A Comparison of the Processing Routes on the Properties of Mg Reinforced With Nanosize MgO

Author(s):  
C. S. Goh ◽  
J. Wei ◽  
M. Gupta

Powder metallurgy and liquid metallurgy techniques were used to fabricate Mg reinforced with different volume fraction of nano-size MgO particles. A higher volume fraction of MgO particles could be added into the Mg matrix when the liquid metallurgy technique was used. Microstructural analysis was carried out to examine the distribution of the nanoparticles in the Mg matrix when different processing routes were chosen. Individual particles together with sparsely distributed agglomerations could be discerned in the Mg matrix for both processing routes. Mechanical properties results revealed that a more substantial improvement in macrohardness and tensile properties could be achieved by using the liquid metallurgy route where a higher amount of nano-size MgO particles could be incorporated.

Materials ◽  
2005 ◽  
Author(s):  
C. S. Goh ◽  
J. Wei ◽  
M. Gupta

Magnesium nanocomposites with 0.1, 0.2, 0.3 and 0.4 volume percentages of MgO were synthesized using the powder metallurgy technique. The nanocomposite billets obtained were subsequently hot extruded at a temperature of 350 °C with an extrusion ratio of 20.25:1. The extruded nanocomposites were characterized for their microstructural, physical and mechanical properties. The microstructures of the nanocomposites showed individual particles of MgO uniformly distributed in the magnesium matrix. The thermomechanical analysis results revealed that a more thermally stable magnesium nanocomposite could be obtained with a threshold amount of MgO. The tensile properties results indicated that the yield strength peaks at 0.3 vol.% of reinforcement incorporated, with an improvement of approximately 17%. An attempt is made to correlate the volume fraction of the MgO with the resultant physical and mechanical properties of the magnesium nanocomposites.


Author(s):  
S. M. L. Nai ◽  
J. Wei ◽  
M. Gupta

In the present study, using powder metallurgy route, varying volume fraction of ZrO2 stabilized with 8 mol.% of Y2O3 particulates were incorporated into Sn-3.5Ag-0.7Cu solder to develop nanocomposite solders. The samples were extruded and characterized in terms of microstructural and tensile properties. With the addition of nano length scale reinforcement, the results revealed an improvement in 0.2% yield strength (upto ∼ 39%) and ultimate tensile strength (upto ∼ 43%), when compared with that of monolithic Sn-Ag-Cu solder. An attempt is made in this study to interrelate the tensile behavior of Sn-Ag-Cu with the presence of nano-size reinforcement.


Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 906
Author(s):  
Dong Han ◽  
Yongqing Zhao ◽  
Weidong Zeng

The present study focuses on the effect of 1% Zr addition on the microstructure, tensile properties and superplasticity of a forged SP700 alloy. The results demonstrated that Zr has a significant effect on inhibiting the microstructural segregation and increasing the volume fraction of β-phase in the forged SP700 alloy. After annealing at 820 °C for 1 h and aging at 500 °C for 6 h, the SP700 alloy with 1% Zr showed a completely globular and fine microstructure. The yield strength, ultimate tensile strength and tensile elongation of the alloy with optimized microstructure were 1185 MPa, 1296 MPa and 10%, respectively. The superplastic deformation was performed at 750 °C with an elongation of 1248%. The improvement of tensile properties and superplasticity of the forged SP700 alloy by Zr addition was mainly attributed to the uniform and fine globular microstructures.


Nanomaterials ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 1024 ◽  
Author(s):  
Milad Haghighi ◽  
Mohammad Shaeri ◽  
Arman Sedghi ◽  
Faramarz Djavanroodi

The effect of graphene nanosheet (GNS) reinforcement on the microstructure and mechanical properties of the titanium matrix composite has been discussed. For this purpose, composites with various GNS contents were prepared by cold pressing and sintering at various time periods. Density calculation by Archimedes’ principle revealed that Ti/GNSs composites with reasonable high density (more than 99.5% of theoretical density) were produced after sintering for 5 h. Microstructural analysis by X-ray diffraction (XRD) and a field emission scanning electron microscope (FESEM) showed that TiC particles were formed in the matrix during the sintering process as a result of a titanium reaction with carbon. Higher GNS content as well as sintering time resulted in an increase in TiC particle size and volume fraction. Microhardness and shear punch tests demonstrated considerable improvement of the specimens’ mechanical properties with the increment of sintering time and GNS content up to 1 wt. %. The microhardness and shear strength of 1 wt. % GNS composites were enhanced from 316 HV and 610 MPa to 613 HV and 754 MPa, respectively, when composites sintered for 5 h. It is worth mentioning that the formation of the agglomerates of unreacted GNSs in 1.5 wt. % GNS composites resulted in a dramatic decrease in mechanical properties.


