alloys with the addition of Li (0, 0.5 and 1.0 wt.%) were investigated. The Al–Zn–Cu–Mg–xLi alloys were cast and homogenized at 570 °C for 4 hours. The billets were hot extruded into rod that were 12 mm in diameter with a reduction ratio of 38:1 at 550 °C. As the amount of Li added increased from 0 to 1.0 wt.%, the average grain size of the extruded Al alloy increased from 259.2 to 383.0 µm, and the high-angle grain boundaries (HGBs) fraction decreased from 64.0 to 52.1%. As the Li content increased from 0 to 1.0 wt.%, the elongation was not significantly different from 27.8 to 27.4% and the ultimate tensile strength (UTS) was improved from 146.7 to 160.6 MPa. As Li was added, spherical particles bonded to each other, forming an irregular particles. It is thought that these irregular particles contribute to the strength improvement.


2018 ◽  
Vol 44 (8) ◽  
pp. 663-666 ◽  
Author(s):  
N. L. Savchenko ◽  
T. Yu. Sablina ◽  
I. N. Sevost’yanova ◽  
A. G. Burlachenko ◽  
S. P. Buyakova ◽  
...  

2014 ◽  
Vol 875-877 ◽  
pp. 63-67 ◽  
Author(s):  
Dinh van Hai ◽  
Nguyen Trong Giang

In this work, ECAP technique was combined with cold rolling process in order to enhance mechanical properties and microstructure of pure Titanium. Coarse grain (CG) Titanium with original grain size of 150 μm had been pressed by ECAP at 425oC by 4, 8 and 12 passes, respectively. This process then was followed by rolling at room temperature with 35%, 55%, and 75% rolling strains. After two steps, mechanical properties such as strength, hardness and microstructure of processed Titanium have been measured. The result indicated significant effect of cold rolling on tensile strength, hardness and microstructure of ECAP-Titanium.


2021 ◽  
Vol 2101 (1) ◽  
pp. 012074
Author(s):  
Weixin Yu ◽  
Zhen Dai ◽  
Jifeng Zhao ◽  
Lulu Fang ◽  
Yiwen Zhang

Abstract The strength of P92 steel (tensile strength, specified plastic elongation strength) will decrease after its hardness is reduced, ferrite and carbides forming the structure. Carbides of grain size 5-6 are precipitated in the grains and grain boundaries. The martensite lath shape has completely disappeared. M23C6 carbide coarsened obviously, with a maximum size of about 500nm; The Laves phase is also aggregated and coarsened, connecting in a chain shape with a maximum size of more than 500nm. Evolution of microstructure, namely the obvious coarsening of M23C6 carbides and the aggregation and connection of Laves phases in a chain shape, are the main causes for rapid decrease in the stability of the material substructure and evident decline in mechanical properties and hardness. In addition, the MX phase did not change significantly, hardly affecting the hardness reduction of P92 steel.


2010 ◽  
Vol 667-669 ◽  
pp. 457-461
Author(s):  
Wei Guo ◽  
Qu Dong Wang ◽  
Man Ping Liu ◽  
Tao Peng ◽  
Xin Tao Liu ◽  
...  

Cyclic channel die compression (CCDC) of AZ31-1.7 wt.% Si alloy was performed up to 5 passes at 623 K in order to investigate the microstructure and mechanical properties of compressed alloys. The results show that multi-pass CCDC is very effective to refine the matrix grain and Mg2Si phases. After the alloy is processed for 5 passes, the mean grain size decreases from 300 μm of as-cast to 8 μm. Both dendritic and Chinese script type Mg2Si phases break into small polygonal pieces and distribute uniformly in the matrix. The tensile strength increases prominently from 118 MPa to 216 MPa, whereas the hardness of alloy deformed 5 passes only increase by 8.4% compared with as-cast state.


Materials ◽  
2020 ◽  
Vol 13 (20) ◽  
pp. 4563
Author(s):  
Yu Hou ◽  
Xujun Mi ◽  
Haofeng Xie ◽  
Wenjing Zhang ◽  
Guojie Huang ◽  
...  

The size (grain size and specimen size) effect makes traditional macroscopic forming technology unsuitable for a microscopic forming process. In order to investigate the size effect on mechanical properties and deformation behavior, pure copper wires (diameters range from 50 μm to 500 μm) were annealed at different temperatures to obtain different grain sizes. The results show that a decrease in wire diameter leads to a reduction in tensile strength, and this change is pronounced for large grains. The elongation of the material is in linear correlation to size factor D/d (diameter/grain size), i.e., at the same wire diameter, more grains in the section bring better plasticity. This phenomenon is in relationship with the ratio of free surface grains. A surface model combined with the theory of single crystal and polycrystal is established, based on the relationship between specimen/grain size and tensile property. The simulated results show that the flow stress in micro-scale is in the middle of the single crystal model (lower critical value) and the polycrystalline model (upper critical value). Moreover, the simulation results of the hybrid model calculations presented in this paper are in good agreement with the experimental results.


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