Tensile Properties of Hydroxyapatite Whisker Reinforced Polyetheretherketone

2005 ◽  
Vol 898 ◽  
Author(s):  
Gabriel Converse ◽  
Ryan Roeder
Keyword(s):  
Tensile Strength ◽  
Elastic Modulus ◽  
Ultimate Tensile Strength ◽  
Cortical Bone ◽  
Composite Powder ◽  
Open Channel ◽  
Powder Processing ◽  
Longitudinal Direction ◽  
Stiffness Coefficients ◽  
Human Cortical Bone

AbstractPolyetheretherketone (PEEK) was reinforced with 0-40 vol% hydroxyapatite (HA) whiskers using a novel powder processing and compression molding technique. A powder mixture was uniaxially pressed into a composite powder compact and compression molded into a flat composite bar using an open-channel die, such that the HA whiskers exhibited a preferred orientation along the length of the bar and tensile specimens. As expected, increased HA whisker reinforcement resulted in increased elastic modulus, but decreased ultimate tensile strength and strain- or work-to-failure. PEEK reinforced with 40 vol% HA whiskers exhibited an elastic modulus of 16-18 GPa. PEEK reinforced with 20 vol% HA whiskers had an ultimate tensile strength of 70-80 MPa. Human cortical bone exhibits an elastic modulus of 17-26 GPa and an ultimate tensile strength of 80-150 MPa in the longitudinal direction (direction of principal stress). Stiffness coefficients measured by ultrasonic wave propagation indicated a level orthotropy also similar to that of human cortical bone tissue.

Impact of Process Parameters on the Tensile Properties of DLP Additively Manufactured ELAST-BLK 10 UV-Curable Elastomer

2021 ◽  
Author(s):  
Asma Ul Hosna Meem ◽  
Kyle Rudolph ◽  
Allyson Cox ◽  
Austin Andwan ◽  
Timothy Osborn ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Elastic Modulus ◽  
Ultimate Tensile Strength ◽  
Tensile Properties ◽  
Process Parameters ◽  
Uv Light ◽  
Uv Curable ◽  
Build Orientation ◽  
Static Tensile ◽  
The Impact

Abstract Digital light processing (DLP) is an emerging vatphotopolymerization-based 3D-printing technology where full layers of photosensitive resin are irradiated and cured with projected ultraviolet (UV) light to create a three-dimensional part layer-by-layer. Recent breakthroughs in polymer chemistry have led to a growing number of UV-curable elastomeric photoresins developed exclusively for vat photopolymerization additive manufacturing (AM). Coupled with the practical manufacturing advantages of DLP AM (e.g., industry-leading print speeds and sub-micron-level print resolution), these novel elastomeric photoresins are compelling candidates for emerging applications requiring extreme flexibility, stretchability, conformability, and mechanically-tunable stiffness (e.g., soft robotic actuators and stretchable electronics). To advance the role of DLP AM in these novel and promising technological spaces, a fundamental understanding of the impact of DLP manufacturing process parameters on mechanical properties is requisite. This paper highlights our recent efforts to explore the process-property relationship for ELAST-BLK 10, a new commercially-available UV-curable elastomer for DLP AM. A full factorial design of experiments is used to investigate the effect of build orientation and layer thickness on the quasi-static tensile properties (i.e., small-strain elastic modulus, ultimate tensile strength, and elongation at fracture) of ELAST-BLK 10. Statistical results, based on a general linear model via ANOVA methods, indicate that specimens with a flat build orientation exhibit the highest elastic modulus, ultimate tensile strength, and elongation at fracture, likely due to a larger surface area that enhances crosslink density during the curing process. Several popular hyperelastic constitutive models (e.g., Mooney-Rivlin, Yeoh, and Gent) are calibrated to our quasi-static tensile data to facilitate component-level predictive analyses (e.g., finite-element modeling) of soft robotic actuators and other emerging soft-matter applications.

