scholarly journals Pengaruh Lama Penyulingan terhadap Rendemen dan Mutu Minyak Atsiri pada Biji Pala (Myristica fragrans Houtt)

2018 ◽  
Vol 11 (1) ◽  
pp. 50-58
Author(s):  
Fadillah Ramadhanti Rangkuti ◽  
Raida Agustina ◽  
Mustaqimah Mustaqimah ◽  
Mustafril Mustafril
Keyword(s):  
Refractive Index ◽  
Essential Oil ◽  
High Refractive Index ◽  
The Other ◽  
A Value ◽  
Myristica Fragrans ◽  
Weight Value ◽  
Myristica Fragrans Houtt ◽  
Index Value

Abstrak. Pala merupakan salah satu tanaman rempah yang menghasilkan minyak atsiri. Penelitian ini bertujuan untuk mengetahui pengaruh lama penyulingan terhadap rendemen dan mutu minyak biji pala. Variasi perlakuan yang digunakan adalah lama penyulingan yaitu 0-3 jam, 3-6 jam, 6-9 jam, 9-12 jam, 12-15 jam, 15-18 jam, 18-21 jam, 21-24 jam, 24-27 jam, dan 27-30 jam. Analisis karakteristik yang dilakukan meliputi rendemen, bobot jenis, indeks bias dan kelarutan dalam alkohol. Hasil penelitian yang telah dilakukan didapat rendemen minyak pala yang bervariasi, tergantung dari lama penyulingan. Pada jam ke 3 menghasilkan rendemen yang lebih besar dibandingkan dengan jam yang lain, dimana rendemen minyak pala pada jam ke 3 didapat sebesar 5,58 % sedangkan rendemen yang paling rendah terdapat pada jam ke 30 dengan hasil sebesar 0.12%. Berdasarkan hasil perhitungan rendemen kumulatif yang didapat dari range waktu 0-3, 3-6, 6-9, 9-12, 12-15, 15-18, 18-21, 21-24, 24-27, dan 27-30 adalah sebesar 10, 48 %. Nilai bobot jenis minyak pala yang diperoleh dari hasil penyulingan pada jam ke 24 menunjukkan angka yang lebih tinggi dibandingkan hasil yang lainnya dengan nilai 0,936 dan tidak memenuhi standar SNI. Sedangkan yang paling rendah terdapat pada jam ke 3 dengan nilai 0.872 yang juga tidak sesuai dengan standar SNI. Penyulingan dengan nilai bobot jenis yang sesuai dengan standar SNI terdapat pada jam ke 6 dengan nilai 0,902. Nilai indeks bias yang tinggi didapatkan pada jam ke 12- 15, 18-21, 21-24 dan 24- 27 dengan nilai 1,496 dan memenuhi standar SNI sedangkan pada jam ke 3-6 diperoleh nilai indeks bias sebesar 1,436 dan tidak memenuhi standar SNI. Tingkat kelarutan dalam alkohol 90% minyak pala yang dihasilkan dari 6 jam sampai 30 jam adalah sama, yaitu jernih yang diuji dengan perbandingan 1:3 dan sudah sesuai standar SNI sedangkan pada ke 3 jam hasilnya adalah opalisensi yaitu tidak keruh dan tidak jernih. Effect of Old Distillation on Rendemen and Quality of Essential Oils on Nutmeg (Myristica fragrans Houtt) Abstract. Nutmeg is one of the herbs that produce essential oil. This study aims to determine the effect of distillation on rendemen and quality of nutmeg oil. The variation of treatment used was the distillation time of 0-3 hours, 3-6 hours, 6-9 hours, 9-12 hours, 12-15 hours, 15-18 hours, 18-21 hours, 21-24 hours, 24- 27 hours, and 27-30 hours. Characteristic analyzes performed include rendemen, species weight, refractive index and solubility in alcohol. The results of the research have been obtained the yield of various nutmeg oil, depending on the length of distillation. At third hours it produces a higher yield compared to the other hour, where the yield of nutmeg oil at third hourswas5.58%, while the lowest yield was at 30thhours with a yield of 0.12%. Based on the results of cumulative rendemen calculations obtained from the range of time 0-3, 3-6, 6-9, 9-12, 12-15, 15-18, 18-21, 21-24, 24-27, and 27-30 was 10, 48%. The weight value of nutmeg oil obtained from the distillation at 24 hours indicates a higher rate than the other results with a value of 0.936 and didn't meet the SNI standard. While the lowest was at third hours with a value of 0.872 which was also not in accordance with SNI standards. Distillation with value of weight of type according to SNI standard is at 6th hours with value 0,902. High refractive index values were obtained at 12 to 15, 18-21, 21-24 and 24-27 hours with a value of 1.496 and met the SNI standard while at 3-6 hours the refractive index value was 1.436 and did not meet the SNI standard. The solubility rate in 90% alcohol of nutmeg oil produced from 6th hours to 30th hours is the same, that was clear tested with ratio of 1: 3 and was accordance with SNI standard while in 3 hours the result is opalisensi that is not cloudy and not clear.

