scholarly journals Characterization of Flax and Hemp Using Spectrometric Methods

2021 ◽  
Vol 11 (18) ◽  
pp. 8341
Author(s):  
Luisa Andronie ◽  
Ioana Delia Pop ◽  
Rodica Sobolu ◽  
Zoriţa Diaconeasa ◽  
Alina Truţă ◽  
...  
Keyword(s):  
Antioxidant Capacity ◽  
Nutritional Value ◽  
Cannabis Sativa ◽  
Dry Weight ◽  
Linum Usitatissimum L ◽  
Protein Fiber ◽  
Ft Ir ◽  
Flax Seeds ◽  
Molecular Components

The comparison of the antioxidant activity of the studied seeds of fiber crop (hemp and flax) emphasized a hierarchy of antioxidant capacity. The purpose of the study was to investigate the antioxidant capacity and nutritional value of flax seeds (Linum usitatissimum L.) and hemp seeds (Cannabis sativa L.) in powder form. In this study, the FT-IR technique was utilized in order to detect molecular components in analyzed samples. Antioxidant capacity was evaluated with photochemical assay as well as humidity, protein, fiber, lipid and carbohydrate content. The FT-IR results reveal the presence of different bio-active compounds in hemp such as flavonoids, tannins, sugars, acids, proanthocyanidins, carotenoids and citric metabolites. The highest antioxidant capacity was observed in flax seeds, 18.32 ± 0.98, in comparison with hemp seeds, 4 ± 0.71 (μg/mg dry weight equivalent ascorbic acid). Regarding nutritional parameters, flax seeds showed the most increased content of protein, displaying average values of 534.08 ± 3.08, as well as 42.20 ± 0.89 of lipids and 27.30 ± 0.89 of fiber (g/100 g/sample). Hemp seeds showed the highest protein content of 33 ± 1.24 (g/100 g/sample).

scholarly journals Antioxidant Capacity of Several Romanian Forest Fruits (Rosa canina L., Prunus spinosa L., Vaccium vitis-idaea L. and Cornus mas L.)

2019 ◽  
Vol 47 (4) ◽  
pp. 1178-1184
Author(s):  
Luisa ANDRONIE ◽  
Liviu HOLONEC ◽  
Ioana POP ◽  
Alina M. TRUTA ◽  
Antonia ODAGIU ◽  
...  
Keyword(s):  
Antioxidant Capacity ◽  
Nutritional Value ◽  
Digital Object Identifier ◽  
Rosa Canina ◽  
Cornelian Cherry ◽  
Cornus Mas ◽  
Ft Ir ◽  
Molecular Components ◽  
Molecular Compounds ◽  
Ft Ir Spectroscopy

The comparison of the antioxidant activity of the studied forest fruits emphasized a hierarchy of the antioxidant capacity in rosehip, blackthorn, lingonberry and cornelian cherry. The purpose of the study was to investigate the antioxidant capacity and nutritional value of rosehip, blackthorn, lingonberry and cornelian cherry. In the current study, the FT-IR spectroscopy technique was applied to detect molecular components in forest fruits samples. Antioxidant capacity was evaluated with photochemical assay as well as humidity, protein, fibre, lipid and carbohydrate content. The FT-IR results revealed the presence of different bio-active compounds in berries such as flavonoids, tannins, sugars, acids, proanthocyanidins, carotenoids, citric metabolites and others. The highest antioxidant capacity was observed in rosehip 105.67±1.38 and blackthorn 49.89±1.92 (μg/mg equivalent ascorbic acid). Regarding nutritional parameters, rosehip showed the most increased content of protein displaying average values of 1.60, carbohydrates 38.20 and fibre 24.10 (g/100 g/sample). These results can provide useful information providing a research interest for the identification of new molecular compounds from Romanian flora samples.   ********* In press - Online First. Article has been peer reviewed, accepted for publication and published online without pagination. It will receive pagination when the issue will be ready for publishing as a complete number (Volume 47, Issue 4, 2019). The article is searchable and citable by Digital Object Identifier (DOI). DOI link will become active after the article will be included in the complete issue. *********    

scholarly journals Green Synthesis, Characterization, and Antibacterial Properties of Silver Nanoparticles Obtained by Using Diverse Varieties of Cannabis sativa Leaf Extracts