RELATIONS OF ANISOTROPIC ELASTIC MODULI TO DENSITY AND CT NUMBER IN BOVINE CORTICAL BONE

2008 ◽  
Vol 20 (03) ◽  
pp. 139-143 ◽  
Author(s):  
Jui-Ting Hsu ◽  
Ming-Tzu Tsai ◽  
Heng-Li Huang
Keyword(s):  
Elastic Modulus ◽  
Bone Density ◽  
Cortical Bone ◽  
Elastic Moduli ◽  
Transversely Isotropic ◽  
Longitudinal Direction ◽  
Coefficient Of Determination ◽  
Ct Number ◽  
Noninvasive Technique ◽  
Anisotropic Elastic

It would be useful to be able to determine the mechanical properties of bone using a noninvasive technique such as computed tomography (CT). However, in contrast to cancellous bone tissue, quantifying the elastic modulus of cortical bone from bone density and CT number has not been investigated extensively. This study measured the elastic moduli of cortical bone from eight bovine femora in the longitudinal, circumferential, and radial directions using mechanical compressive testing. Before testing, the CT number and wet apparent bone density were obtained. The experimentally determined coefficient of determination between CT number and bone density was around 0.6. Bone density was a good predictor of the elastic modulus of cortical bone in the longitudinal direction (r2 > 0.79), but it could not be used to predict the elastic moduli in the circumferential (r2 < 0.4) and radial (r2 < 0.22) directions. The coefficient of determination between CT number and the elastic modulus in the longitudinal direction was higher than 0.41. However, the correlations between CT number and elastic moduli were weak in the circumferential (r2 < 0.21) and radial (r2 < 0.19) directions. Moreover, the elastic modulus was much higher in the longitudinal direction than the circumferential and radial directions, and hence cortical bone can be considered a transversely isotropic property.

scholarly journals Finite Element Analysis of Porous Ti-6Al-4V Alloy Structures for Biomedical Applications

2021 ◽  
Vol 2070 (1) ◽  
pp. 012224
Author(s):  
N Ganesh ◽  
S Rambabu
Keyword(s):  
Finite Element ◽  
Elastic Modulus ◽  
Cortical Bone ◽  
Bone Ingrowth ◽  
Stress Shielding ◽  
Shielding Effect ◽  
Element Analysis ◽  
Human Cortical Bone ◽  
Porous Ti ◽  
Manufacturing Technologies

Abstract In this article, design and finite element simulation of porous Ti-6Al-4V alloy structures was presented. Typically, titanium and titanium alloy implants can be manufactured with required pore size and porosity volume by using powder bed fusion techniques due to advancement in additive manufacturing technologies. However, the mismatch of elastic modulus between human cortical bone and the dense Ti-6Al-4V alloy implant resulted in stress shielding which accelerate the implant failure. The porous implant structures help in reduce the mismatch of elastic modulus between the cortical bone and implant structure and also improve the bone ingrowth. Hence, the present work focuses on design of Ti-6Al-4V alloy porous structures with various porosities ranging from 10% to 70% and simulated to determine the elastic modulus suitable for human cortical bone. The sample with 45% porosity is found to be best suited for replacement of cortical bone with elastic modulus of 74Gpa, preventing stress shielding effect and enhanced chances of bone ingrowth.

scholarly journals Kearns texture parameters, mechanical properties and damageability of titanium sheet after alternating bending

2021 ◽  
Vol 22 (3) ◽  
pp. 543-550
Author(s):  
V.V. Usov ◽  
N.M. Shkatulyak ◽  
O.S. Savchuk ◽  
N.I. Rybak
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Elastic Modulus ◽  
Ultimate Tensile Strength ◽  
Yield Stress ◽  
Rolling Direction ◽  
Initial State ◽  
Texture Parameters ◽  
Experimental Values ◽  
Alternating Bending

This work aims to determine the Kearns texture parameters and evaluate on their basis the elastic moduli, mechanical properties (ultimate tensile strength, conditional yield stress), as well as damageability parameters of the sheets commercial titanium (CT-grade 1: 0.04% Fe; 0.015% C; 0.05% N 0.05% c; 0.009% H)  as delivered after rolling and annealing at 840°C (original sheet) and further alternating bending (AB) in the amount of 0.5; 1, 3 and 5 cycles. Damageability parameters characterizing damage accumulation were determined from the elastic modulus change after the above-mentioned number of AB cycles relative to the values ​​of the elastic modulus in different directions of the original sheet of the studied titanium. The elastic constants of the single crystal and the Kearns texture parameters were used to estimate the elastic modulus in the rolling direction (RD) and transverse direction (TD) of the original sheet, and sheets after an above number of AB cycles. The deviation of the calculated and experimental values ​​of the elastic modulus did not exceed 5%. The deviation of the calculated and experimental values of the ultimate tensile strength and yield stress in the RD and TD both in the initial state and after the corresponding number cycles of the AB did not exceed 10%.