scholarly journals Prediksi Kadar Air Bubuk Biji Kakao Menggunakan Nirs Dengan Metode PLS

2016 ◽  
Vol 1 (1) ◽  
pp. 1069-1076
Author(s):  
Hasmayani Hasmayani ◽  
Rita Khathir ◽  
Mustafril Mustafril
Keyword(s):  
Refractive Index ◽  
Essential Oil ◽  
Specific Gravity ◽  
Raw Materials ◽  
Raw Material ◽  
Yield And Quality ◽  
Fresh Material ◽  
Index Value ◽  
Red Ginger

Abstrak. Minyak atsiri jahe merah merupakan salah satu komoditas dari hasil budidaya jahe merah. Jenis minyak ini didapatkan dengan cara penyulingan jahe merah yang berumur sekitar 10 bulan hingga 1 tahun. Penelitian ini bertujuan untuk mengetahui kajian pengkondisian bahan baku terhadap rendemen dan mutu minyak atsiri yang dihasilkan dari penyulingan jahe merah. Pengkondisian bahan baku jahe merah dilakukan dengan 2 taraf yaitu jahe merah segar dan jahe merah yang dikeringanginkan selama 24 jam dengan 2 kali ulangan. Hasil penelitian menunjukkan bahwa rendemen  minyak atsiri dari penyulingan jahe merah segar diperoleh 0,0705%, sedangkan rendemen pada penyulingan jahe merah dikeringanginkan 0,0435%. Hasil Nilai indeks bias minyak atsiri  jahe merah segar diperoleh sebesar 1,4885 sedangkan nilai indeks bias jahe merah dikeringanginkan diperoleh sebesar 1,4885. Nilai  bobot jenis minyak atsiri pada penyulingan jahe merah segar diperoleh sebesar 0,90423 dan bobot jenis minyak atsiri jahe merah yang dikeringanginkan sebesar 0,89679. Kelarutan dalam alkohol minyak atsiri jahe merah segar dan jahe merah dikeringanginkan jernih pada perbandingan 1:5.The study of raw material conditioning to the quality of the red ginger essential oil Abstract. Red ginger essential oil is one commodity from the cultivation of red ginger. These types of oils obtained by distillation of red ginger have old after 10 months to 1 year cultivation. This study aimed to determine the effect of raw materials conditioning to the yield and quality of essential oils produced. The raw materials conditioning  red ginger is done with two levels i.e fresh red ginger and air-dried red ginger about  24 hours under 2 repeated. The results showed that the yield of essential oil obtained by distillation of fresh red gingerwas  0.0705%, while the yield on the distillation of air- dried red was ginger 0.0435%. Refractive index value of red ginger essential oil from fresh  material was 1.4885  while  the refractive index of air-dried red ginger driedwas 1.4885. Furthermore, the specific grafity of  at the distillation of fresh red ginger obtained at 0.90423 and the specific gravity of red ginger essential oil is dried at 0.89679. Solubility in alcohol red ginger essential oil of fresh and dried red gingerwere clearly at a ratio of 1: 5. 

