Rice Husk Ash Impregnated with Silver Nanoparticles for Water Purification

2014 ◽  
Vol 798-799 ◽  
pp. 727-731 ◽  
Author(s):  
Angela M. Gutierrez ◽  
Dachamir Hotza ◽  
Gabriel B. Dutra ◽  
André L. Nogueira ◽  
César V. Franco ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Escherichia Coli ◽  
Silver Nanoparticles ◽  
Surface Area ◽  
Rice Husk ◽  
Rice Husk Ash ◽  
Substrate Surface ◽  
Antimicrobial Effect ◽  
Microbiological Analyses ◽  
Scanning Electron

In this work, silver nanoparticles were incorporated in four different concentrations into rice husk ash (RHA) to promote an antimicrobial effect. The suspension was magnetic stirred and dried at 80°C for 24 h. The samples were characterized by scanning electron microscopy (SEM), specific surface area and zeta potential measurements. Microbiological analyses were conducted test the efficiency of the material in the elimination of the bacteria Escherichia coli. SEM results revealed a homogeneous dispersion of silver nanoparticles on the substrate, surface area values similar to those found in the literature and effective antimicrobial activity at low silver concentration.

Natural Rubber/Bombyx Mori Silk Fibroin Composites: Preparation and Properties

2011 ◽  
Vol 306-307 ◽  
pp. 894-900
Author(s):  
Qing Huang Wang ◽  
Yong Yue Luo ◽  
Zhi Feng Yi ◽  
Chun Fang Feng ◽  
Yue Qiong Wang ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Escherichia Coli ◽  
Natural Rubber ◽  
Bombyx Mori ◽  
Silk Fibroin ◽  
Antimicrobial Effect ◽  
Bombyx Mori Silk ◽  
Latex Compounding ◽  
And Staphylococcus Aureus ◽  
Scanning Electron

A novel natural rubber/silk fibroin (NR/SF) antibacterial composite was prepared firstly by using bombyx mori silk fibroin as the antimicrobial filler through latex compounding techniques. The results from scanning electron microscopy and universal tensile machine proved that the compatibility between SF and NR matrix is excellent, and the tensile strength of composite sheets is enhanced to some extent. NR/SF antibacterial composite sheets have a good antimicrobial effect on Escherichia coli and Staphylococcus aureus. Moreover, the suitable loading of SF is 0.5~1 wt% according to the results above.

scholarly journals Utilization of Rice Husk Ash in the Preparation of Graphene-Oxide-Based Mesoporous Nanocomposites with Excellent Adsorption Performance

Materials ◽  
2021 ◽  
Vol 14 (5) ◽  
pp. 1214
Author(s):  
Tzong-Horng Liou ◽  
Yuan Hao Liou
Keyword(s):  
Electron Microscopy ◽  
Graphene Oxide ◽  
Adsorption Capacity ◽  
Surface Area ◽  
Rice Husk ◽  
Rice Husk Ash ◽  
High Surface ◽  
Dye Adsorption ◽  
Value Added ◽  
Biomass Waste

Rice husk is an agricultural biomass waste. Burning rice husks in an oxygenic atmosphere releases thermal energy and produces ash that is rich in silica. Rice husk ash (RHA) can be used as a sustainable source of silica for producing high-value-added products. In this study, mesostructural graphene oxide (GO)/SBA-15, a graphene-based hybrid material, was synthesized from RHA. The materials are inspected by Fourier transform infrared spectrometer, Raman spectrometer, field-emission scanning electron microscopy, transmission electron microscopy, surface area analyzer, and X-ray diffraction analyzer. Studies have revealed that GO/SBA-15 possesses various oxygen functional groups that are helpful for dye adsorption. The material consisted of high pore volume of 0.901 cm3/g, wide pores of diameter 11.67 nm, and high surface area of 499 m2/g. Analysis of the methylene blue (MB) adsorption behavior of GO/SBA-15 composites revealed that their adsorption capacity depended on the gelation pH, GO content, adsorbent dosage, and initial dye (MB) concentration. The highest adsorption capacity of GO/SBA-15 was 632.9 mg/g. Furthermore, the adsorption isotherms and kinetics of GO/SBA-15 were investigated. This study demonstrated the great advantage of treated RHA and the potential of this material for use in organic dye adsorption.