Experimental Investigation of Stratasys J750 PolyJet Printer: Effects of Orientation and Layer Thickness on Mechanical Properties

2019 ◽  
Author(s):  
Xingjian Wei ◽  
Abhinav Bhardwaj ◽  
Chin-Cheng Shih ◽  
Li Zeng ◽  
Bruce Tai ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Elastic Modulus ◽  
Ultimate Tensile Strength ◽  
Layer Thickness ◽  
Axial Direction ◽  
Limited Information ◽  
Direction Parallel ◽  
Control Factors ◽  
Significant Difference

Abstract The J750 PolyJet printer is the newest model of full-color, multi-material 3D printer from Stratasys. Currently, limited information is available about the effects of control factors on mechanical properties such as elastic modulus, ultimate tensile strength, and elongation. In this study, the effects of two control factors, orientation and layer thickness, on mechanical properties of samples printed by the Stratasys J750 printer are investigated. The results show that orientation significantly affects mechanical properties. Specifically, samples printed with its axial direction parallel to the direction of printing have the highest elastic modulus, and elongation, whereas samples printed with its axial direction perpendicular to the direction of printing have the highest ultimate tensile strength. Also, layer thickness makes a significant difference for mechanical properties, and larger layer thickness leads to higher ultimate tensile strength and elongation. These results would be valuable to researchers and practitioners who use J750.

scholarly journals Mechanical Properties of Laser-Sintered 3D-Printed Cobalt Chromium and Soft-Milled Cobalt Chromium

Prosthesis ◽  
2020 ◽  
Vol 2 (4) ◽  
pp. 313-320
Author(s):  
Abdullah Barazanchi ◽  
Kai Chun Li ◽  
Basil Al-Amleh ◽  
Karl Lyons ◽  
J. Neil Waddell
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Elastic Modulus ◽  
Ultimate Tensile Strength ◽  
High Stress ◽  
Uniform Structure ◽  
Cobalt Chromium ◽  
Proof Stress ◽  
Fracture Surfaces ◽  
3D Printed

Purpose: To compare the mechanical properties and fracture behaviour of laser-sintered/3D-printed cobalt chromium (LS CoCr) with soft-milled cobalt chromium (SM CoCr) to assess their suitability for use in high-stress areas in the oral cavity. Material and Method: Two computer-aided manufacturing methods were used to fabricate dumbbell specimens in accordance with the ASTM standard E8. Specimens were fractured using tensile testing and elastic modulus, and proof stress and ultimate tensile strength were calculated. Fracture surfaces were examined using scanning electron microscopy. Plate specimens were also fabricated for the examination of hardness and elastic modulus using nanoindentation. Unpaired t-test was used to evaluate statistical significance. Results: LS CoCr specimens were found to have significantly higher ultimate tensile strength (UTS) and proof stress (PS) (p < 0.05) but not a significantly higher elastic modulus (p > 0.05). Examination of the dumbbell fracture surfaces showed uniform structure for the LS CoCr specimens whilst the SM CoCr specimens were perforated with porosities; neither showed an obvious point of fracture. Nanoindentation also showed that LS CoCr specimens possessed higher hardness compared with SM CoCr specimens. Conclusion: LS CoCr and SM CoCr specimens were both found to exhibit uniformly dense structure; although porosities were noted in the SM CoCr specimens. LS CoCr specimens were found to have superior tensile properties, likely due to lack of porosities, however both had mean values higher than those reported in the literature for cast CoCr. Uniformity of structure and high tensile strength indicates that LS CoCr and SM CoCr fabricated alloys are suitable for long-span metallic frameworks for use in the field of prosthodontics.

scholarly journals Biomechanical characterization of human temporal muscle fascia in uniaxial tensile tests for graft purposes in duraplasty

