Adhesion shear strength test method for freshwater/seawater ice on carbon ceramic brake pads of amphibious aircraft

Purpose Based on the mechanical model of typical shear tests, this study aims to propose the test principle and method of freshwater/seawater ice adhesion shear strength of carbon ceramic brake pads for amphibious aircraft, designs and builds the test equipment, prepares the freshwater/seawater ice samples and completes the tests. Design/methodology/approach This study examines the influence of the icing process, mechanism, temperature and freshwater/seawater on ice adhesion shear strength of carbon ceramic brake pads and puts forward a test method for the freshwater/seawater ice adhesion shear strength of amphibious aircraft brake pads. Findings The obtained results examine the influence of the icing process, mechanism, temperature and freshwater/seawater on ice adhesion shear strength of carbon ceramic brake pads. The adhesion shear strength of frozen freshwater and of the seawater of Dalian, Qingdao, Fuzhou and Zhuhai on the surface of aircraft brake pads is measured at –10 to –50°C. It is found that the shear strength of freshwater increases first and then decreases with the decrease of temperature. The adhesion shear strength of seawater; however, increases mainly linear with the decrease of temperature. Originality/value The value of this paper is that the test method proposed and test results for the freshwater/seawater ice adhesion shear strength of amphibious aircraft brake pads provide technical support for the anti-icing design of amphibious aircraft brake devices.

A Multi-Tool Analysis to Assess the Effectiveness of Passive Ice Protection Materials to Assist Rotorcraft Manual De-Icing

Search and rescue missions using rotorcrafts need to be reliable all year long, even in winter conditions. In some cases of deployment prior to take off, the crew may need to manually remove accumulated contaminant from the critical surfaces using tools at their disposal. However, icy contaminant may be hard to remove since the rotorcrafts critical surfaces could be cooler than the environment, thus promoting adhesion. Currently, there exists several passive ice protection materials that could reduce the ice adhesion strength and assist the manual de-icing. The aim of this paper is to propose a detailed comparative procedure to assess the ability of materials to assist the manual de-icing of rotorcrafts. The proposed procedure consists of the characterization of materials using several laboratory tests in order to determine their characteristics pertaining to wettability, their icephobic behavior, and finally their assessment under a multi-tool analysis to evaluate if they can assist. The multi-tool analysis uses different mechanical tools, which are currently used during normal operation, to execute a gradual de-icing procedure, which begins with the softest to the hardest tool using a constant number of passes or strokes, under different types of simulated precipitation. Five different materials were used to evaluate the proposed procedure: Aluminum (used as a reference), two silicone-based coatings (Nusil and SurfEllent), an epoxy-based coating (Wearlon), and finally a commercial ski wax (Swix). All of the tested materials could assist the manual de-icing, within a certain limit, when compared to the bare aluminum. However, SurfEllent was the material that obtained the best overall results. This procedure could be easily adapted to different fields of application and could be used as a development tool for the optimization and the assessment of new materials aimed to reduce ice adhesion.

Icephobic and Anticorrosion Coatings Deposited by Electrospinning on Aluminum Alloys for Aerospace Applications

Anti-icing or passive strategies have undergone a remarkable growth in importance as a complement for the de-icing approaches or active methods. As a result, many efforts for developing icephobic surfaces have been mostly dedicated to apply superhydrophobic coatings. Recently, a different type of ice-repellent structure based on slippery liquid-infused porous surfaces (SLIPS) has attracted increasing attention for being a simple and effective passive ice protection in a wide range of application areas, especially for the prevention of ice formation on aircrafts. In this work, the electrospinning technique has been used for the deposition of PVDF-HFP coatings on samples of the aeronautical alloy AA7075 by using a thickness control system based on the identification of the proper combination of process parameters such as the flow rate and applied voltage. In addition, the influence of the experimental conditions on the nanofiber properties is evaluated in terms of surface morphology, wettability, corrosion resistance, and optical transmittance. The experimental results showed an improvement in the micro/nanoscale structure, which optimizes the superhydrophobic and anticorrosive behavior due to the air trapped inside the nanotextured surface. In addition, once the best coating was selected, centrifugal ice adhesion tests (CAT) were carried out for two types of icing conditions (glaze and rime) simulated in an ice wind tunnel (IWT) on both as-deposited and liquid-infused coatings (SLIPs). The liquid-infused coatings showed a low water adhesion (low contact angle hysteresis) and low ice adhesion strength, reducing the ice adhesion four times with respect to PTFE (a well-known low-ice-adhesion material used as a reference).

