Pore geometry effects on elastic properties of Opalinus Clay

Geophysics ◽  
2016 ◽  
Vol 81 (5) ◽  
pp. D543-D551 ◽  
Author(s):  
Lukas M. Keller
Keyword(s):  
Elastic Properties ◽  
Volume Fraction ◽  
Water Saturation ◽  
Pore Space ◽  
Ion Beam ◽  
Evaluation Process ◽  
Preferred Orientation ◽  
Opalinus Clay ◽  
Pore Geometry ◽  
Anisotropy Parameters

Regarding the storage of nuclear waste within clay rock formations requires fundamental understanding of elastic properties of this rock type with regard to the risk evaluation process. The influence of the pore geometry on elastic properties of Opalinus Clay is studied on the basis of realistic pore microstructure, which is reconstructed from image data acquired by focused ion beam nanotomography. These microstructures are used as input pore geometries for linear elastic finite-element modeling to determine Thomsen’s [Formula: see text], [Formula: see text], and [Formula: see text] anisotropy parameters and the effective elastic moduli related to the porous material. The presence of fully drained intergranular pores substantially increases the values of [Formula: see text] and [Formula: see text]. For the investigated sample with an expected porosity of approximately 10 vol.%, the anisotropic pore space contributes similarly to the anisotropy parameters when compared with the contribution related to the preferred orientation of minerals. On the other hand, if the pore space is undrained, the effect of pores is smaller and the anisotropy is largely controlled by the preferred orientation of minerals. It is revealed that the value of [Formula: see text] is most sensitive to changes in water saturation. In case water is drained from the pores, the vertical Young’s modulus [Formula: see text] reduces significantly more when compared with the horizontal modulus [Formula: see text]. Presuming that the drainable porosity corresponds to a volume fraction of 10 vol.%, [Formula: see text] reduces by approximately 15%–20%. The effect of drainage is even more pronounced for the Poisson’s ratios, whereas the shear moduli are not much affected by drainage.

On the application of focused ion beam nanotomography in characterizing the 3D pore space geometry of Opalinus clay

2011 ◽  
Vol 36 (17-18) ◽  
pp. 1539-1544 ◽  
Author(s):  
Lukas M. Keller ◽  
Lorenz Holzer ◽  
Roger Wepf ◽  
Philippe Gasser ◽  
Beat Münch ◽  
...  
Keyword(s):  
Focused Ion Beam ◽  
Pore Space ◽  
Ion Beam ◽  
Opalinus Clay ◽  
Space Geometry

Elastic properties of microporous cemented grainstones

Geophysics ◽  
2011 ◽  
Vol 76 (6) ◽  
pp. E211-E226 ◽  
Author(s):  
François Fournier ◽  
Philippe Leonide ◽  
Kévin Biscarrat ◽  
Arnaud Gallois ◽  
Jean Borgomano ◽  
...  
Keyword(s):  
Elastic Properties ◽  
Pore Space ◽  
Micropore Volume ◽  
Pore Geometry ◽  
Petrographic Analysis ◽  
S Wave ◽  
Lower Porosity ◽  
Diagenetic History ◽  
Space Architecture ◽  
The Impact

We investigated the effect of porosity, pore geometry, and diagenetic history on the elastic properties of dry, tightly cemented grainstones whose pore space consists dominantly of intragranular microporosity within micritic grains. The integration of laboratory petrophysical measurements (porosity, P- and S-wave velocity), petrographic analysis and scanning electron microscope (SEM) imaging of micropore space of 80 Lower Cretaceous microporous carbonate samples from Provence (south-east France) allows (1) the changes in porosity and pore geometry during the diagenetic history to be related to changes in elastic properties, and (2) the impact of micritic grain diagenesis on the elastic properties of microporous grainstones to be quantified by means of fitting parameters derived from equivalent elastic medium modeling. The Urgonian microporous cemented grainstones are elastically equivalent to a homogeneous calcitic host with spherical calcitic inclusions comprising spheroidal pores. The best fit is obtained when porous spheres are modelled using the differential effective medium (DEM) approach and the whole composite using the self-consistent (SC) method (DEM-SC model). At lower porosity values ([Formula: see text]), when the micropore volume is controlled by intercrystalline cementation processes without compaction, the equivalent pore aspect ratio (EPAR) derived from DEM-SC modelling is nearly constant and averages 0.15. At higher porosities, changes in micropore space architecture related to leaching processes result in slightly increasing EPAR. The recognition of EPAR-preserving versus EPAR-non preserving elastic property evolution is proposed as a tool for diagenetic pattern detection in microporous carbonate reservoirs.