Electronic and Optical Properties of Indium Selenide Nanosheet Using First-Principle Calculations

2019 ◽  
Vol 11 (11) ◽  
pp. 1148-1154
Author(s):  
Hamza A. Mezerh ◽  
Kadhim J. Kadhim ◽  
Hamad Rahman Jappor
Keyword(s):  
Refractive Index ◽  
Optical Properties ◽  
Density Functional ◽  
Visible Region ◽  
High Refractive Index ◽  
Indium Selenide ◽  
Experimental Investigations ◽  
Ultraviolet Region ◽  
Electronic And Optical Properties ◽  
Index Value

Density functional theory (DFT) have been used to examine the electronic and optical, properties of two-dimensional (2D) indium selenide (InSe) nanosheet. Our calculations indicate that the energy band gap of InSe is indirect and equal to 1.53 eV. It can be seen that for the pristine case, the majority and minority density of state (DOS) are fully symmetric. The optical properties are considered up to 36 eV. Our results established that the absorption starts in the visible region, while the peaks in the ultraviolet region. The refractive index value is 1.84 at zero photon energy limit and increase to 2.31. The high refractive index allows this nanosheet to be utilized as an internal layer coating between the substrate and the ultraviolet absorbing layer. Additionally, we observed that the gained optical properties of InSe nanosheet are in the ultraviolet range and the results are significant. It is expected that from these calculations to provide useful information for further experimental investigations of InSe nanosheet.

scholarly journals Kinetic Degradation of Myristicin, Elemicin, and Safrole in Encapsulated Banda Nutmeg (Myristica fragrans Houtt) Oleoresin

2017 ◽  
Vol 14 (1) ◽  
pp. 43
Author(s):  
Dewi Amrih ◽  
Chusnul Hidayat ◽  
Pudji Hastuti
Keyword(s):  
Activation Energy ◽  
Physicochemical Properties ◽  
Spray Drying ◽  
Myristica Fragrans ◽  
Drying Techniques ◽  
Myristica Fragrans Houtt ◽  
Dark Glass ◽  
C 50 ◽  
Flavoring Agent

Spices, in the form of oleoresin, have advantages as a flavoring agent. Nutmeg oleoresin compounds that play an important role in the formation of nutmeg flavor are myristicin, elemicin, and safrole. These compounds are not stable, so that the quality of oleoresin decreased easily. An alternative to overcome this problem is the encapsulation of oleoresin using spray drying techniques. The objective of this research was to evaluate the physicochemical properties of oleoresin with respect to the degradation of myristicin, elemicin, and safrole of nutmeg oleoresin. Microencapsulated nutmeg oleoresin was prepared using 12% WPC and 88% maltodextrin as encapsulate materials. It was stored in dark glass bottles at a various temperature, namely 30°C, 40°C, 50°C, 60°C, and 70°C, for 0, 4, 7, 10, 14, 21, 28, 35, 42, 49, 56 and 63 days. The content of myristicin, elemicin, and safrole were analysed. The results showed that myristicin, elemicin, and safrole in the encapsulated nutmeg oleoresin decreased during the storage until 28 days of storage and then they were relatively stable until 63 days. The activation energy of myristicin, elemicin, and safrole were 2.21 kJ/mol.K, 2.71 kJ/mol.K and 3.22 kJ/mol.K, respectively.

scholarly journals Utilization of Nutmeg (Myristica fragrans Houtt.) Seed Hydrodistillation Time to Produce Essential Oil Fractions with Varied Compositions and Pharmacological Effects

Molecules ◽  
2020 ◽  
Vol 25 (3) ◽  
pp. 565 ◽  
Author(s):  
Mohamed A. Ibrahim ◽  
Charles L. Cantrell ◽  
Ekaterina A. Jeliazkova ◽  
Tess Astatkie ◽  
Valtcho D. Zheljazkov
Keyword(s):  
Plasmodium Falciparum ◽  
Essential Oil ◽  
Seed Oil ◽  
Antimalarial Activity ◽  
Chemical Compositions ◽  
Pharmacological Effects ◽  
Substantial Variation ◽  
Myristica Fragrans ◽  
Oil Fractions ◽  
Myristica Fragrans Houtt