Microstructural and mechanical characterization of novel AA7075 composites reinforced with rice husk ash and carbonized eggshells

2021 ◽  
pp. 146442072110312
Author(s):  
Vivudh Gupta ◽  
Balbir Singh ◽  
RK Mishra
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Rice Husk ◽  
Rice Husk Ash ◽  
Low Cost ◽  
Agricultural Waste ◽  
Stir Casting ◽  
Light Weight ◽  
Weight Percentage ◽  
Scanning Electron

This paper investigates microstructural and mechanical characteristics of novel AA7075 composites supplemented with agricultural waste, i.e. rice husk ash and poultry waste, i.e. carbonized eggshells. Both these wastes possess important constituents which make them potential reinforcement material for composites, and their utilization also reduces the problem of disposal to a certain extent. AA7075 composites with varying weight percentages of rice husk ash and carbonized eggshells were prepared through stir casting route. The sum of weight percentages of both reinforcements was kept constant at 5 wt.%. Composites were tested for density and different mechanical properties. Prior to these tests, composites were examined through scanning electron microscopy and energy-dispersive X-ray spectroscopy techniques, wherein uniform distribution of reinforcements was observed. Inclusion of light weight reinforcements decreased the density of composites. Among these composites, highest hardness value was shown by composite having 5 wt.% of rice husk ash with 24.47% enhancement over unreinforced AA7075. Maximum tensile strength and compression strength were exhibited by hybrid composite with 3.75 wt.% rice husk ash and 1.25 wt.% carbonized eggshells. This increment is 28.20% and 16%, respectively, over base composition. Impact strength decreased as the weight percentage of CES increased, thereby indicating brittleness in behaviour. Fractography analysis of tensile and impact test specimens was done through scanning electron microscopy to determine failure mode wherein presence of cracks, voids, dimples, debonding, etc. was observed. Hence, these light weight and low cost green AA7075 composites showed improved properties making them as an alternative as well as sustainable material for automotive and aerospace applications.

Chemical and Mineralogical Properties of Rice Husk Ash (RHA)

2014 ◽  
Vol 70 (5) ◽  
Author(s):  
Jamo Usman Hassan ◽  
Mohamad Kamal Zaky Noh ◽  
Zainal Arifin Ahmad
Keyword(s):  
Electron Microscopy ◽  
Rice Husk ◽  
Cellular Structure ◽  
Rice Husk Ash ◽  
Amorphous Structure ◽  
X Ray Diffraction ◽  
X Ray ◽  
Silica Source ◽  
Microscopic Techniques ◽  
Scanning Electron

Rice husk ash (RHA) as a silica source was studied, resulting from burning at a temperature of       700oC in an electric furnace. RHA consists of inorganic, incombustible matter in the rice husk that has been fused into an amorphous structure. Microscopic techniques, such as X-ray fluorescence (XRF), X-ray diffraction (XRD) and scanning electron microscopy (SEM) were used to observe the surface and internal structure of the RHA. The results among other things revealed that RHA consist of mainly SiO2, with amorphous structure, Microscopic examination showed that has a porous cellular structure and consists of irregular-shaped particles.   

