The effects of strain and strain rate on residual microstructures in copper

Author(s):  
M. F. Stevens ◽  
P. S. Follansbee

The strain rate sensitivity of a variety of materials is known to increase rapidly at strain rates exceeding ∼103 sec-1. This transition has most often in the past been attributed to a transition from thermally activated guide to viscous drag control. An important condition for imposition of dislocation drag effects is that the applied stress, σ, must be on the order of or greater than the threshold stress, which is the flow stress at OK. From Fig. 1, it can be seen for OFE Cu that the ratio of the applied stress to threshold stress remains constant even at strain rates as high as 104 sec-1 suggesting that there is not a mechanism transition but that the intrinsic strength is increasing, since the threshold strength is a mechanical measure of intrinsic strength. These measurements were made at constant strain levels of 0.2, wnich is not a guarantee of constant microstructure. The increase in threshold stress at higher strain rates is a strong indication that the microstructural evolution is a function of strain rate and that the dependence becomes stronger at high strain rates.

2013 ◽  
Vol 2013 ◽  
pp. 1-5
Author(s):  
Tao-Hsing Chen ◽  
Chih-Kai Tsai ◽  
Te-Hua Fang

The high strain shear rate behaviour of Inconel 690 alloy was investigated by using the split Hopkinson torsional bar. The shear strain rates were tested at 900 s−1, 1900 s−1, and 2600 s−1and at temperatures of −100°C, 25°C, and 300°C, respectively. It was found that the dynamic shear behaviour of Inconel 690 alloy was sensitive to strain rate and temperature. The fracture shear strain increased with increasing strain rate and temperature. In addition, the strain rate sensitivity was increased with increasing strain and strain rate but decreased with increasing temperature. Finally, the fracture surfaces were found to contain dimple-like features, and the dimple density increased with increasing strain rate and temperature.


2012 ◽  
Vol 535-537 ◽  
pp. 353-356
Author(s):  
Li Yuan Qin ◽  
Jian She Lian ◽  
Long Zhe Quan ◽  
En Chen Jiang

A fully dense nanocrystalline Ni-Co alloy with 18 nm grain size exhibited high strength of about 2200 MPa and ductility of 8.19.2% at strain rates of 1.04×10-5 to 1.04 s-1 and room temperature. The alloying of Co element induces the grain refinement, solid solution hardening and decrease of stacking fault energy should contribute to the favorable combination of mechanical performance. The obvious distinctions of fracture-surface morphologies with strain rate alteration were attributed to underlying deformation mechanism transition. The high strain rate sensitivity exponent and small activation volume indicate that grain boundary activity may be expected in this alloy.


1999 ◽  
Vol 601 ◽  
Author(s):  
D. Kum ◽  
W. J. Kim

AbstractUltra-fine microstructure consisting of equiaxed Al-grains and aluminide particulate was produced by powder metallurgy process using gas-atomized powders of Al-10wt%Ti-2wt%Fe alloy. High strain rate superplasticity (HSRS) has been investigated at 873-923K and strain rates higher than 10−3s−1 in tension, and total elongation up to 500% was observed at the strain-rate of 10−1s−1. The strain rate vs. flow stress behavior exhibits the typical aspect of HSRS such as the increase of strain-rate sensitivity exponent with increase in strain-rate and an apparent activation energy higher than that for lattice diffusion in aluminum. The concept of threshold stress has been incorporated to illustrate the HSRS behavior, where the stress exponent of 3 describes the experimental data. The determined threshold stress showed strong temperature dependency as in the case of a similarly processed Al-10wt%Ti alloy, which exhibited the stress exponent of 2 in the same testing conditions. Solute drag mechanism has been postulated for the Al-Ti-Fe alloy.