Molecules ◽  
2021 ◽  
Vol 26 (13) ◽  
pp. 4041
Author(s):  
Adriana Cecilia Csakvari ◽  
Cristian Moisa ◽  
Dana G. Radu ◽  
Leonard M. Olariu ◽  
Andreea I. Lupitu ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Green Synthesis ◽  
Antioxidant Capacity ◽  
Cannabis Sativa ◽  
Antibacterial Properties ◽  
Green Building ◽  
Human Pathogens ◽  
Leaf Extracts ◽  
Vis Spectroscopy ◽  
Ft Ir

Cannabis sativa L. (hemp) is a plant used in the textile industry and green building material industry, as well as for the phytoremediation of soil, medical treatments, and supplementary food products. The synergistic effect of terpenes, flavonoids, and cannabinoids in hemp extracts may mediate the biogenic synthesis of metal nanoparticles. In this study, the chemical composition of aqueous leaf extracts of three varieties of Romanian hemp (two monoecious, and one dioecious) have been determined by Fourier-Transformed Infrared spectroscopy (FT-IR), high-performance liquid chromatography, and mass spectrometry (UHPLC-DAD-MS). Then, their capability to mediate the green synthesis of silver nanoparticles (AgNPs) and their pottential antibacterial applications were evaluated. The average antioxidant capacity of the extracts had 18.4 ± 3.9% inhibition determined by 2,2-diphenyl-1-picrylhydrazyl (DPPH•) and 78.2 ± 4.1% determined by 2,2′-azino-bis (3-ethylbenzothiazoline-6-sulfonic acid) diammonium salt (ABTS™) assays. The total polyphenolic content of the extracts was 1642 ± 32 mg gallic acid equivalent (GAE) L−1. After this, these extracts were reacted with an aqueous solution of AgNO3 resulting in AgNPs, which were characterized by UV−VIS spectroscopy, FT-IR, scanning electron microscopy (SEM-EDX), and dynamic light scattering (DLS). The results demonstrated obtaining spherical, stable AgNPs with a diameter of less than 69 nm and an absorbance peak at 435 nm. The mixture of extracts and AgNPs showed a superior antioxidant capacity of 2.3 ± 0.4% inhibition determined by the DPPH• assay, 88.5 ± 0.9% inhibition as determined by the ABTS•+ assay, and a good antibacterial activity against several human pathogens: Escherichia coli, Klebsiella pneumoniae, Pseudomonas fluorescens, and Staphylococcus aureus.

Characterization of Hemp (Cannabis sativa L.) Biodiesel Blends with Euro Diesel, Butanol and Diethyl Ether Using FT-IR, UV–Vis, TGA and DSC Techniques

2018 ◽  
Vol 11 (3) ◽  
pp. 1097-1113 ◽  
Author(s):  
M. N. Mohammed ◽  
A. E. Atabani ◽  
Gediz Uguz ◽  
Chyi-How Lay ◽  
Gopalakrishnan Kumar ◽  
...  
Keyword(s):  
Diethyl Ether ◽  
Cannabis Sativa ◽  
Biodiesel Blends ◽  
Ft Ir ◽  
Tga And Dsc

scholarly journals Extraction and Characterization of Sugarcane Peel Wax

ISRN Agronomy ◽  
2012 ◽  
Vol 2012 ◽  
pp. 1-6 ◽  
Author(s):  
Mangesh B. Inarkar ◽  
S. S. Lele
Keyword(s):  
Fatty Acids ◽  
Molecular Weight ◽  
Gas Chromatography ◽  
Fourier Transform ◽  
Dry Weight ◽  
Weight Basis ◽  
Ft Ir ◽  
Gas Chromatography Mass Spectroscopy ◽  
Layer Chromatography

