scholarly journals Features of the electrophysical and mechanical properties of n-component ferroactive solid solutions of composition PZT–PZN–PMN

2021 ◽  
pp. 2160001
Author(s):  
K. P. Andryushin ◽  
I. N. Andryushina ◽  
A. V. Cherpakov ◽  
A. V. Popov ◽  
I. A. Verbenko ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Mechanical Strength ◽  
Solid Solutions ◽  
Strontium Content ◽  
Average Grain Size ◽  
Polarization Characteristics ◽  
Fatigue Endurance

Study of the fatigue endurance and mechanical strength of solid solutions of the PZT–PZN–PMN system, modified with Ba and Sr, corresponding to the formula (Pb[Formula: see text]Sr[Formula: see text]Ba[Formula: see text] [Ti[Formula: see text]Zr[Formula: see text](Nb[Formula: see text]Zn[Formula: see text] (Nb[Formula: see text]Mg[Formula: see text]]O3, with [Formula: see text] = 0.02 ÷ 0.12; [Formula: see text] = 0.02, [Formula: see text] = 0.0036 ÷ 0.073; [Formula: see text]= 0.385 ÷ 0.430, [Formula: see text]= 0.402 ÷ 0.447 is presented. It is shown that the evolution of the polarization characteristics with an increase in the number of repolarization cycles, [Formula: see text], is characterized by two sections: slow fatigue and logarithmic evolution. It was found that an increase in the strontium content shifts the beginning of the logarithmic stage towards to the large [Formula: see text]. It is shown that an increase in the average grain size decreases the mechanical strength. A conclusion is made about the expediency of using the obtained data in the development of devices operating in power modes.

Surface Modification and its Influence on the Microstructure and Creep Resistance of Nickel Based Superalloy René 77 / Modyfikacja Powierzchniowa Oraz Jej Wpływ Na Mikrostrukture I Wytrzymałosc Na Pełzanie Odlewów Z Nadstopu Niklu Ren´E 77

2013 ◽  
Vol 58 (1) ◽  
pp. 95-98 ◽  
Author(s):  
M. Zielinska ◽  
J. Sieniawski
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Surface Modification ◽  
Turbine Blades ◽  
Processing Parameters ◽  
Grain Structure ◽  
Creep Tests ◽  
Cobalt Aluminate ◽  
Nickel Based Superalloy ◽  
Average Grain Size

Superalloy René 77 is very wide used for turbine blades, turbine disks of aircraft engines which work up to 1050°C. These elements are generally produced by the investment casting method. Turbine blades produced by conventional precision casting methods have coarse and inhomogeneous grain structure. Such a material often does not fulfil basic requirements, which concern mechanical properties for the stuff used in aeronautical engineering. The incorporation of controlled grain size improved mechanical properties. This control of grain size in the casting operation was accomplished by the control of processing parameters such as casting temperature, mould preheating temperature, and the use of grain nucleates in the face of the mould. For nickel and cobalt based superalloys, it was found that cobalt aluminate (CoAl2O4) has the best nucleating effect. The objective of this work was to determine the influence of the inoculant’s content (cobalt aluminate) in the surface layer of the ceramic mould on the microstructure and mechanical properties at high temperature of nickel based superalloy René 77. For this purpose, the ceramic moulds were made with different concentration of cobalt aluminate in the primary slurry was from 0 to 10% mass. in zirconium flour. Stepped and cylindrical samples were casted for microstructure and mechanical examinations. The average grain size of the matrix ( phase), was determined on the stepped samples. The influence of surface modification on the grain size of up to section thickness was considered. The microstructure investigations with the use of light microscopy and scanning electron microscopy (SEM) enable to examine the influence of the surface modification on the morphology of ’ phase and carbides precipitations. Verification of the influence of CoAl2O4 on the mechanical properties of castings were investigated on the basis of results obtained form creep tests.

scholarly journals Development of Al–Mg–Si alloy performance by addition of grain refiner Al–5Ti–1B alloy

2021 ◽  
Vol 104 (2) ◽  
pp. 003685042110294
Author(s):  
Khaled Abd El-Aziz ◽  
Emad M Ahmed ◽  
Abdulaziz H Alghtani ◽  
Bassem F Felemban ◽  
Hafiz T Ali ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Corrosion Resistance ◽  
Testing Machine ◽  
Dendritic Structure ◽  
Grain Refiner ◽  
Corrosion Properties ◽  
Average Grain Size ◽  
Structural Applications ◽  
Alloy Addition