2006 ◽  
Vol 503-504 ◽  
pp. 31-36 ◽  
Author(s):  
Johannes Mueller ◽  
Karsten Durst ◽  
Dorothea Amberger ◽  
Matthias Göken

The mechanical properties of ultrafine-grained metals processed by equal channel angular pressing is investigated by nanoindentations in comparison with measurements on nanocrystalline nickel with a grain size between 20 and 400 nm produced by pulsed electrodeposition. Besides hardness and Young’s modulus measurements, the nanoindentation method allows also controlled experiments on the strain rate sensitivity, which are discussed in detail in this paper. Nanoindentation measurements can be performed at indentation strain rates between 10-3 s-1 and 0.1 s-1. Nanocrystalline and ultrafine-grained fcc metals as Al and Ni show a significant strain rate sensitivity at room temperature in comparison with conventional grain sized materials. In ultrafine-grained bcc Fe the strain rate sensitivity does not change significantly after severe plastic deformation. Inelastic effects are found during repeated unloading-loading experiments in nanoindentations.


2011 ◽  
Vol 82 ◽  
pp. 124-129 ◽  
Author(s):  
Ezio Cadoni ◽  
Matteo Dotta ◽  
Daniele Forni ◽  
Stefano Bianchi

In this paper the first results of the mechanical characterization in tension of two high strength alloys in a wide range of strain rates are presented. Different experimental techniques were used for different strain rates: a universal machine, a Hydro-Pneumatic Machine and a JRC-Split Hopkinson Tensile Bar. The experimental research was developed in the DynaMat laboratory of the University of Applied Sciences of Southern Switzerland. An increase of the stress at a given strain increasing the strain-rate from 10-3 to 103 s-1, a moderate strain-rate sensitivity of the uniform and fracture strain, a poor reduction of the cross-sectional area at fracture with increasing the strain-rate were shown. Based on these experimental results the parameters required by the Johnson-Cook constitutive law were determined.


1992 ◽  
Vol 59 (3) ◽  
pp. 485-490 ◽  
Author(s):  
P. Tugˇcu

The plane-strain tension test is analyzed numerically for a material with strain and strain-rate hardening characteristics. The effect of the prescribed rate of straining is investigated for an additive logarithmic description of the material strain-rate sensitivity. The dependency to the imposed strain rate so introduced is shown to have a significant effect on several features of the load-elongation curve such as the attainment of the load maximum, the onset of localization, and the overall engineering strain.


2018 ◽  
Vol 183 ◽  
pp. 04005 ◽  
Author(s):  
Bar Nurel ◽  
Moshe Nahmany ◽  
Adin Stern ◽  
Nahum Frage ◽  
Oren Sadot

Additive manufacturing by Selective Laser Melting of metals is attracting substantial attention, due to its advantages, such as short-time production of customized structures. This technique is useful for building complex components using a metallic pre-alloyed powder. One of the most used materials in AMSLM is AlSi10Mg powder. Additively manufactured AlSi10Mg may be used as a structural material and it static mechanical properties were widely investigated. Properties in the strain rates of 5×102–1.6×103 s-1 and at higher strain rates of 5×103 –105 s-1 have been also reported. The aim of this study is investigation of dynamic properties in the 7×102–8×103 s-1 strain rate range, using the split Hopkinson pressure bar technique. It was found that the dynamic properties at strain-rates of 1×103–3×103 s-1 depend on a build direction and affected by heat treatment. At higher and lower strain-rates the effect of build direction is limited. The anisotropic nature of the material was determined by the ellipticity of samples after the SHPB test. No strain rate sensitivity was observed.


2018 ◽  
Vol 183 ◽  
pp. 02037 ◽  
Author(s):  
Taamjeed Rahmaan ◽  
Ping Zhou ◽  
Cliff Butcher ◽  
Michael J. Worswick

Shear tests were performed at strain rates ranging from quasi-static (0.01 s-1) to 500 s-1 for AA7075-T6 sheet metal alloy at room temperature. A miniature sized shear specimen was used in this work to perform high strain rate shear testing. Digital image correlation (DIC) techniques were employed to measure the strains in the experiments. At maximum in-plane shear strains greater than 20%, the AA7075-T6 alloy demonstrated a reduced work hardening rate at elevated strain rates. At lower strains, the AA7075-T6 alloy showed mild positive rate sensitivity. The strain to localization (using the Zener-Holloman criterion), measured using the DIC technique, decreased with strain rate in shear loading. The strain at complete failure, however, exhibited an increase at the highest strain rate (500 s-1). The current work also focused on characterization of the thermal conditions occurring during high rate loading in shear with in situ high speed thermal imaging. Experimental results from the highest strain rate (500 s-1) tests showed a notable increase in temperature within the specimen gauge region as a result of the conversion of plastic deformation energy into heat.