Sugarcane peel is an agrowaste product and contains considerable amount of wax. This has a good technoeconomic potential. In view of this, the present study aims at extraction and characterization of wax from sugarcane peel. The yield of crude wax was 0.95% on dry weight basis. During Fourier transform-infrared spectroscopy (FT-IR) prominent peaks obtained at 2921.73 and 2851.64 (–CH), 1463.44 (–CH2), 1376.96 (–CH3), 1108.4 and 1170.16 (–C–O) 3395.60 (–OH), 1710.25 (–CHO), and 1736.63 (–COOH) indicate presence of alkanes, ketones, alcohols, aldehydes, and carboxylic acids, respectively. Alcohol and hydrocarbon fractions were also found by thin layer chromatography (TLC). Melting point of crude wax was observed to be 62.1°C. Molecular weight of wax was estimated to be 1706 Dalton. Composition of crude wax found using gas chromatography-mass spectroscopy (GC-MS) was alkanes (28.83%), ester (66.26%), fatty acids (4.58%), aldehyde (0.11%), and alcohol (0.22%).

scholarly journals Agro-morphological characterization of flax (Linum usitatissimum L.) accessions at north-western part of Bangladesh

2020 ◽  
Vol 5 (4) ◽  
pp. 465-469
Author(s):  
A.K.M. Golam Sarwar ◽  
Md. Eakramul Haque ◽  
Most. Morshada Khatun ◽  
Md. Sabibul Haque
Keyword(s):  
Linum Usitatissimum ◽  
Agricultural Research ◽  
Block Design ◽  
Morphological Characterization ◽  
Growth And Yield ◽  
Research Station ◽  
Agricultural Crop ◽  
Linum Usitatissimum L ◽  
Flax Seeds

Flax (Linum usitatissimum L.), grown throughout the world for millennia. It is a multipurpose agricultural crop that can provide food, fuel and fibre. An agro-morphological characterization based on 13 traits of 26 flax accessions was carried out during the Rabi season 2017-2018 at the Agricultural Research Station, Bangladesh Agricultural Research Institute, Rangpur. The field experiment was laid out in a randomized completed block design having four replications. Flax seeds were sown in 3.0 m × 0.6 m plot with continuous line sowing (two lines). The seed germination (%) and vigour indices of all flax accessions varied from 44.1 – 77.7 and 44.1 – 119.4, respectively. A significant variation in all growth and yield attributing descriptors was observed except 1000-seed weight of flax. Among the accessions, BD-10708 possessed the highest seed yield (182.9 g plant–1) and yield attributing descriptors viz., number of capsules plant–1 (142) and seeds plant–1 (513) of flax. The performance of the local accesson Ulipur was observed poor compared to some of the test accessions of flax. Some of these flax accessions could be used as breeding materials in varietal developmental and improvement programmes with higher yield potentials of flax in Bangladesh.

Cultivar, sowing date and plant density studies of fibre hemp (Cannabis sativa L.) in Tasmania

2000 ◽  
Vol 40 (7) ◽  
pp. 975 ◽  
Author(s):  
S. N. Lisson ◽  
N. J. Mendham
Keyword(s):  
Plant Density ◽  
Cannabis Sativa ◽  
Initial Density ◽  
Dry Weight ◽  
Sowing Date ◽  
Planting Density ◽  
North West ◽  
Linum Usitatissimum L ◽  
Short Period ◽  
Final Harvest

This paper reports on a 3-year agronomic study into fibre hemp (Cannabis sativa L.) conducted in Tasmania, Australia. The performance of selected hemp cultivars, and the responses to sowing date and plant density were investigated as part of a broad feasibility study to assess the potential of fibre hemp and flax (Linum usitatissimum L.) as sources of fibre for the Australian newsprint industry. Trials were conducted at separate sites in north-west and south-east Tasmania. Nine cultivars from the Ukraine, Hungary and France were examined in 2 separate trials. The Hungarian cultivars, Kompolti and Unico B, and the French cultivar Futura 77 had the highest single plot dry stem yields (up to 1500 g/m 2 ) and bark proportions (up to 40%). All the cultivars flowered toward the end of January, suggesting that the growing season in Tasmania could accommodate much later flowering and potentially higher yielding genotypes. Levels of the psychoactive agent, delta-9-tetrahydrocannabinol were consistently below the legal maximum of 0.35% (dry weight basis). Three sowing date trials were conducted across 2 seasons incorporating dates between mid September and mid November and a single autumn planting at the end of May. Interactions with cultivar and planting density were also considered. Stem and bark yield declined with delays in sowing after early–mid October in response to a decline in calendar days and thermal time from sowing to flowering. The response was most pronounced in sowings of Kompolti, which flowered within a short period and differed more substantially in durations to flowering. Earlier sowings were limited by premature flowering in response to shorter daylengths and by poor drainage at one of the 2 trial sites. The success of early sowings in Tasmania would appear to depend on finding cultivars less sensitive tophotoperiod, and cultivation on well drained sites. A further trial was conducted to investigate the influence of plant density on hemp yields. Treatments included densities from 50 to 300 plants/m 2 . Plant density declined with crop growth across all treatments and was most pronounced for populations of 200 and 300 plants/m 2 . Final harvest stem yield responded in a parabolic manner to plant density, with maximum yields at about 110 plants/m 2 . Differences in the percentage of the long, high quality bark fibre at final harvest were generally small and not significant. However, regression analysis of the response of bark percentage suggested a linear decline with increasing initial density.

