Modulated Hall-Effect Techniques for the Study of Transport Properties of Microcrystalline Silicon with Different Grain Sizes

1996 ◽  
Vol 420 ◽  
Author(s):  
P. Hapke ◽  
U. Backhausen ◽  
R. Carius ◽  
F. Finger ◽  
S. Ray

AbstractHighly doped μc-Si:H samples with a wide range of crystalline volume fractions and grain sizes have been investigated by Hall-effect experiments. We present an experimental set-up with a current modulation technique and a 6-pole contact geometry which allows the measurement of the Hall-effect on highly doped μc-Si:H down to 10K. The experimental results exhibit a clear correlation between the mobility μ and the grain size δ. Further, the results show that the transport in μc-Si:H can not be described by thermal emission over grain boundaries alone, additional transport paths, e.g. tunneling processes through the barriers have to be taken into account.

2007 ◽  
Vol 558-559 ◽  
pp. 1283-1294 ◽  
Author(s):  
Cheng Xu ◽  
Z. Horita ◽  
Terence G. Langdon

It is now well-established that processing through the application of severe plastic deformation (SPD) leads to a significant reduction in the grain size of a wide range of metallic materials. This paper examines the fabrication of ultrafine-grained materials using high-pressure torsion (HPT) where this process is attractive because it leads to exceptional grain refinement with grain sizes that often lie in the nanometer or submicrometer ranges. Two aspects of HPT are examined. First, processing by HPT is usually confined to samples in the form of very thin disks but recent experiments demonstrate the potential for extending HPT also to bulk samples. Second, since the strains imposed in HPT vary with the distance from the center of the disk, it is important to examine the development of inhomogeneities in disk samples processed by HPT.


Soil Research ◽  
1998 ◽  
Vol 36 (1) ◽  
pp. 167 ◽  
Author(s):  
R. H. Crockford ◽  
P. M. Fleming

A comprehensive sediment sampling program was undertaken in the upper Molonglo catchment in south-eastern New South Wales to determine if mineral magnetics could be used to estimate sidestream contribution at river confluences in this environment. Some 12 confluences were examined over 1400 km 2 in 2 major basins and over 2 contrasting geological types. Sediment samples were divided into 7 size classes and the following magnetic properties measured: magnetic susceptibility at 2 frequencies, isothermal remanent magnetisation at 3 flux densities, and anhysteristic remanent magnetisation. The sidestream inputs were calculated for each particle size class from the range of magnetic parameters. Significant discrepancies and differences appeared in the resultant sidestream inputs, and this paper outlines the conclusions as to the reliability of the different analytical procedures. It is shown that both the concentration and magnetic grain size of ferrimagnetic minerals in the sediments must be taken into account. Where the difference in magnetic grain size between the upstream and sidestream sediments is small, the use of parameter crossplots or bulked magnetic ratios is generally not appropriate. The use of mass (concentration) magnetic values may be better. The difference in the demands of the crossplots and mass values methods is that crossplots require a wide range of mass magnetic concentrations in each branch, with the upstream and sidestream sediments having different magnetic grain sizes, whereas the mass values procedure does best with a very limited (but different) range of concentrations at the upstream and sidestream branches, but similar magnetic grain sizes. This paper provides an extensive discussion of the estimation technique using different parameter combinations, and uses 3 contrasting confluences as case studies.


1996 ◽  
Vol 452 ◽  
Author(s):  
U. Backhausen ◽  
R. Carius ◽  
F. Finger ◽  
P. Hapke ◽  
U. Zastrow ◽  
...  

AbstractHall-effect experiments on <n>-type microcrystalline silicon samples with a wide range of structural composition and doping have been performed. For highly doped samples the conductivity Σ and the mobility μ show a non-singly activated behaviour while the carrier density is almost temperature independent. The comparison of the carrier density with the phosphorous concentration in conjunction with the conductivity gives strong evidence that the Hall-effect data have to be corrected with the crystalline volume fraction Xc. Furthermore, the increase of the mobility with Xc, which is linked in our case to the grain size, can be explained when the length of the transport paths is taken into account. Our results will be discussed in the framework of different transport models. It is concluded that transport in μc-Si:H can not be explained in terms of thermionic emission over barriers with a well defined barrier height; instead a distribution of barrier heights have to be considered. A transport model is suggested where μc-Si:H is viewed as an interconnected network.