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Johann Zwirner ◽  
Benjamin Ondruschka ◽  
Mario Scholze ◽  
Gundula Schulze-Tanzil ◽  
Niels Hammer
Keyword(s):  
Tensile Strength ◽  
Elastic Modulus ◽  
Ultimate Tensile Strength ◽  
Dura Mater ◽  
Uniaxial Tensile ◽  
Graft Material ◽  
Post Mortem ◽  
Temporal Muscle ◽  
Post Mortem Interval ◽  
Muscle Fascia

AbstractThe human temporal muscle fascia (TMF) is used frequently as a graft material for duraplasty. Encompassing biomechanical analyses of TMF are lacking, impeding a well-grounded biomechanical comparison of the TMF to other graft materials used for duraplasty, including the dura mater itself. In this study, we investigated the biomechanical properties of 74 human TMF samples in comparison to an age-matched group of dura mater samples. The TMF showed an elastic modulus of 36 ± 19 MPa, an ultimate tensile strength of 3.6 ± 1.7 MPa, a maximum force of 16 ± 8 N, a maximum strain of 13 ± 4% and a strain at failure of 17 ± 6%. Post-mortem interval correlated weakly with elastic modulus (r = 0.255, p = 0.048) and the strain at failure (r =  − 0.306, p = 0.022) for TMF. The age of the donors did not reveal significant correlations to the TMF mechanical parameters. Compared to the dura mater, the here investigated TMF showed a significantly lower elastic modulus and ultimate tensile strength, but a larger strain at failure. The human TMF with a post-mortem interval of up to 146 h may be considered a mechanically suitable graft material for duraplasty when stored at a temperature of 4 °C.

scholarly journals Tensile properties of PLA/PBAT blends and PLA fibre-reinforced PBAT composite

2018 ◽  
Vol 192 ◽  
pp. 03014 ◽  
Author(s):  
Eakasit Sritham ◽  
Phakaimat Phunsombat ◽  
Jedsada Chaishome
Keyword(s):  
Tensile Strength ◽  
Elastic Modulus ◽  
Ultimate Tensile Strength ◽  
Tensile Properties ◽  
Room Temperature ◽  
Dsc Measurements ◽  
Significant Difference ◽  
Two Phases

The tensile properties of PLA/PBAT blends, PLA fibre reinforced PBAT composite (PLAF) at room temperature and -18°C were investigated. The concentrations of PLA in the blends were 10%, 20%, 30% and 40% (by volume). There was an improvement of elastic modulus (E) for PLA/PBAT blends when PLA was 40%. There was no significant difference of ultimate tensile strength (UTS) among the blends. For the same concentration of PLA (40%) in PLA-PBAT mixture, PLAF exhibited higher values of E and UTS than that of PLA/PBAT blends. Elongation of PLA/PBAT blends rapidly decreased upon the addition of PLA to the blends. The values of E and UTS for PLA/PBAT blends and composite, neat PLA, and PP increased with the decreasing of temperature from room temperature to -18°C. The effect of decreasing temperature was not observed on elongation. It was appeared from the results obtained for FTIR and DSC measurements that PLA and PBAT were immiscible, separating into two phases.

The Study of Properties of Cu-0.8Cr-0.2Zr Alloy Used as Contact Materials

2012 ◽  
Vol 602-604 ◽  
pp. 616-622
Author(s):  
Liu Cheng Hao ◽  
Li Juan Han ◽  
Ya Fei Li ◽  
Bao Zeng Li ◽  
Lu Ping Wang ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Tensile Strength ◽  
Elastic Modulus ◽  
Ultimate Tensile Strength ◽  
High Voltage ◽  
Brinell Hardness ◽  
Softening Temperature ◽  
Alloy Matrix ◽  
Contact Materials ◽  
The Matrix

Although alloy QCr0.5 has been used as the contact materials in the high-voltage equipment extensively, but it always confronts the awkwardness of over aging in the heat treatment, and results in brittleness during the switching on and breaking process. In the present work by the technology of interalloy-adding, the Zr-containing alloy Cu-0.8Cr-0.2Zr has been prepared and investigated. The results of the microstructure and properties indicate that the alloy matrix maintains FCC microstructure and lots of Zr-containing precipitation is dispersed in the matrix uniformly. The brinell hardness, the ultimate tensile strength and the elastic modulus increase greatly, reach 140 MPa, 430 Mpa and 130 GPa respectively, meanwhile the electric conductivity maintains 75%IACS and the softening temperature is up to 550 °C.

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