The stabilization of B.C.C. Cu in Cu/Nb nanolayered composites

1996 ◽  
Vol 54 ◽  
pp. 228-229
Author(s):  
H. Kung ◽  
A.J. Griffin ◽  
Y.C. Lu ◽  
K.E. Sickafus ◽  
T.E. Mitchell ◽  
...  
Keyword(s):  
Electrical Resistivity ◽  
Layer Thickness ◽  
Volume Fraction ◽  
Ion Beam ◽  
High Strength ◽  
Cross Sectional ◽  
Metastable Structure ◽  
High Resolution Tem ◽  
Potential Improvement ◽  
Two Phases

Materials with compositionally modulated structures have gained much attention recently due to potential improvement in electrical, magnetic and mechanical properties. Specifically, Cu-Nb laminate systems have been extensively studied mainly due to the combination of high strength, and superior thermal and electrical conductivity that can be obtained and optimized for the different applications. The effect of layer thickness on the hardness, residual stress and electrical resistivity has been investigated. In general, increases in hardness and electrical resistivity have been observed with decreasing layer thickness. In addition, reduction in structural scale has caused the formation of a metastable structure which exhibits uniquely different properties. In this study, we report the formation of b.c.c. Cu in highly textured Cu/Nb nanolayers. A series of Cu/Nb nanolayered films, with alternating Cu and Nb layers, were prepared by dc magnetron sputtering onto Si {100} wafers. The nominal total thickness of each layered film was 1 μm. The layer thickness was varied between 1 nm and 500 nm with the volume fraction of the two phases kept constant at 50%. The deposition rates and film densities were determined through a combination of profilometry and ion beam analysis techniques. Cross-sectional transmission electron microscopy (XTEM) was used to examine the structure, phase and grain size distribution of the as-sputtered films. A JEOL 3000F high resolution TEM was used to characterize the microstructure.

scholarly journals Estimation of permeability and saturation based on imaginary component of complex resistivity spectra: A laboratory study

2020 ◽  
Vol 12 (1) ◽  
pp. 299-306
Author(s):  
Jiang Jia ◽  
Shizhen Ke ◽  
Junjian Li ◽  
Zhengming Kang ◽  
Xuerui Ma ◽  
...  
Keyword(s):  
Water Saturation ◽  
Pore Space ◽  
Evaluation Model ◽  
Low Frequency ◽  
Petroleum Exploration ◽  
Western China ◽  
Imaginary Component ◽  
Estimation Model ◽  
Complex Resistivity ◽  
Linear Relationships

AbstractLow-frequency resistivity logging plays an important role in the field of petroleum exploration, but the complex resistivity spectrum of rock also contains a large amount of information about reservoir parameters. The complex resistivity spectra of 15 natural sandstone cores from western China, with different water saturations, were measured with an impedance analyzer. The pore space of each core was saturated with NaCl solution, and measurements were collected at a frequency range of 40–15 MHz. The results showed a linear relationship between the real resistivity at 1 kHz and the maximum values of imaginary resistivity for each core with different water saturations. The slopes of the linear best-fit lines had good linear relationships with the porosity and the permeability of cores. Based on this, a permeability estimation model was proposed and tested. In addition, the maxima of imaginary resistivity had power exponential relationships with the porosity and the water saturation of the cores. A saturation evaluation model based on the maxima of imaginary resistivity was established by imitating Archie’s formula. The new models were found to be feasible for determining the permeability and saturation of sandstone based on complex resistivity spectrum measurements. These models advance the application of complex resistivity spectrum in petrophysics.