Aluminum alloys are the most essential part of all shaped castings manufactured, mainly in the automotive, food industry, and structural applications. There is little consensus as to the precise relationship between grain size after grain refinement and corrosion resistance; conflicting conclusions have been published showing that reduced grain size can decrease or increase corrosion resistance. The effect of Al–5Ti–1B grain refiner (GR alloy) with different percentages on the mechanical properties and corrosion behavior of Aluminum-magnesium-silicon alloy (Al–Mg–Si) was studied. The average grain size is determined according to the E112ASTM standard. The compressive test specimens were made as per ASTM: E8/E8M-16 standard to get their compressive properties. The bulk hardness using Vickers hardness testing machine at a load of 50 g. Electrochemical corrosion tests were carried out in 3.5 % NaCl solution using Autolab Potentiostat/Galvanostat (PGSTAT 30).The grain size of the Al–Mg–Si alloy was reduced from 82 to 46 µm by the addition of GR alloy. The morphology of α-Al dendrites changes from coarse dendritic structure to fine equiaxed grains due to the addition of GR alloy and segregation of Ti, which controls the growth of primary α-Al. In addition, the mechanical properties of the Al–Mg–Si alloy were improved by GR alloy addition. GR alloy addition to Al–Mg–Si alloy produced fine-grained structure and better hardness and compressive strength. The addition of GR alloy did not reveal any marked improvements in the corrosion properties of Al–Mg–Si alloy.

Vibratory weld conditioning during gas tungsten arc welding of al 5052 alloy on the mechanical and micro-structural behavior

2020 ◽  
Vol 17 (6) ◽  
pp. 831-836
Author(s):  
M. Vykunta Rao ◽  
Srinivasa Rao P. ◽  
B. Surendra Babu
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Tensile Strength ◽  
Ultimate Tensile Strength ◽  
Welded Joints ◽  
Great Influence ◽  
Welding Process ◽  
Microstructural Characterization ◽  
Content Type ◽  
Average Grain Size

Purpose Vibratory weld conditioning parameters have a great influence on the improvement of mechanical properties of weld connections. The purpose of this paper is to understand the influence of vibratory weld conditioning on the mechanical and microstructural characterization of aluminum 5052 alloy weldments. An attempt is made to understand the effect of the vibratory tungsten inert gas (TIG) welding process parameters on the hardness, ultimate tensile strength and microstructure of Al 5052-H32 alloy weldments. Design/methodology/approach Aluminum 5052 H32 specimens are welded at different combinations of vibromotor voltage inputs and time of vibrations. Voltage input is varied from 50 to 230 V at an interval of 10 V. At each voltage input to the vibromotor, there are three levels of time of vibration, i.e. 80, 90 and 100 s. The vibratory TIG-welded specimens are tested for their mechanical and microstructural properties. Findings The results indicate that the mechanical properties of aluminum alloy weld connections improved by increasing voltage input up to 160 V. Also, it has been observed that by increasing vibromotor voltage input beyond 160 V, mechanical properties were reduced significantly. It is also found that vibration time has less influence on the mechanical properties of weld connections. Improvement in hardness and ultimate tensile strength of vibratory welded joints is 16 and 14%, respectively, when compared without vibration, i.e. normal weld conditions. Average grain size is measured as per ASTM E 112–96. Average grain size is in the case of 0, 120, 160 and 230 is 20.709, 17.99, 16.57 and 20.8086 µm, respectively. Originality/value Novel vibratory TIG welded joints are prepared. Mechanical and micro-structural properties are tested.

Microstructures and Mechanical Properties of AZ61 Mg Alloy Processed by Equal Channel Angular Pressing

2012 ◽  
Vol 468-471 ◽  
pp. 2124-2127 ◽  
Author(s):  
Shao Feng Zeng ◽  
Kai Huai Yang ◽  
Wen Zhe Chen
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Equal Channel Angular Pressing ◽  
Uniform Elongation ◽  
Considerable Decrease ◽  
Angular Pressing ◽  
Az61 Magnesium Alloy ◽  
Average Grain Size ◽  
Microstructures And Mechanical Properties ◽  
Bimodal Grain Size