Author(s):  
M. A. Salem ◽  
I. G. El-Batanony ◽  
M. Ghanem ◽  
Mohamed Ibrahim Abd ElAal

Different Al-SiC metal matrix composites (MMCs) with a different matrix, reinforcement sizes, and volume fractions were fabricated using ball milling (BM) and powder metallurgy (PM) techniques. Al and Al-SiC composites with different volume fractions were milled for 120 h. Then, the Al and Al-SiC composites were pressed under 125 MPa and finally sintered at 450 °C. Moreover, microsize and combination between micro and nano sizes Al-SiC samples were prepared by the same way. The effect of the Al matrix, SiC reinforcement sizes and the SiC volume fraction on the microstructure evolution, physical and mechanical properties of the produced composites was investigated. The BM and powder metallurgy techniques followed by sintering produce fully dense Al-SiC composite samples with different matrix and reinforcement sizes. The SiC particle size was observed to have a higher effect on the thermal conductivity, electrical resistivity, and microhardness of the produced composites than that of the SiC volume fraction. The decreasing of the Al and SiC particle sizes and increasing of the SiC volume fraction deteriorate the physical properties. On the other hand, the microhardness was enhanced with the decreasing of the Al, SiC particle sizes and the increasing of the SiC volume fraction.


2007 ◽  
Vol 546-549 ◽  
pp. 499-502
Author(s):  
X. Qiu ◽  
Xiao Jun Wang ◽  
Ming Yi Zheng ◽  
Kun Wu

The fabrication processing, mechanical properties and fracture characters of SiCp/AZ91 magnesium matrix composites fabricated by squeeze casting were investigated. The SiC particles with different diameters (5μm, 20μm and 50μm) were employed as the reinforcement in the composites, the volume fraction of them was 50% in all cases. Experimental results showed that when the size of SiC particle decreased, the tensile properties of the composite increased. The tensile properties of SiCp/AZ91 composite with small particles are controlled by the properties of matrix alloy and the strength of the interface between the matrix and reinforcements, but the composites reinforced by large particles are controlled by the fracture of the particles.


Metals ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 1483
Author(s):  
Jinxin Zang ◽  
Pan Dai ◽  
Yanqing Yang ◽  
Shuai Liu ◽  
Bin Huang ◽  
...  

The requirement for 7085 Al alloy as large airframe parts has been increasing due to its low quenching sensitivity and high strength. However, the relationship between high temperature mechanical properties and the evolution of precipitates in hot environments is still unclear. In this work, thermal exposure followed by tensile tests were conducted on the 7085 Al alloy at various temperatures (100 °C, 125 °C, 150 °C and 175 °C). Variations of hardness, electrical conductivity and tensile properties were investigated. The evolution of the nano scale precipitates was also quantitatively characterized by transmission electron microscopy (TEM). The results show that the hardness and electrical conductivity of the alloy are more sensitive to the temperature than to the time. The strength decreases continuously with the increase of temperature due to the transformation from η′ to η phase during the process. Furthermore, the main η phase in the alloy transformed from V3 and V4 to V1 and V2 variants when the temperature was 125 °C. Additionally, with increasing the temperature, the average precipitate radius increased, meanwhile the volume fraction and number density of the precipitates decreased. The strengthening effect of nano scale precipitates on tensile properties of the alloy was calculated and analyzed.


Entropy ◽  
2019 ◽  
Vol 21 (5) ◽  
pp. 448 ◽  
Author(s):  
Cui Zhang ◽  
Bin Liu ◽  
Yong Liu ◽  
Qihong Fang ◽  
Wenmin Guo ◽  
...  

A CoCrFeNiMo0.2 high entropy alloy (HEA) was prepared through powder metallurgy (P/M) process. The effects of annealing on microstructural evolution and mechanical properties of P/M HEAs were investigated. The results show that the P/M HEA exhibit a metastable FCC single-phase structure. Subsequently, annealing causes precipitation in the grains and at the grain boundaries simultaneously. As the temperature increases, the size of the precipitates grows, while the content of the precipitates tends to increase gradually first, and then decrease as the annealing temperature goes up to 1000 °C. As the annealing time is prolonged, the size and content of the precipitates gradually increases, eventually reaching a saturated stable value. The mechanical properties of the annealed alloys have a significant correspondence with the precipitation behavior. The larger the volume fraction and the size of the precipitates, the higher the strength and the lower the plasticity of the HEA. The CoCrFeNiMo0.2 high entropy alloy, which annealed at 800 °C for 72 h, exhibited the most excellent mechanical properties with the ultimate tensile strength of about 850 MPa and an elongation of about 30%. Nearly all of the annealed HEAs exhibit good strength–ductility combinations due to the significant precipitation enhancement and nanotwinning. The separation of the coarse precipitation phase and the matrix during the deformation process is the main reason for the formation of micropores. Formation of large volume fraction of micropores results in a decrease in the plasticity of the alloy.


2012 ◽  
Vol 05 ◽  
pp. 607-614 ◽  
Author(s):  
Mohammad Amin Baghchesara ◽  
Hossein Abdizadeh ◽  
Hamid Reza Baharvandi

The objective of the present investigation was to evaluate the microstructural and mechanical properties of Al /nano MgO composite prepared via powder metallurgy method. Pure atomized aluminum powder with an average particle size of 1μm and MgO particulate with an average particle size between 60 to 80 nm were used. Composites containing 1.5, 2.5 and 5 percent of volume fraction of MgO were prepared by powder metallurgy method. The specimens were pressed by Cold Isostatic Press machine (CIP), subsequently were sintered at 575, 600 and 625°C. After sintering and preparing the samples, mechanical properties were measured. The results of microstructure, compression and hardness tests indicated that addition of MgO particulates to aluminum matrix composites improves the mechanical properties.


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