2019 ◽  
Vol 2019 (1) ◽  
pp. 000480-000487
Author(s):  
Luke A. Wentlent ◽  
James Wilcox ◽  
Xuanyi Ding

Abstract As the electronics industry continues to evolve a concerted effort has developed to implement lower melting point solders. The ability to minimize the thermal exposure that an assembly is subjected to affords significant benefits with respect to both the reliability and the materials that can be used. One of the most popular low melt solder alloys currently being investigated by the industry is the Bi-Sn eutectic system, which has a melting point of 139°C. The BiSn system itself is not particularly novel as it was posited as a SAC alternative during the initial shift from Pb based solders. While a body of knowledge currently exists regarding this system, and the near eutectic variant BiSnAg, there are still concerns regarding its ductility, especially as a function of thermal exposure and strain rate. Bismuth is widely acknowledged as a brittle element and its presence in such quantities raises concerns of not just Cu6Sn5 embrittlement but also solder fragility in high strain rate types of environments. A challenge with regards to near term implementation is that most packages are not available with BiSn solder bumps. Therefore, it will be necessary to use components already balled with SAC 305 solder. This means that the resulting solder interconnect, reflowed below conventional SAC reflow temperatures, will form a type of mixed hybrid microstructure. This non-equilibrium microstructure will be composed of two regions, one Bi-rich region which is well past saturation and a second region which is Bi-deficient. It is of specific industrial interest then to not just investigate the BiSn solder system but also within the context of a realistic mixed interconnect. Recent work by several researchers has shown that this hybrid microstructure is unstable and quite active with respect to the movement and localized concentration of the Bismuth. The degree of mixing of these two regions has been shown to be highly dependent upon reflow temperature and the paste to ball volume ratio. Mixed SAC-BiSn solder joints were formed by placing SAC 305 spheres on BiSn paste deposits for a paste to ball volume ratio of .18. These samples were then reflowed at either 175°C or 200°C. SAC 305 control samples were also made using a conventional Pb-free reflow profile with a peak temperature of 247°C. A 22 mil Cu-OSP pad on a 1.0 mm thick FR4 substrate was used for all samples. A selection of the solder joints were then isothermally aged at 90°C for 200 hours. Using a joint level micromechanical tester, ball shear tests were conducted at a range of strain rates for samples in the as-reflowed and aged state. Using this information, the strain rate sensitivity of the interconnects was mapped and correlated with the observed failure modes. Investigations into the fracture mechanisms were conducted by examining the shear fracture surface with optical and scanning electron microscopy. Additionally, the evolution of the microstructure was characterized. Results showed a clear transition from ductile solder failure to a brittle separation failure at the higher strain rates.


Metals ◽  
2019 ◽  
Vol 9 (3) ◽  
pp. 344 ◽  
Author(s):  
Simon Sevsek ◽  
Christian Haase ◽  
Wolfgang Bleck

The strain-rate-dependent deformation behavior of an intercritically annealed X6MnAl12-3 medium-manganese steel was analyzed with respect to the mechanical properties, activation of deformation-induced martensitic phase transformation, and strain localization behavior. Intercritical annealing at 675 °C for 2 h led to an ultrafine-grained multi-phase microstructure with 45% of mostly equiaxed, recrystallized austenite and 55% ferrite or recovered, lamellar martensite. In-situ digital image correlation methods during tensile tests revealed strain localization behavior during the discontinuous elastic-plastic transition, which was due to the localization of strain in the softer austenite in the early stages of plastic deformation. The dependence of the macroscopic mechanical properties on the strain rate is due to the strain-rate sensitivity of the microscopic deformation behavior. On the one hand, the deformation-induced phase transformation of austenite to martensite showed a clear strain-rate dependency and was partially suppressed at very low and very high strain rates. On the other hand, the strain-rate-dependent relative strength of ferrite and martensite compared to austenite influenced the strain partitioning during plastic deformation, and subsequently, the work-hardening rate. As a result, the tested X6MnAl12-3 medium-manganese steel showed a negative strain-rate sensitivity at very low to medium strain rates and a positive strain-rate sensitivity at medium to high strain rates.


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