Equal channel angular pressing (ECAP) was applied to a commercial AZ61 magnesium alloy for up to 8 passes at temperatures as low as 473K. Microstructures and mechanical properties of as-received and ECAP deformed samples were investigated. The microstructure was initially not uniform with a “bimodal” grain size distribution but became increasingly homogeneous with further ECAP passes and the average grain size was considerably reduced from over 26 μm to below 5 μm. The ultimate tensile strength (UTS) decreases clearly after one pass, but increases significantly up to two passes, and then continuously slowly decreases up to six passes, and again increases slightly up to eight passes. In contrast, the uniform elongation increased significantly up to 3 passes, followed by considerable decrease up to 8 passes. These observations may be attributed to combined effects of grain refinement and texture development.

scholarly journals Influence of Steel Grain Size on Residual Stress in Grinding Processing

2010 ◽  
Vol 638-642 ◽  
pp. 2389-2394 ◽  
Author(s):  
Masahide Gotoh ◽  
Katsuhiro Seki ◽  
M. Shozu ◽  
Hajime Hirose ◽  
Toshihiko Sasaki
Keyword(s):  
Mechanical Properties ◽  
Residual Stress ◽  
Grain Size ◽  
Stress State ◽  
Mechanical Grinding ◽  
Fine Grained ◽  
Residual Stress State ◽  
Analysis Methods ◽  
Average Grain Size ◽  
Fine Grained Steels

The fine-grained rolling steels NFG600 and the conventional usual rolling steels SM490 were processed by sand paper polishing and mechanical grinding to compare the residual stress generated after processing. The average grain size of NFG600 and SM490 is 3 μm and 15μm respectively. Therefore improvement of mechanical properties for such fine-grained steels is expected, it is important to understand the residual stress state of new fine-grained materials with processing. In this study, multi axial stresses of two kinds of specimens after polishing and grinding were measured by three kinds of analysis methods including cos-ψ method. As a result, as for σ33, the stress of NFG was compression, though that of SM490 was tension.

Effect of Li on Mechanical Properties and Electrical Conductivity of the Al–Zn–Cu–Mg Based Alloys

2021 ◽  
Vol 21 (9) ◽  
pp. 4897-4901
Author(s):  
Hyo-Sang Yoo ◽  
Yong-Ho Kim ◽  
Hyeon-Taek Son
Keyword(s):  
Mechanical Properties ◽  
Electrical Conductivity ◽  
Grain Size ◽  
Tensile Strength ◽  
Spherical Particles ◽  
Al Alloy ◽  
High Angle ◽  
Average Grain Size ◽  
Strength Improvement ◽  
Li Content

In this study, changes in the microstructure, mechanical properties, and electrical conductivity of cast and extruded Al–Zn–Cu–Mg based alloys with the addition of Li (0, 0.5 and 1.0 wt.%) were investigated. The Al–Zn–Cu–Mg–xLi alloys were cast and homogenized at 570 °C for 4 hours. The billets were hot extruded into rod that were 12 mm in diameter with a reduction ratio of 38:1 at 550 °C. As the amount of Li added increased from 0 to 1.0 wt.%, the average grain size of the extruded Al alloy increased from 259.2 to 383.0 µm, and the high-angle grain boundaries (HGBs) fraction decreased from 64.0 to 52.1%. As the Li content increased from 0 to 1.0 wt.%, the elongation was not significantly different from 27.8 to 27.4% and the ultimate tensile strength (UTS) was improved from 146.7 to 160.6 MPa. As Li was added, spherical particles bonded to each other, forming an irregular particles. It is thought that these irregular particles contribute to the strength improvement.

scholarly journals Formation and Properties of the Ta-Y2O3, Ta-ZrO2, and Ta-TaC Nanocomposites

2018 ◽  
Vol 2018 ◽  
pp. 1-12
Author(s):  
J. Jakubowicz ◽  
M. Sopata ◽  
G. Adamek ◽  
P. Siwak ◽  
T. Kachlicki
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Mechanical Alloying ◽  
Young’S Modulus ◽  
Young's Modulus ◽  
Ceramic Composites ◽  
Ceramic Phase ◽  
Plasma Sintering ◽  
Average Grain Size ◽  
Bulk Nanocrystalline

The nanocrystalline tantalum-ceramic composites were made using mechanical alloying followed by pulse plasma sintering (PPS). The tantalum acts as a matrix, to which the ceramic reinforced phase in the concentration of 5, 10, 20, and 40 wt.% was introduced. Oxides (Y2O3 and ZrO2) and carbides (TaC) were used as the ceramic phase. The mechanical alloying results in the formation of nanocrystalline grains. The subsequent hot pressing in the mode of PPS results in the consolidation of powders and formation of bulk nanocomposites. All the bulk composites have the average grain size from 40 nm to 100 nm, whereas, for comparison, the bulk nanocrystalline pure tantalum has the average grain size of approximately 170 nm. The ceramic phase refines the grain size in the Ta nanocomposites. The mechanical properties were studied using the nanoindentation tests. The nanocomposites exhibit uniform load-displacement curves indicating good integrity and homogeneity of the samples. Out of the investigated components, the Ta-10 wt.% TaC one has the highest hardness and a very high Young’s modulus (1398 HV and 336 GPa, resp.). For the Ta-oxide composites, Ta-20 wt.% Y2O3 has the highest mechanical properties (1165 HV hardness and 231 GPa Young’s modulus).