scholarly journals Comparative study of elastic properties and mode I fracture energy of carbon nanotube/epoxy and carbon fibre/epoxy laminated composites

2020 ◽  
Vol 8 (1) ◽  
Author(s):  
Jyotikalpa Bora ◽  
Sushen Kirtania
Keyword(s):  
Carbon Nanotube ◽  
Carbon Fibre ◽  
Fracture Energy ◽  
Elastic Properties ◽  
Volume Fraction ◽  
Laminated Composites ◽  
Laminated Composite ◽  
Fe Analysis ◽  
Mode I ◽  
Mode I Fracture

Abstract A comparative study of elastic properties and mode I fracture energy has been presented between conventional carbon fibre (CF)/epoxy and advanced carbon nanotube (CNT)/epoxy laminated composite materials. The volume fraction of CNT fibres has been considered as 15%, 30%, and 60% whereas; the volume fraction of CF has been kept constant at 60%. Three stacking sequences of the laminates viz.[0/0/0/0], [0/90/0/90] and [0/30/–30/90] have been considered in the present analysis. Periodic microstructure model has been used to calculate the elastic properties of the laminated composites. It has been observed analytically that the addition of only 15% CNT in epoxy will give almost the same value of longitudinal Young’s modulus as compared to the addition of 60% CF in epoxy. Finite element (FE) analysis of double cantilever beam specimens made from laminated composite has also been performed. It has been observed from FE analysis that the addition of 15% CNT in epoxy will also give almost the same value of mode I fracture energy as compared to the addition of 60% CF in epoxy. The value of mode I fracture energy for [0/0/0/0] laminated composite is two times higher than the other two types of laminated composites.

scholarly journals Effect of the matrix subsystem on hydrostatic parameters of a novel 1–3-type piezo-composite

2015 ◽  
Vol 08 (05) ◽  
pp. 1550049 ◽  
Author(s):  
Vitaly Yu. Topolov ◽  
Christopher R. Bowen ◽  
Paolo Bisegna ◽  
Anatoly E. Panich
Keyword(s):  
Elastic Properties ◽  
Electromechanical Coupling ◽  
Volume Fraction ◽  
Electromechanical Coupling Factor ◽  
Ferroelectric Ceramic ◽  
Coupling Factor ◽  
Polyurethane Composite ◽  
The Matrix ◽  
Type Composite

The influence of the aspect ratio and volume fraction of ferroelectric ceramic inclusions in a 0–3 matrix on the hydrostatic parameters of a three-component 1–3-type composite is studied to demonstrate the important role of the elastic properties of the two-component matrix on the composite performance. Differences in the elastic properties of the 0–3 matrix and single-crystal rods lead to a considerable dependence of the hydrostatic response of the composite on the anisotropy of the matrix elastic properties. The performance of a 1–0–3 0.92 Pb ( Zn 1/3 Nb 2/3) O 3–0.08 PbTiO 3 SC/modified PbTiO 3 ceramic/polyurethane composite suggests that this composite system is of interest for hydroacoustic applications due to its high hydrostatic piezoelectric coefficients [Formula: see text] and [Formula: see text], squared figure of merit [Formula: see text], and electromechanical coupling factor [Formula: see text].

Micromechanical analysis of effective mechanical properties of graphene/ZrO2-hybrid poly (methyl methacrylate) nanocomposites

2021 ◽  
pp. 251659842110388
Author(s):  
Ankit Rathi ◽  
S. I. Kundalwal
Keyword(s):  
Methyl Methacrylate ◽  
Elastic Properties ◽  
Mechanical Performance ◽  
Volume Fraction ◽  
Element Model ◽  
Two Phase ◽  
Effective Elastic Properties ◽  
Poly Methyl Methacrylate ◽  
Three Phase ◽  
Effective Mechanical Properties

In this study, the tensile properties of two-phase and three-phase graphene/ZrO2-hybrid poly (methyl methacrylate) (PMMA) nanocomposites are investigated by developing finite element model using ANSYS. Primarily, the effective elastic properties of two- and three-phase graphene/ZrO2-hybrid PMMA nanocomposites (GRPCs) are estimated by developing mechanics of material (MOM) model. Results indicated that the effective elastic properties of GRPCs increase with an increase in the volume fraction of graphene. Also, the stiffness of GRPCs is increased by 78.12% with increasing in the volume fraction of graphene from 0.1 to 0.5 Vf. The incorporation of an additional ZrO2 interphase significantly improved the mechanical performance of resulting GRPCs.

