Primary Creep of Ni3(Al, Ta) Single Crystals at Room Temperature

1996 ◽  
Vol 460 ◽  
Author(s):  
M. D. Uchic ◽  
W. D. Nix
Keyword(s):  
Single Crystals ◽  
Applied Stress ◽  
Room Temperature ◽  
Primary Creep ◽  
Plastic Response ◽  
Stress Increment ◽  
Creep Tests ◽  
Creep Curves ◽  
Anti Phase Boundary ◽  
Test Stress

ABSTRACTThis study examines the time-dependent deformation of Ni3(Al, Ta) at room temperature. Tension creep experiments have been performed on single crystals with one {111}<101> slip system active at the start of the test, where the applied stress ranged from 66.4 MPa (the measured 0.01% flow stress) to 143 MPa (which produced approximately 9% plastic strain). All creep curves displayed primary creep leading to eventual exhaustion, where the measured creep strain declined at a rate faster than predicted for logarithmic creep. However, no correlation between the applied stress and the form of the declining creep rate can be made at this rime. Many creep curves can be obtained from one sample, as the creep curves from both virgin samples and samples with prior deformation history (at the same test stress) were indistinguishable. At the beginning of an incremental creep test, where the stress is increased by a small amount to reinitiate plastic flow in an exhausted sample, a significant retardation of the plastic response of the sample occurred when the stress increment was below 4 MPa. Preliminary TEM studies of a sample strained to 6% suggest that room temperature creep tests may not be ideal for examining the flow of Anti-Phase-Boundary (APB) dissociated dislocations.

Viscoplasticity Based on Total Strain. The Modelling of Creep With Special Considerations of Initial Strain and Aging

1979 ◽  
Vol 101 (4) ◽  
pp. 380-386 ◽  
Author(s):  
Erhard Krempl
Keyword(s):  
Strain Relaxation ◽  
Stress Test ◽  
Time Derivative ◽  
Constant Load ◽  
Primary Creep ◽  
True Stress ◽  
Initial Strain ◽  
304 Stainless Steel ◽  
Creep Tests ◽  
Creep Curves

A previously proposed theory is specialized for the uniaxial state of stress and its prediction for creep and relaxation is analyzed in detail. Constant true stress and constant load creep tests are simulated in the presence and absence of thermal aging together with the constant strain relaxation test. The signs of the creep rate and its time derivative as well as the relaxation rate and its time derivative are introduced as criteria. The constant load creep test can reproduce the normal creep curves and nonclassical creep curves (ε˙ > 0; ε¨ > 0 for all ε and for σ0 > 0). The capabilities of the constant true stress test are limited to primary creep if the work-hardening slope is positive. When aging is introduced almost any creep curve can be reproduced in both tests. The importance of initial strain is discussed and demonstrated by room temperature creep tests on Type 304 Stainless Steel. It is suggested that the initial strains together with the creep curves be reported in the future. Poisson’s ratio in creep needs to be measured and tests are proposed which will enable a quantitative assessment of aging.

Creep Behavior for Alloy 617 in Air at 950°C

2010 ◽  
Vol 654-656 ◽  
pp. 508-511 ◽  
Author(s):  
Woo Gon Kim ◽  
Song Nan Yin ◽  
Gyeong Geon Lee ◽  
Yong Wan Kim
Keyword(s):  
Creep Behavior ◽  
Primary Creep ◽  
Secondary Creep ◽  
Creep Tests ◽  
Alloy 617 ◽  
Very High Temperature Reactor ◽  
Creep Curves ◽  
High Temperature Reactor ◽  
Very High ◽  
Cr2o3 Layer

Creep behavior for Alloy 617, which is considered as one of the major structural materials of a very high temperature reactor, was investigated in air at 950oC. Creep experimental data was obtained by a series of creep tests with different stress levels at 950oC. Alloy 617 revealed little primary creep strains and unclear secondary creep stages. A tertiary creep stage was initiated from a low strain level and was dominant in full creep curves. The creep constants of A, n, m, and C in Norton’s power law and Monkman-Grant relationships were determined. In microstructure observations of crept specimens, it was found that a Cr2O3 oxidation layer was formed on the surface, and just beneath the Cr2O3 layer, an internal Al-oxide sub layer was formed with rod shapes. Also, below the internal sub layer, a thick carbide-depleted zone was developed due to reaction of the chromia and carbide precipitates. The thickness of the outer Cr-oxide layer increased with increasing creep rupture times. The increasing tendency showed a smooth slope like a parabolic curve.