2021 ◽  
Vol 1042 ◽  
pp. 9-16
Author(s):  
Zhi Hao Zhao ◽  
Jian Ping Lin ◽  
Jun Ying Min ◽  
Yong Hou ◽  
Bo Sun

Thermally-induced phase transformation (PT) is of significance and value to the application of NiTi alloy components. Low-temperature aging (LTA) treatment was used to alter PT characteristics of NiTi alloys avoiding undesirable grain growth. Effect of LTA on PT of NiTi wires with a wide range of grain sizes from 34 nm to 8021 nm was investigated in this study. As the average grain size varies from 34 to 217 nm, the temperature of the B2↔R transformation increase as a result of LTA, and the increasing effect is more obvious at a larger grain size. For NiTi alloys with average grain sizes ranging from 523 to 1106 nm, transformation sequence changes from B2↔B19' to B2↔R due to LTA. For the sample with an average grain size of 2190 nm, the B2↔B19' transformation is replaced by B2↔R←B19' after LTA. When the average grain size is larger than 2190 nm, transformation sequence changes from B2↔B19' to B2↔R↔B19' after LTA. Transmission emission microscope observations reveal that the above-mentioned PT behavior correlates with the coupled effect of grain size and precipitation. The precipitation of Ni4Ti3 in the grains with a size smaller than ~150 nm is inhibited after LTA, the temperature of B2→R of samples with average GS smaller than ~150 nm still is elevated due to the inhomogeneous grain size of NiTi wires.


1993 ◽  
Vol 30 (5) ◽  
pp. 727-738 ◽  
Author(s):  
P.G. Nicholson ◽  
R.B. Seed ◽  
H.A. Anwar

Several alternative approaches have been suggested for evaluation and correction of the testing errors caused by membrane compliance. The degree to which membrane compliance may affect the results of an undrained test is a function of the soil grain size and overall geometry of the test specimen, as well as specimen density and range of effective confining stresses during a given test. Membrane-compliance effects may be negligible for fine sands and silts tested in conventional 71 mm diameter samples, since even very thin membranes cannot penetrate significantly into the small surficial voids. For medium to coarse sands and gravels, however, membrane-compliance effects may have a significant influence on test results. The scope of this paper is threefold: firstly, to review, examine, and evaluate the variety of methods to measure and characterize membrane compliance; secondly, to develop an improved understanding of the factors affecting membrane compliance; and thirdly, to provide an enhanced, updated, and expanded correlation for estimating membrane compliance characteristics as a function of material grain size for a range of soil types, including a wide range of gradation types and representative grain sizes from silts through gravels. Key words : membrane, penetration, compliance, undrained testing, triaxial, measurement, evaluation.


2012 ◽  
Vol 17 (2) ◽  
pp. 121
Author(s):  
Sutopo Ghani Nugroho ◽  
. Dermiyati ◽  
Jamalam Lumbanraja ◽  
Sugeng Triyono ◽  
Hanung Ismono ◽  
...  

The objective of multi years study was to formulate an alternative organic based fertilizer by mixing a fresh manureand phosphate rock with several different grain sizes conducted in the Field Experimental Station of the Universityof Lampung. Both materials of the fresh manure and phosphate rock were obtained from local sources. Five levelsof mixture of fresh manure and phosphate rock, three levels of grain size of phosphate rock, and two kinds ofcomposting technique were factorial set up. The mixture materials were aerobically composted for 12 weeks. Theresults of the first year study show that (a) the optimum ratio of the mixture of fresh manure and phosphate rock was80% to 20% with the optimum of grain size of phosphate rock < 3 mm; (b) 6-8 weeks of incubation of the mixturematerials has been optimally composted under aerobic conditions of the complete mixture of batch compostedtechnique; (c) the quality of the final produced compost was considered to fulfill the requirement of standard criteriaof organic fertilizer; while (d) the quantity of compost recovered up to 75.07% which was a reliable quantity of massproduction of organic fertilizer.[How to Cite: Nugroho SG, Dermiyati, J Lumbanraja, S Triyono, H Ismono, YT Sari and E Ayuandari. 2012. Optimum Ratio of Fresh Manure and Grain Size of Phosphate Rock Mixture in a Formulated Compost for Organomineral NP Fertilizer. J Trop Soils 17 (2) : 121-128. Doi: 10.5400/jts.2012.17.2.121][Permalink/DOI: www.dx.doi.org/10.5400/jts.2012.17.2.121]


MRS Advances ◽  
2018 ◽  
Vol 3 (31) ◽  
pp. 1749-1754 ◽  
Author(s):  
Said El Chamaa ◽  
Mitesh Patel ◽  
Catrin M. Davies ◽  
Mark R. Wenman