Preparation of SiC Powders by Utilizing Rice Husk Ash from Biomass Cogeneration Plant

2013 ◽  
Vol 634-638 ◽  
pp. 1990-1993 ◽  
Author(s):  
Ming Yu Fan ◽  
Wen Jie Yuan ◽  
Cheng Ji Deng ◽  
Hong Xi Zhu
Keyword(s):  
Electron Microscopy ◽  
Rice Husk ◽  
Industrial Waste ◽  
Rice Husk Ash ◽  
Cogeneration Plant ◽  
Optimal Temperature ◽  
X Ray Diffraction ◽  
X Ray ◽  
Effects Of Temperature ◽  
Scanning Electron

A large amount of rice husk ash (RHA) is produced in the biomass cogeneration plant using rice husk as fuel. For utilization of this kind of industrial waste, SiC powders were synthesized with RHA and carbon black calcined at the temperature from 1500 to 1650 °C in argon. The phase composition and microstructure of samples were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The effects of temperature and SiO2/C ratio on the synthesis of SiC powders were investigated. The results show that the formation of SiC increases with SiO2/C ratio increasing as a whole, and SiC whisker appears at the temperature up to 1650 °C. The optimal temperature and SiO2/C ratio are 1550 °C and 5:8 respectively.

scholarly journals Effects of Long Durations of RF–Magnetron Sputtering Deposition of Hydroxyapatite on Titanium Dental Implants

2021 ◽  
Author(s):  
Ihab Nabeel Safi ◽  
Basima Mohammed Ali Hussein ◽  
Hikmat J. Aljudy ◽  
Mustafa S. Tukmachi
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Magnetron Sputtering ◽  
Dental Implants ◽  
Substrate Surface ◽  
Rf Magnetron Sputtering ◽  
P Value ◽  
Edx Analysis ◽  
Significant Difference ◽  
Scanning Electron

Abstract Objectives Dental implant is a revolution in dentistry; some shortages are still a focus of research. This study use long duration of radiofrequency (RF)–magnetron sputtering to coat titanium (Ti) implant with hydroxyapatite (HA) to obtain a uniform, strongly adhered in a few micrometers in thickness. Materials and Methods Two types of substrates: discs and root form cylinders were prepared using a grade 1 commercially pure (CP) Ti rod. A RF–magnetron sputtering device was used to coat specimens with HA. Magnetron sputtering was set at 150 W for 22 hours at 100°C under continuous argon gas flow and substrate rotation at 10 rpm. Coat properties were evaluated via field emission scanning electron microscopy (FESEM), scanning electron microscopy–energy dispersive X-ray (EDX) analysis, atomic force microscopy, and Vickers hardness (VH). Student’s t-test was used. Results All FESEM images showed a homogeneous, continuous, and crack-free HA coat with a rough surface. EDX analysis revealed inclusion of HA particles within the substrate surface in a calcium (Ca)/phosphorus (P) ratio (16.58/11.31) close to that of HA. Elemental and EDX analyses showed Ca, Ti, P, and oxygen within Ti. The FESEM views at a cross-section of the substrate showed an average of 7 µm coat thickness. Moreover, these images revealed a dense, compact, and uniform continuous adhesion between the coat layer and the substrate. Roughness result indicated highly significant difference between uncoated Ti and HA coat (p-value < 0.05). A significant improvement in the VH value was observed when coat hardness was compared with the Ti substrate hardness (p-value < 0.05). Conclusion Prolonged magnetron sputtering successfully coat Ti dental implants with HA in micrometers thickness which is well adhered essentially in excellent osseointegration.

Distribution of diaphragmatic lymphatic stomata

1991 ◽  
Vol 70 (4) ◽  
pp. 1544-1549 ◽  
Author(s):  
D. Negrini ◽  
S. Mukenge ◽  
M. Del Fabbro ◽  
C. Gonano ◽  
G. Miserocchi
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Surface Area ◽  
Frequency Distribution ◽  
Maximum Diameter ◽  
Minimum Diameter ◽  
Average Value ◽  
Scanning Electron