Analysis of Creep Curves of Haynes 230 Superalloy

2010 ◽  
Vol 638-642 ◽  
pp. 2285-2290 ◽  
Author(s):  
Maurizio Maldini ◽  
Giuliano Angella ◽  
Valentino Lupinc
Keyword(s):  
Applied Stress ◽  
High Temperatures ◽  
Creep Curve ◽  
Creep Behaviour ◽  
Strong Dependence ◽  
Solution Treatment ◽  
Constant Load ◽  
Creep Tests ◽  
Haynes 230 ◽  
Creep Curves

The creep behaviour of the solid solution strengthened nickel-based superalloy Haynes 230 has been investigated under constant load and temperature conditions on as received, after conventional solution treatment, and on overaged conditions. The experimental results have shown a very strong dependence of the creep curve shape with the applied stress/temperature: in the tests performed at high stresses/low temperatures, the primary/decelerating stage takes an important portion of the creep curve. At these test conditions, the accelerating creep is mainly caused by the increase of the applied stress with the strain as it happens in constant load creep tests. In the tests performed at low stresses/high temperatures, the primary stage is very small and the following accelerating creep is characterized by different accelerating creep stages. The analysis of the creep curves on the as received and overaged alloys, has shown that a large portion of the accelerating creep at low stresses/high temperatures is caused by microstructural instability.

Deformation Behavior of Fe-Al Single Crystals Containing Fe2AlTi Precipitates

2018 ◽  
Vol 941 ◽  
pp. 1372-1377
Author(s):  
Hiroyuki Y. Yasuda ◽  
Hiroyuki Yakage ◽  
Yunima Shinohara ◽  
Ken Cho
Keyword(s):  
Single Crystals ◽  
Yield Stress ◽  
Deformation Behavior ◽  
Room Temperature ◽  
Precipitation Hardening ◽  
High Strength ◽  
Misfit Strain ◽  
High Yield ◽  
High Yield Stress ◽  
Anti Phase Boundary

Fe-20Al-5Ti (at.%) single crystals composed of the bcc Fe-Al matrix and the Fe2AlTi precipitates with the L21 structure was examined. In the single crystals furnace-cooled (FC) from 1373 K to room temperature, coarse Fe2AlTi phase about 300 nm in diameter were precipitated in the bcc matrix. A misfit strain and a dissolution temperature of the L21 precipitates are +0.59% and 1151 K, respectively. The single crystals exhibited high yield stress above 600 MPa up to 973 K while further increase in temperature resulted in a decrease in yield stress due to the dissolution of the precipitates. In the FC crystals, 1/2<111> dislocations in the bcc matrix bypassed the coarse L21 precipitates due to their large misfit strain, resulting in high strength. In contrast, the fine L21 precipitates about 30 nm in diameter were observed in the crystals after solutionization and annealing at 873 K. The crystals with the fine L21 precipitates demonstrated high yield stress above 1100 MPa at and below 773 K. Uncoupled or paired 1/2<111> dislocations cut the fine L21 precipitates, leaving an anti-phase boundary (APB) inside the precipitates. The APB inside the precipitates was considered to be responsible for strong precipitation hardening.

Long-Term Creep Modeling of Modified 9Cr-1Mo Steel for a Sodium Cooled Fast Reactor

2010 ◽  
Author(s):  
Woo-Gon Kim ◽  
Jae-Young Park ◽  
Sung-Ho Kim ◽  
Chan-Bock Lee
Keyword(s):  
Constant Load ◽  
Primary Creep ◽  
Least Square ◽  
Creep Data ◽  
Creep Tests ◽  
Omega Method ◽  
Creep Curves ◽  
The Individual ◽  
Term Creep

This paper focused on long-term creep modeling for describing total creep curves of up to rupture for modified 9Cr-1Mo steel (G91). Creep data was obtained by a series of constant-load creep tests at 600°C. Three modified constitutive equations of modified power-law method (MPM), modified theta method (MTM) and modified omega method (MOM), described as a sum of a decaying primary creep and an accelerating tertiary creep, were proposed. A nonlinear least square fitting (NLSF) analysis was carried out on the basis of the creep data so that they provide the best fit to experimental data in optimizing parameter constants of the individual equation. Results of the NLSF analysis showed that in the lower stress regions of 160MPa (σ/σys&lt;0.65), the MTM matched well with the experimental creep data compared with the MPM and MOM, but that in the higher stress regions of 160MPa (σ/σy &gt; 0.65), the MPM revealed better agreement than the MTM and MOM. It was found that the MTM was superior in the modeling of long-term creep curves to the MPM and MOM. Long-term creep curves for the G91 steel were numerically modeled and its creep life was predicted by the MTM.