Properties of Nanoscaled Multiphase Structures and Non-Equilibrium Solid Solutions Obtained by Severe Plastic Deformation [Abstract + Supplemental Data]

2006 ◽  
Vol 977 ◽  
Author(s):  
Xavier Sauvage ◽  
Xavier Quelennec ◽  
Peter Jessner ◽  
Florian Wetscher ◽  
Reinhard Pippan
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
Grain Size ◽  
Severe Plastic Deformation ◽  
Solid Solutions ◽  
Atom Probe ◽  
Size Reduction ◽  
Pure Metals ◽  
Pure Cu ◽  
Non Equilibrium

AbstractGrain size reduction induced by severe plastic deformation (SPD) and the resulting mechanical properties have been widely investigated for pure metals but less is known and reported about multi-phase materials. To study the grain size reduction mechanisms in multiphase structure subjected to SPD, two copper based composites (Cu-10%Fe and Cu-43%Cr) were severely deformed by torsion under high pressure. The grain size achieved with these composite materials is much smaller than in pure metals. It is for example in a range of 10 to 20 nm for the Cu-43%Cr composite, e.g. one order of magnitude lower than in pure Cu processed by SPD. Three dimensional atom probe data show also the formation of non equilibrium supersaturated solid solutions. The mechanisms of the deformation induced intermixing are discussed together with its influence on the mechanical properties.

scholarly journals Morphology and Mechanical Properties of 3Y-TZP Nanofiber Mats

Nanomaterials ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 2097
Author(s):  
Alexander I. Tyurin ◽  
Vyacheslav V. Rodaev ◽  
Svetlana S. Razlivalova ◽  
Viktor V. Korenkov ◽  
Andrey O. Zhigachev ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Phase Composition ◽  
Calcination Temperature ◽  
Tetragonal Zirconia ◽  
Calcination Temperatures ◽  
Nanoindentation Testing ◽  
Average Grain Size ◽  
Nanofiber Mats ◽  
Morphology And Mechanical Properties

The mats of yttria-stabilized tetragonal zirconia nanofibers were prepared using electrospinning. The effect of calcination temperature in the range of 600–1200 °C on their microstructure, phase composition and mechanical properties was investigated. Phase composition of the nanofibers did not change in all ranges of the calcination temperatures, while the average grain size increased from 8 to 39 nm. Nanoindentation testing of the mats showed a decrease in the hysteresis loop energy in samples with higher calcination temperature. Hardness and the elastic modulus measured with the indentation technique were the highest for the mats calcined at 900 °C.

scholarly journals Effect of Interlayer Cooling on the Preparation of Ni-Based Coatings on Ductile Iron

Coatings ◽  
2020 ◽  
Vol 10 (6) ◽  
pp. 544
Author(s):  
Yuyu He ◽  
Yijian Liu ◽  
Jiquan Yang ◽  
Fei Xie ◽  
Wuyun Huang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Additive Manufacturing ◽  
Dilution Rate ◽  
Process Parameters ◽  
Ductile Iron ◽  
Storage Effect ◽  
Thickness Increase ◽  
Average Grain Size ◽  
Metal Additive

In metal additive manufacturing without interlayer cooling, the macro-size of the layer itself is difficult to control due to the thermal storage effect. The effect of interlayer cooling was studied by cladding Ni-based coatings on the substrate of ductile iron. The results show that under the same process parameters, compared with non-interlayer cooling deposition, the dilution rate is better, and the thickness increase of interlayer cooling deposition is more uniform, which is conducive to controlling the macro-size of the interlayer cooling deposition. Furthermore, interlayer cooling deposition has fewer impurities and more uniform microstructures. Moreover, the average grain size is refined and the dendrite growth is inhibited, which improves the mechanical properties of the coating. Therefore, the hardness of the interlayer cooling specimens is greater than that of the non-interlayer-cooled specimens.

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