In seven anesthetized rabbits we measured the size, shape, and density of lymphatic stomata on the peritoneal and pleural sides of the diaphragm. The diaphragm was fixed in situ and processed for scanning electron microscopy. Results are from 2,902 peritoneal and 3,086 pleural fields (each 1,620 microns 2) randomly chosen from the various specimens. Stomata were seen in 9% of the fields examined, and in 30% of the cases they appeared grouped in clusters with 2-14 stomata/field. Stoma density was 250 +/- 242 and 72 +/- 57 (SD) stomata/mm2 on peritoneal and pleural sides, respectively, and it was similar over the muscular and tendinous portion of the two surfaces. The maximum diameter ranged from less than 1 to approximately 30 microns, with an average value of 1.2 +/- 3.1 micron. The ratio of the maximum to the minimum diameter and the surface area averaged 2 +/- 1.4 and 0.7 +/- 2.4 micron 2, respectively. The maximum and minimum diameter and surface area values followed a lognormal frequency distribution, suggesting that stomata geometry is affected by diaphragmatic tension.

scholarly journals GREEN TECHNOLOGY MEDIATED SYNTHESIS OF SILVER NANOPARTICLES FROM MOMORDICA CHARANTIA FRUIT EXTRACT AND ITS BACTERICIDAL ACTIVITY

2017 ◽  
Vol 10 (3) ◽  
pp. 196 ◽  
Author(s):  
S C Joshi ◽  
Utkarsh Kaushik ◽  
Aproova Upadhyaya ◽  
Priyanka Sharma
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Silver Nanoparticles ◽  
Atomic Force Microscope ◽  
Momordica Charantia ◽  
Diffusion Method ◽  
Fruit Extract ◽  
Atomic Force ◽  
Vis Spectroscopy ◽  
Scanning Electron

ABSTRACTObjective: The synthesis of nanoparticles from biological processes is evolving a new era of research interests in nanotechnology. Silver nanoparticlesare usually synthesized by chemicals and physical method, which are quite toxic and flammable in nature. This study deals with an environmentfriendly biosynthesis process of antibacterial silver nanoparticles using Momordica charantia fruit.Methods: AgNO3 (5 mM) was allowed to react with fruit extract of M. charantia. Biosynthesis of AgNPs was optimized by changing temperature,pH, and solvent. The silver nanoparticles so formed were characterized using ultraviolet-visible (UV-VIS) spectroscopy, Fourier transform infraredspectroscopy (FTIR), dynamic light scattering (DLS), atomic force microscope (AFM), and scanning electron microscopy (SEM).Results: UV-VIS spectra show absorption peak between 420 and 430 nm. The FTIR analysis showed the alcoholic, lactam, and nitro group presentin the plant extract, which were responsible for the reduction in AgNPs. The SEM images showed the size distribution of the nanoparticles and theaverage size was found to be 50-100 nm. By DLS analysis and AFM analysis, average sizes of the silver nanoparticles were of 150 nm. The results ofthese analyses confirmed the formation of silver nanoparticles. Silver nanoparticles were tested against Bacillus cereus and Staphylococcus epidermidisstrains using disc diffusion method and were found to be effective.Conclusion: Silver nanoparticles so synthesized in this study using fruit extract of M. charantia are simple, easy, and effective technique of nanoparticlesproduction.Keywords: Silver nanoparticles, Momordica charantia, Optimization, Antibacterial, Atomic force microscope, Scanning electron microscopy.

scholarly journals Pengaruh Suhu Sintering Terhadap Sintesis Silicon Carbide (SiC) Berbahan Dasar Abu Sekam Padi dan Grafit Pensil 2B

2015 ◽  
Vol 5 (01) ◽  
pp. 31
Author(s):  
Resky Irfanita ◽  
Asnaeni Ansar ◽  
Ayu Hardianti Pratiwi ◽  
Jasruddin J ◽  
Subaer S
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Silicon Carbide ◽  
Rice Husk Ash ◽  
Sintering Temperature ◽  
Solid State Reaction Method ◽  
X Ray Diffraction ◽  
Reaction Method ◽  
X Ray ◽  
Scanning Electron