The intent of this study was to utilize distillation timeframes (DT) of nutmeg (Myristica fragrans) essential oil (EO) to generate fractions with differential chemical compositions and bioactivity. Ten fractions were captured at the following distillation timeframes: 0.0–0.5, 0.5–1.0, 1.0–2.5, 2.5–5.0, 5.0–10, 10–30, 30–60, 60–90, 90–120, and 120–240 min. In addition, a control EO was collected from a straight 0–240 min non-stop distillation. ANOVA and advanced regression modeling revealed that the produced EO fractions possess substantial variation in the concentration of potentially desired compounds. The concentrations (%) of α-phellandrene, 3-carene, p-cymene, limonene, α-thujene, α-pinene, camphene, sabinene, β-pinene, and myrcene decreased, while the concentrations (%) of α-terpinene, γ-terpinene, terpinolene, and myristicin increased in later DT fractions. Nutmeg EO showed some antimalarial activity against Plasmodium falciparum D6, but did not exhibit significant antifungal activity. In general, nutmeg seed oil yields increased with an increase of DT. These results may be utilized by industries using nutmeg EO.

scholarly journals Larvicidal Activity of Essential Oils from the Leaves and Fruits of Nutmeg (Myristica fragrans Houtt) Against Aedes aegypti (Diptera: Culicidae)

2016 ◽  
Vol 4 (7) ◽  
pp. 552
Author(s):  
Anne Carolina ◽  
Maman Maman
Keyword(s):  
Essential Oil ◽  
Aedes Aegypti ◽  
Larvicidal Activity ◽  
Steam Distillation ◽  
Chemical Compounds ◽  
Chemical Components ◽  
Myristica Fragrans ◽  
Leaf Oil ◽  
Myristica Fragrans Houtt ◽  
Fruit Oil

The aim of this research was to examine the larvicidal activity of essential oil (EO) extracted from nutmeg (Myristica fragrans Houtt) leaves and fruits by steam distillation, and to analyze its chemical compounds. The EO yield of nutmeg leaves and fruits collected from the same tree was 0.66% and 0.30%, respectively. Larvicidal tests with the EO were carried out against Aedes aegypti (L.) (Diptera: Culicidae). The concentrations of nutmeg EO used for the larvicidal assay were 50, 100, 150, 200, and 250 μg/mL. The results showed that fruit oil was more toxic than the leaf oil. LC50 values of leaf and fruit EOs were 133.8 and 110.1 µg/mL, respectively. The chromatogram of GC-MS showed that the chemical components in nutmeg leaf and fruit EOs were dominated by α-pinene, sabinene, β-pinene, delta-3-carene, limonene, β-phellandrene, α-terpinolene, linalool, safrole, croweacin, and myristicin.

scholarly journals Pengaruh Ukuran Bahan terhadap Rendemen dan Kualitas Minyak Biji Pala (Myristica Fragrans Houtt) dengan Metode Soxhletasi

Jurnal MIPA ◽  
2018 ◽  
Vol 7 (1) ◽  
pp. 39
Author(s):  
Andika Saranaung ◽  
Meiske S. Sangi ◽  
Dewa G. Katja
Keyword(s):  
Seed Oil ◽  
Acid Number ◽  
Peroxide Number ◽  
Value Set ◽  
Myristica Fragrans ◽  
Myristica Fragrans Houtt