Dislocation structures around SiO2 Particles in aged Cu-Cr-SiO2

1978 ◽  
Vol 36 (1) ◽  
pp. 594-595
Author(s):  
N.J. Long ◽  
M.H. Loretto ◽  
C.H. Lloyd
Keyword(s):  
Flow Stress ◽  
Single Crystals ◽  
Room Temperature ◽  
Thin Foil ◽  
Age Hardening ◽  
Dispersion Strengthening ◽  
Accurate Picture ◽  
The Matrix ◽  
Very High ◽  
Good Agreement

IntroductionThere have been several t.e.m. studies (1,2,3,4) of the dislocation arrangements in the matrix and around the particles in dispersion strengthened single crystals deformed in single slip. Good agreement has been obtained in general between the observed structures and the various theories for the flow stress and work hardening of this class of alloy. There has been though some difficulty in obtaining an accurate picture of these arrangements in the case when the obstacles are large (of the order of several 1000's Å). This is due to both the physical loss of dislocations from the thin foil in its preparation and to rearrangement of the structure on unloading and standing at room temperature under the influence of the very high localised stresses in the vicinity of the particles (2,3).This contribution presents part of a study of the Cu-Cr-SiO2 system where age hardening from the Cu-Cr and dispersion strengthening from Cu-Sio2 is combined.

Bright field and weak-beam images of dislocations gliding on (001) planes in F.C.C. metals

1978 ◽  
Vol 36 (1) ◽  
pp. 352-353
Author(s):  
H. P. Karnthaler ◽  
A. Korner
Keyword(s):  
Single Crystals ◽  
Dislocation Structure ◽  
Room Temperature ◽  
Stage Ii ◽  
Bright Field ◽  
Weak Beam ◽  
Standard Orientation

In f.c.c. metals slip is observed to occur generally on {111} planes. Glide dislocations on intersecting {111} planes can react with each other and form Lomer-Cottrell locks which lie along a <110> direction and are sessile since they are split on two {111} planes. Cottrell already pointed out that these dislocations could glide on {001} planes if they were not split. The first study of this phenomenon has been published recently. It is the purpose of this paper to report some interesting new details of the dislocations gliding on {001} planes in pure Ni, Cu, and Ag deformed at room temperature.Single crystals are grown with standard orientation and strained into stage II. The crystals are sliced parallel to the (001) planes. The dislocation structure is studied by TEM and the Burgers vectors ḇ and glide planes of the dislocations are determined unambiguously.In Fig.l primary P and secondary S dislocations react and form composite dislocations K.

Effect of trytophan as dopant on potassium acid phthalate single crystals

2019 ◽  
Author(s):  
Chem Int
Keyword(s):  
Single Crystals ◽  
Room Temperature ◽  
Visible Region ◽  
X Ray Diffraction ◽  
X Ray ◽  
Slow Evaporation Technique ◽  
Absorption Studies ◽  
Evaporation Technique ◽  
Potassium Acid Phthalate ◽  
Acid Phthalate

Optically transparent single crystals of potassium acid phthalate (KAP, 0.5 g) 0.05 g and 0.1 g (1 and 2 mol %) trytophan were grown in aqueous solution by slow evaporation technique at room temperature. Single crystal X- ray diffraction analysis confirmed the changes in the lattice parameters of the doped crystals. The presence of functional groups in the crystal lattice has been determined qualitatively by FTIR analysis. Optical absorption studies revealed that the doped crystals possess very low absorption in the entire visible region. The dielectric constant has been studied as a function of frequency for the doped crystals. The thermal stability was evaluated by TG-DSC analysis.

Room-temperature synthesis, growth mechanisms and opto-electronic properties of organic–inorganic halide perovskite CH3NH3PbX3 (X = I, Br, and Cl) single crystals

CrystEngComm ◽  
2021 ◽  
Author(s):  
Maryam Bari ◽  
Hua Wu ◽  
Alexei A. Bokov ◽  
Rana Faryad Ali ◽  
Hamel N. Tailor ◽  
...  
Keyword(s):  
Electronic Properties ◽  
Single Crystals ◽  
Room Temperature ◽  
Solubility Curve ◽  
Inverse Temperature ◽  
Growth Mechanisms ◽  
Temperature Synthesis ◽  
Room Temperature Synthesis ◽  
Halide Perovskite ◽  
Temperature Crystallization

Growth of MAPbX3 (X = I, Br, and Cl) single crystals by room temperature crystallization (RTC) method, and the crystallization pathway illustrated by the solubility curve of MAPbCl3 in DMSO, compared with inverse temperature crystallization (ITC) method.

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