The objective of this study is to investigate the effect of sintering temperature on the synthesis of SiC produced from rice husk ash (RHA) and 2B graphite pencils. The SiC was synthesized by using solid state reaction method sintered at temperatures of 750°C, 1000°C and 1200°C for 26 hours, 11.5 hours and 11.5 hours, respectively. The quantity and crystallinity level of SiC phase were measured by means of Rigaku MiniFlexII X-Ray Diffraction (XRD). The microstructure of SiC was examined by using Tescan Vega3SB Scanning Electron Microscopy (SEM). The XRD results showed that the concentration (wt%) of SiC phase increases with the increasing of sintering temperature. SEM results showed that the crystallinity level of SiC crystal is improving as the sintering temperature increases

scholarly journals SINTESIS NANOKOMPOSIT Nata de coco/TiO2/Ag DAN EFEKTIVITASNYA SEBAGAI ANTIBAKTERI TERHADAP BAKTERI Escherichia coli dan Staphylococcus aureus

2021 ◽  
Vol 14 (1) ◽  
Author(s):  
Heriyanto Tinentang ◽  
Henry F Aritonang ◽  
Harry S. J. Koleangan
Keyword(s):  
Electron Microscopy ◽  
Escherichia Coli ◽  
Scanning Electron Microscopy ◽  
Staphylococcus Aureus ◽  
Chemical Reduction ◽  
Bacterial Activity ◽  
Energy Dispersive ◽  
X Ray ◽  
Escherichia Coli Bacteria ◽  
Scanning Electron

Telah dilakukan penelitian tentang kemampuan aktivitas anti bakteri untuk bakteri Staphylococcus aureus (gram positif) dan Escherichia coli (gram negatif) dengan menggunakan nanokomposit nata de coco/TiO2, nata de coco/Ag, dan nata de coco/TiO2/Ag dengan variasi konsentrasi Ag 0,5 M; 0,6 M; 0,7 M; 0,8 M dan 0,9 M  menggunakan metode reduksi kimia. Nanopartikel tersebut dikarakterisasi menggunakan X-Ray Diffractometry (XRD), scanning electron microscopy-energy dispersive X-ray spectroscopy  (SEM-EDS) dan anti bakteri. Untuk uji aktivitas antibakteri menggunakan metode kertas cakram dan dilakukan sebanyak dua kali ulangan untuk tiap-tiap sampel dan bakteri yang diuji. Hasil penelitian menunjukan, aktivitas anti bakteri nanokomposit yang paling baik dalam menghambat pertumbuhan bakteri adalah nanokomposit Nata de coco/TiO2/Ag mampu menghambat pertumbuhan bakteri Escherichiacoli dan Staphylococcusaureus, namun nanokomposit tersebut lebih efektif menghambat pertumbuhan bakteri Escherichiacoli.ABSRACT Research on the ability of anti-bacterial activity for Staphylococcus aureus (gram positive) and Escherichia coli (gram negative) bacteria using nata de coco / nanocomposites TiO2, nata de coco / Ag, and nata de coco / TiO2 / Ag with variations of Ag 0,5 M; 0.6 M; 0.7 M; 0.8 M and 0.9 M using the chemical reduction method. Nanoparticles were characterized using X-Ray Diffractometry (XRD), scanning electron microscopy-energy dispersive X-ray spctroscopy  (SEM-EDS) and anti-bacterial actvity. Test the antibacterial activity using the paper disc method and repeated two times for each sample and bacteria tested. The results showed that the good anti-bacterial activity of nanocomposites in inhibiting bacterial growth was nanocomposite nata de coco /TiO2/Ag  able to inhibit the growth of Escherichia coli and S. aureus, but the nanocomposite is more effective in inhibiting the growth of Escherichia  coli bacteria.

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