Current Ice Adhesion Testing Methods and the Need for a Standard: A Concise Review

Ice accretion is a serious problem in cold climates, causing automobile and airplane accidents, as well as severe economic losses throughout various sectors. To combat these issues, many solutions have been developed, such as de-icing materials, which can delay or prevent the adhesion of ice to a surface through chemical, temperature, or physical means. To effectively assess the properties of a de-icing material, ice adhesion testing must be conducted, of which there are numerous types, each with their own characteristics. Unfortunately, the same material, tested with different methods, may provide very different ice adhesion values. This makes it difficult to properly characterize a material’s de-icing properties and compare values across the literature. In this review, we identified the main ice adhesion testing methods and compared ice adhesion values for a particular material with different testing methods. We then discussed some of the main issues with current ice testing methods and identified some of the main factors that may affect ice adhesion values, namely ice quality and the use of a mold, which may significantly affect the final ice adhesion results. Finally, we proposed a new, simple standard testing method, in an attempt to eliminate some of the issues with current ice testing methods.

Effects of Discontinuous Thermal Conductivity of a Substrate Surface on Ice Adhesion Strength

This study proposes a novel anti-icing model in which silicone rubber with low thermal conductivity is coated at different positions on a material surface to change the continuity of the thermal conductivity of the surface. During the test, the surfaces of aluminum alloy and polymethyl methacrylate (PMMA) are discontinuously coated with silicone rubber. Repeated experiments are conducted to verify the anti-icing effect of the proposed model. Results showed that compared to the conventional surface ice adhesion strength, the rate of reduction of the ice adhesion strength of the aluminum alloy and PMMA could reach 75.07% and 76.70%, respectively, when the novel method is used. Because of the different levels of thermal conductivity at different positions on the material surface, the water attached to the surface locations without the coated silicone rubber had other freezing times. Combined with the heat and phase change of water during the freezing process, changing the stability of the interface between the ice and substrate could act as an active anti-icing power. The ice adhesion strength on the material surface could then be reduced. Compared with the conventional anti-icing methods, the anti-icing method proposed in this study could significantly increase the active anti-icing characteristics of the material and provide a novel anti-icing method for use in engineering applications.

Design of Icephobic Surfaces by Lowering Ice Adhesion Strength: A Mini Review

Ice accretion can lead to severe consequences in daily life and sometimes catastrophic events. To mitigate the hazard of icing, passive icephobic surfaces have drawn widespread attentions because of their abilities in repelling incoming water droplets, suppressing ice nucleation and/or lowering ice adhesion strength. As time elapses and temperature lowers sufficiently, ice accretion becomes inevitable, and a realistic roadmap to surface icephobicity for various outdoor anti-icing applications is to live with ice but with the lowest ice adhesion strength. In this review, surfaces with icephobicity are critically categorized into smooth surfaces, textured surfaces, slippery surfaces and sub-surface textured surfaces, and discussed in terms of theoretical limit, current status and perspectives. Particular attention is paid to multiple passive anti-icing strategies combined approaches as proposed on the basis of icephobic surfaces. Correlating the current strategies with one another will promote understanding of the key parameters in lowering ice adhesion strength. Finally, we provide remarks on the rational design of state-of-the-art icephobic surfaces with low ice adhesion strength.

Coral-like silicone nanofilament coatings with extremely low ice adhesion

Passive icephobic surfaces can provide a cost and energy efficient solution to many icing problems that are currently handled with expensive active strategies. Water-repellent surface treatments are promising candidates for this goal, but commonly studied systems, such as superhydrophobic surfaces and Slippery Liquid Infused Porous Surfaces (SLIPS), still face challenges in the stability and durability of their properties in icing environments. In this work, environmental icing conditions are simulated using an Icing Wind Tunnel, and ice adhesion is evaluated with a Centrifugal Adhesion Test. We show that superhydrophobic coral-like Silicone Nanofilament (SNF) coatings exhibit extremely low ice adhesion, to the point of spontaneous ice detachment, and good durability against successive icing cycles. Moreover, SNFs-based SLIPS show stably low ice adhesion for the whole duration of the icing test. Stability of surface properties in a cold environment is further investigated with water wettability at sub-zero surface temperature, highlighting the effect of surface chemistry on superhydrophobicity under icing conditions.