Indonesia merupakan salah satu negara yang mempunyai berbagai jenis tanaman yang dapat dimanfaatkan oleh manusia, salah satunya ialah tanaman rempah-rempah. Di antara rempah-rempah utama Indonesia, pala merupakan salah satu rempah-rempah yang cukup tinggi nilainya sehingga perlu dikembangkan pemanfaatannya. Tujuannya menentukan rendemen dan kualitas minyak biji pala 60 mesh, 40 mesh, dan 20 mesh yang diambil dari kabupaten kepulauan talaud dengan metode soxhletasi. Metode yang digunakan adalah soxhletasi dengan pelarut n-hexan. Kualitas minyak biji pala diperoleh dengan menguji bilangan asam, bilangan peroksida, bilangan ester, dan kelarutan dalam etanol 90%. Hasil yang diperoleh dengan soxhletasi minyak biji pala rendemennya adalah 60 mesh (39,61%), 40 mesh (37,52%), dan 20 mesh (28,09%). Bilangan asam 60 mesh (3,9777%), 40 mesh (3,8967%), dan 20 mesh (3,4928%). Bilangan peroksida 60 mesh (0,0114%), 40 mesh (0,0118%), dan 20 mesh (0,0149%). Bilangan ester 60 mesh (29,2059%), 40 mesh (30,0777%), dan 20 mesh (31,5288%), dan kelarutan dalam etanol 90% mendekati nilai yang ditetapkan SNI yaitu 1:1. Hasilnya menunjukkan bahwa rendemen minyak biji pala paling banyak adalah 60 mesh dan kualitas minyak terbaik adalah 20 mesh.Indonesia is a country which has various types of plants that can be utilized by humans one of plants is a spice plant. Among the main spices of Indonesia, nutmeg is one of the spices that is high enough value so that it needs to be developed utilization. The purpose of this research is to determine the rendemen and  its quality of nutmeg seed oil of 60 mesh, 40 mesh, and 20 mesh taken from talaud islands by soxhletasi method with n-hexan solvent. The quality of nutmeg seed oil obtained by testing acid number, peroxide number, ester number, and solubility in ethanol 90%. The results obtained with soxhletasi of nutmeg seed oil are 60 mesh (39,61%), 40 mesh (37,52%), and 20 mesh (28,09%). Acid numbers are 60 mesh (3,9777%), 40 mesh (3,8967%), and 20 mesh (3,4928%). Peroxide numbers are 60 mesh (0,0114%), 40 mesh (0,0118%), and 20 mesh (0,0149%). The ester numbers are 60 mesh (29,2059%), 40 mesh (30,0777%), and 20 mesh (31,5288%), and the solubility in ethanol is 90% close to the value set by the SNI that is 1:1. The results show that the rendement of 60 mesh nutmeg seed oil is most and the best quality oil is 20 mesh

scholarly journals The Diversity and Conservation Status of Snakes in Rawa Mekar Jaya, Riau, Indonesia

2021 ◽  
Vol 6 (2) ◽  
pp. 246-254
Author(s):  
Agung Purnomo Adjie ◽  
Sri Catur Setyawatiningsih
Keyword(s):  
Diversity Index ◽  
Conservation Status ◽  
Mangrove Ecosystem ◽  
Wildlife Habitat ◽  
The Other ◽  
Mangrove Area ◽  
Wiener Diversity Index ◽  
Index Value ◽  
Made In

Snakes in Mekar Jaya mangrove ecosystem have the potential be ecotourism objects. On the other hand ecotourism activities might reduce the quality of wildlife habitat, including that of the snake. This study aimed to determine the diversity and status of snake species in the mangrove ecosystem of Rawa Mekar Jaya. A transect of 20 x 50 m was made in three stations: rivers (S1), ecotourism route (S2), and dense mangroves (S3). The observation was carried out at low tide and repeated three times with a span of 2 days. Snake data was collected using the Visual Encounter Survey (VES) method. We revealed 59 snakes in the mangrove area of Rawa Mekar Jaya consisting of 3 species namely Boiga dendrophila, Cerberus rynchops, and Trimeresurus purpureomaculatus. B. dendrophila and C. rhyncops are mangrove specialists. The Shannon Wiener diversity index value (H ') for all observation stations is below one, so it is classified as low. All types of snakes found are not protected and classified as the least concern. C. rynchops is included in the CITES appendix III

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