Morphological and Mechanical Properties of Poly (Butylene Terephthalate)/High-Density Polyethylene Blends

Poly (butylene terephthalate) (PBT) is a popular thermoplastic polyester resin but has low strength and low melting point. To improve its properties, PBT is often mixed with other resins, such as high-density polyethylene (HDPE). In this study, PBT/HDPE samples with 100% PBT, 5%, 10%, 15%, and 100% HDPE are generated and tested. The samples are analyzed by tensile strength, flexural strength, impact strength, and SEM tests. Adding HDPE will reduce tensile strength compared to pure PBT, in which 5%, 10%, and 15% PBT/HDPE samples obtain the values 40.23, 38.11, and 27.77 MPa, respectively. These values are lower than that of pure PBT but still higher than that of HDPE. Improving the HDPE portion mostly results in decreasing flexural strength. The flexural strengths of these samples are 87.79, 70.47, 55.3, 58.98, and 19.14 MPa corresponding to 100% PBT, 5%, 10%, 15%, and 100% HDPE samples, respectively. Moreover, the SEM microstructure of PBT and HDPE indicates a two-phase heterogeneous mixture with little or no adhesion between these phases.

Study of Deep Cryogenic Treatment Process Effect on Microstructure and Properties of CuBeZr Alloy

The aim of this research was study the influence of the Deep Cryogenic Treatment (DCT) on the microstructure transformation and materials properties of beryllium copper alloy (CuBeZr alloy). Microstructure analysis such as size, shape and number of precipitates were studied by Optical microscopy (OM) and Scanning Electron Microscopy (SEM). Microstructure analysis showed that transformation into the rod shape precipitates appeared after the process. The dispersion of CuNi precipitates and CuNiZr precipitates in the ⍺ matrix after deep cryogenic treatment was found to be increased. The change in number of CuNi precipitates and CuNiZr precipitates led to an increase in hardness and wear resistance. The maximum increase in hardness of 11% was observed with 48 hours soaking time with a reduction in surface wear of approx. 60%.

Analysis on the Causes of Cracking at the Last Stage Blade of the Low-pressure Rotor in thermal power plant

Transverse cracking occurred in the blade body of the last stage of the low pressure rotor of a 200MW unit in a thermal power plant. The causes of blade cracking were analyzed by means of macro morphology, SEM, microstructure, mechanical properties, chemical composition and energy spectrum analysis. The results show that the corrosive Cl- accumulates on leaves, and then combined action of tensile stress is formed with the static load and dynamic load during the blade operation, and the stress corrosion microcracks had been conceived in the Cl- corrosion region. Under the long period cyclic excitation stress of the blade during the rotor rotation at high speed, the crack source extends in fatigue mode, finally resulting in cracking.

Optimization of Friction Surfacing Process Parameters on Low Carbon Steel Using Taguchi Approach

Friction surfacing is a solid-state coating technique process in which a mechtrode is rotated against the substrate under pressure, henceforth forming a coat on the substrate. This process not only can be used as coating process but it also provides flexibility in coating different materials as a revamp manufacturing process and it is suitable for getting excellent mechanical properties after the surfaced deposits. Bond strength is very good and these deposits are expected to serve better service life. The present work deals with mechtrode of SS-316, D3-tool steel and aa-2014 are coated on low carbon steel substrate by friction surfacing process and design of experiment were done by using taguchi L9 orthogonal array where the process parameters are mechtrode, rotational speed and traverse speed. The coating thickness, coating width and the SEM-microstructure analysis were studied.

Microstructures, interface structure and room temperature tensile properties of magnesium materials reinforced by high content submicron SiCp

The present work aims to research the treatment processing of magnesium reinforced with 1 μmsilicon carbide particle (SiCp) using stir casting combined by ultrasonic vibration. Present studies have been done on six different materials: (a) AZ31B alloy without particles, (b) 5 vol.% SiCp/AZ31B composites fabricated with different semi-solid stirring time (5 min, 10 min, 15 min and 20 min), (c) composite with 20 vol.% SiCp. The effects of 1 μm/SiCp pretreatment and stirring time on microstructure and interfacial wettability as well as mechanical properties of the materials were confirmed. Both short and long stirring time for the particle dispersion brought particle agglomeration. Results of SEM microstructure and tensile properties exhibited that the optimal stirring parameters of 625 °C/1500 rpm/15 min are exploited, and 20 vol.% SiCp/AZ31B composite was fabricated by the optimal stirring parameters. The application of optimal stirring parameters for the treatment resulted in homogeneous particle distribution. The addition of SiCp leads to a reduced matrix grain, and 20 vol.% SiCp/AZ31B composite showed smaller grain size than. 5 vol.% SiCp/AZ31B composite. The interface between SiCp and matrix is clear and interfacial wettability well. Tensile test results show that with increasing SiCp content, strengths increase while ductility decreases.