ABSTRACTUnderstanding the precipitation of brittle hydride phases is crucial in establishing a failure criterion for various zirconium alloy nuclear fuel cladding. Accordingly, it is important to quantify the sensitivity of hydride precipitation to the component microstructure. This experimental investigation focuses on two microstructural characteristics and their role as hydride nucleation sites: The grain size and the alloy chemical composition. Samples of commercially pure zirconium (Zr-702) and Zircaloy-4, each with a wide range of grain sizes, were hydrided to 100 ppm and micrographs of the hydride distribution were optically analyzed for inter-granular and intra-granular precipitate sites. For most grain sizes, it was found that a significantly lower fraction of the precipitated hydrides nucleated at grain boundaries in Zircaloy-4 than in Zr-702, suggesting that a higher SPP content encourages the formation of intra-granular hydrides. Moreover, this effect became more prominent as the grain size increased; large-grain specimens contained a higher fraction of intra-granular hydrides than small-grain specimens of both Zr-702 and Zircaloy-4, highlighting the potency of grain boundaries as nucleation sites and how SPPs can influence the hydride distribution profile.


Author(s):  
Takao Suzuki ◽  
Hossein Nuri

For future high density magneto-optical recording materials, a Bi-substituted garnet film ((BiDy)3(FeGa)5O12) is an attractive candidate since it has strong magneto-optic effect at short wavelengths less than 600 nm. The signal in read back performance at 500 nm using a garnet film can be an order of magnitude higher than a current rare earth-transition metal amorphous film. However, the granularity and surface roughness of such crystalline garnet films are the key to control for minimizing media noise.We have demonstrated a new technique to fabricate a garnet film which has much smaller grain size and smoother surfaces than those annealed in a conventional oven. This method employs a high ramp-up rate annealing (Γ = 50 ~ 100 C/s) in nitrogen atmosphere. Fig.1 shows a typical microstruture of a Bi-susbtituted garnet film deposited by r.f. sputtering and then subsequently crystallized by a rapid thermal annealing technique at Γ = 50 C/s at 650 °C for 2 min. The structure is a single phase of garnet, and a grain size is about 300A.


Author(s):  
Jozefien De Bock

Historically, those societies that have the longest tradition in multicultural policies are settler societies. The question of how to deal with temporary migrants has only recently aroused their interest. In Europe, temporary migration programmes have a much longer history. In the period after WWII, a wide range of legal frameworks were set up to import temporary workers, who came to be known as guest workers. In the end, many of these ‘guests’ settled in Europe permanently. Their presence lay at the basis of European multicultural policies. However, when these policies were drafted, the former mobility of guest workers had been forgotten. This chapter will focus on this mobility of initially temporary workers, comparing the period of economic growth 1945-1974 with the years after the 1974 economic crisis. Further, it will look at the kind of policies that were developed towards guest workers in the era before multiculturalism. This way, it shows how their consideration as temporary residents had far-reaching consequences for the immigrants, their descendants and the receiving societies involved. The chapter will finish by suggesting a number of lessons from the past. If the mobility-gap between guest workers and present-day migrants is not as big as generally assumed, then the consequences of previous neglect should serve as a warning for future policy making.


2016 ◽  
Vol 3 (2) ◽  
pp. 82-93
Author(s):  
Gugulethu Shamaine Nkala ◽  
Rodreck David

Knowledge presented by Oral History (OH) is unique in that it shares the tacit perspective, thoughts, opinions and understanding of the interviewee in its primary form. While teachers, lecturers and other education specialists have at their disposal a wide range of primary, secondary and tertiary sources upon which to relate and share or impart knowledge, OH presents a rich source of information that can improve the learning and knowledge impartation experience. The uniqueness of OH is presented in the following advantages of its use: it allows one to learn about the perspectives of individuals who might not otherwise appear in the historical record; it allows one to compensate for the digital age; one can learn different kinds of information; it provides historical actors with an opportunity to tell their own stories in their own words; and it offers a rich opportunity for human interaction. This article discusses the placement of oral history in the classroom set-up by investigating its use as a source of learning material presented by the National Archives of Zimbabwe to students in the Department of Records and Archives Management at the National University of Science and Technology (NUST). Interviews and a group discussion were used to gather data from an archivist at the National Archives of Zimbabwe, lecturers and students in the Department of Records and Archives Management at NUST, respectively. These groups were approached on the usability, uniqueness and other characteristics that support this type of knowledge about OH in a tertiary learning experience. The findings indicate several qualities that reflect the richness of OH as a teaching source material in a classroom set-up. It further points to weak areas that may be addressed where the source is considered a viable strategy for knowledge sharing and learning. The researchers present a possible model that can be used to champion the use of this rich knowledge source in classroom education at this university and in similar set-ups. 


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