The Effect of Diagenetic Evolution on Shale Gas Exploration and Development of the Longmaxi Formation Shale, Sichuan Basin, China

2021 ◽  
Vol 9 ◽  
Author(s):  
Jia Wang ◽  
Xianfeng Tan ◽  
Jingchun Tian ◽  
Long Luo ◽  
Xuanbo Gao ◽  
...  
Keyword(s):  
Shale Gas ◽  
Sichuan Basin ◽  
Pore Space ◽  
Ion Beam ◽  
Central Basin ◽  
Burial History ◽  
Longmaxi Formation ◽  
Diagenetic Evolution ◽  
Basin Margin ◽  
Exploration And Development

Diagenetic evolution is an important controlling factor of shale gas reservoirs. In this study, based on field outcrop and drilling core data, analytical techniques including X-ray diffraction (XRD), field emission scanning electron microscope combined with a focused ion beam (FIB-FESEM), and energy-dispersive spectroscopy (EDS) analyses were performed to determine the diagenetic evolution of the Longmaxi Formation shale and reveal the effect of diagenetic evolution on the shale gas exploration and development in the Sichuan Basin, Southwest China. The eodiagenesis phase was subdivided into two evolution stages, and the mesodiagenesis phase was subdivided into three evolution stages in the basin margin and center. Absorbed capacity and artificial fracturing effect of the Longmaxi Formation shale gas were related to mineral composition, which was influenced by sedimentary characteristics and diagenetic evolution. The diagenetic system in the basin margin was more open than that in the basin center due to a different burial history. The more open diagenetic system, with more micro-fractures and soluble constitute (e.g., feldspar), was in favor for the formation and preservation of secondary dissolved pores and organic pores in the basin margin. The relatively closed diagenetic system with stronger compaction resulted in deformation of pore space in the central basin.

Low Resistivity Pay Carbonates: A Practical Approach to Quantify Water Saturation Using a Modified Archie's Model

2021 ◽  
Author(s):  
Ramsin Eyvazzadeh ◽  
Abdullatif Al-Omair ◽  
Majed Kanfar ◽  
Achong Christon
Keyword(s):  
Machine Learning ◽  
Water Saturation ◽  
Pore Space ◽  
Learning Algorithms ◽  
Machine Learning Algorithms ◽  
Theoretical Research ◽  
Low Contrast ◽  
Practical Applications ◽  
Low Resistivity ◽  
New Models

Abstract A detailed description of a modified Archie's equation is proposed to accurately quantify water saturation within low resistivity/low contrast pay carbonates. The majority of previous work on low resistivity/low contrast reservoirs focused on clastics, namely, thin beds and/or clay effects on resistivity measurements. Recent publications have highlighted a "non-Archie" behavior in carbonates with complex pore structures. Several theoretical models were introduced, but new practical applications were not derived to solve this issue. Built upon previous theoretical research in a holistic approach, new models and workflows have been developed. Specifically, utilizing a combination of machine learning algorithms, nuclear magnetic resonance (NMR), core and geological data, field specific calibrated equations to compute water saturation (Sw) in complex carbonate formations are presented. Essentially, these new models partition the porosity into pore spaces and calculate their relative contribution to water saturation in each pore space. These calibrated equations robustly produce results that have proven invaluable in pay identification, well placement, and have greatly enhanced the ability to manage these types of reservoirs. This paper initially explains the theory behind the development of the analysis illustrating workflows and validation techniques used to qualify this methodology. A key benefit performing this research is the utilization of machine-learning algorithms to predict NMR derived values in wells that do not have NMR data. Several examples explore where results of this analysis are compared to dynamic testing, formation testing and laboratory measured samples to validate and demonstrate the utility of this new analysis.

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