Ferroelectromagnetic Properties of PbFe1/2Nb1/2O3 (PFN) Material Synthesized by Chemical-Wet Technology

In this work, PbFe1/2Nb1/2O3 (PFN) ceramic samples synthesized by chemically wet method (precipitation from the solution) were obtained. Due to the tendency to form powder agglomerates, the synthesized powder was subjected to ultrasound. The sintering was carried out under various technological conditions, mainly through controlling the sintering temperature. -X-ray powder-diffraction (XRD), scanning electron microscope (SEM) microstructure analysis, as well as the examinations of dielectric, ferroelectric, and magnetic properties of the PFN ceramics were carried out. Studies have shown that hard ceramic agglomerates can be partially minimized by ultrasound. Due to this treatment, closed porosity decreases, and the ceramic samples have a higher density. Optimization and improvement of the technological process of the PFN material extends the possibility of its use for the preparation of multiferroic composites or multicomponent solid solutions based on PFN. Such materials with functional properties find applications in microelectronic applications, e.g., in systems integrating ferroelectric and magnetic properties in one device. The optimal synthesis conditions of PFN ceramics were determined to be 1050 °C/2 h.

Protective Properties of a Microstructure Composed of Barrier Nanostructured Organics and SiOx Layers Deposited on a Polymer Matrix

The SiOx barrier nanocoatings have been prepared on selected polymer matrices to increase their resistance against permeation of toxic substances. The aim has been to find out whether the method of vacuum plasma deposition of SiOx barrier nanocoatings on a polyethylene terephthalate (PET) foil used by Aluminium Company of Canada (ALCAN) company (ALCAN Packaging Kreuzlingen AG (SA/Ltd., Kreuzlingen, Switzerland) within the production of CERAMIS® packaging materials with barrier properties can also be used to increase the resistance of foils from other polymers against the permeation of organic solvents and other toxic liquids. The scanning electron microscopy (SEM) microstructure of SiOx nanocoatings prepared by thermal deposition from SiO in vacuum by the Plasma Assisted Physical Vapour Deposition (PA-PVD) method or vacuum deposition of hexamethyldisiloxane (HMDSO) by the Plasma-enhanced chemical vapour deposition (PECVD) method have been studied. The microstructure and behavior of samples when exposed to a liquid test substance in relation to the barrier properties is described.

Effect of WC Additive on Microstructural Evolution and Properties of TiC Steel-Bonded Carbide

TiC base high manganese steel-bonded carbide was manufactured by powder metallurgy technique, and the effect of adding mode of WC additive on microstructural evolution and properties of the alloy was studied. SEM microstructure showed that surrounding structure appeared obviousely with WC additive; while microstructure of the alloy was well-distributed and particle shape was distinct very much. The shape of TiC particles became irregular with pure WC powder addition, and irregular with further increase of WC content, and the shape of some TiC particles became angular because of excessive reaction between TiC particles and WC additive. microstructure of the alloy was refiner and the strength, toughness were improved with the increase of WC addition. (Ti, W)C solid solution is superior to form on the surface of TiC particles through dissolution precipitation mechanism because the activity energy of WC was higher than that of TiC-WC compound carbides when WC was added in the alloy, and the particle shape of TiC became more irregular and the properties were improved significantly.

Production of oxide coatings by sol-gel method and electrophoresis

The paper reports the results of depositing SiO2 and SiO2-TiO2 coatings on titanium alloy Ti-6Al-4V ELI (ASTM-grade 5). Oxide coatings were deposited onto the titanium alloy substrate by sol-gel method and by electrophoresis. The produced coatings were chemically uniform, compact and highly dense. We then performed SEM microstructure examination, as well as microhardness and surface roughness measurements for different coating combinations. The significance of the results was assessed by the Shapiro-Wilk and t-Student tests using the STATISTICA software. It has been found that there are statistically significant differences in the hardness of SiO2 and SiO2-TiO2 coatings. The results of roughness parameters reveal significant differences only for individual coatings.