scholarly journals Production and Characterization of a Novel Low-Sugar Beverage from Red Jujube Fruits and Bamboo Shoots Fermented with Selected Lactiplantibacillus plantarum

Foods ◽  
2021 ◽  
Vol 10 (7) ◽  
pp. 1439
Author(s):  
Chu-Min Zhao ◽  
Ting Du ◽  
Ping Li ◽  
Xin-Jun Du ◽  
Shuo Wang
Keyword(s):  
Antioxidant Capacity ◽  
Nutritional Value ◽  
Ph Value ◽  
Raw Materials ◽  
High Yield ◽  
Total Phenolic ◽  
Fermentation Products ◽  
Bamboo Shoots ◽  
Different Strains

Red jujube fruits and bamboo shoots are rich in many nutrients and have the advantage of high yield in China. However, the storage of fresh fruits is difficult, and there are no fermented products using both as raw materials. In order to develop the two raw materials into novel products and improve their nutritional value, this study reports the production and characterization of a beverage via fermentation of red jujube fruits and bamboo shoots with Lactiplantibacillus plantarum. L. plantarum TUST-232 was selected as the starter from several different strains by comparing pH value and the number of viable cells, which reached 8.91 log CFU/mL in the beverage fermented for 14 h at 37 °C with 0.3% inoculation. After fermentation, the beverage showed improvement in the contents of several nutrients and antioxidant indices, with a decrease of 44.10% in sucrose content, along with increases of 11.09%, 12.30%, and 59.80% in total phenolic content, total antioxidant capacity, and superoxide anion scavenging ability, respectively. These results indicate that L. plantarum fermentation of red jujube fruits and bamboo shoots could be an effective way to develop a new beverage with high nutritional value, high antioxidant capacity, and high dietary fiber content. This research provided experimental support for the development of new fermentation products with the functions of improving health and body functions.

scholarly journals Comparative FT-IR Prospecting for Cellulose in Stems of Some Fiber Plants: Flax, Velvet Leaf, Hemp and Jute

2021 ◽  
Vol 11 (18) ◽  
pp. 8570
Author(s):  
Rodica Vârban ◽  
Ioana Crișan ◽  
Dan Vârban ◽  
Andreea Ona ◽  
Loredana Olar ◽  
...  
Keyword(s):  
Cannabis Sativa ◽  
Raw Materials ◽  
Screening Method ◽  
Qualitative Assessment ◽  
Crystalline Region ◽  
Plant Fibers ◽  
Practical Applications ◽  
Extraction Procedures ◽  
Ft Ir

Plant fibers are sustainable sources of materials for many industries, and can be obtained from a variety of plants. Cellulose is the main constituent of plant-based fibers, and its properties give the characteristics of the fibers obtained. Detailed characterization of cellulosic fibers is often performed after lengthy extraction procedures, while fast screening might bring the benefit of quick qualitative assessment of unprocessed stems. The aim of this research was to define some marker spectral regions that could serve for fast, preliminary qualitative characterization of unprocessed stems from some textile plants through a practical and minimally invasive method without lengthy extraction procedures. This could serve as a screening method for sorting raw materials by providing an accurate overall fingerprint of chemical composition. For this purpose, we conducted comparative Fourier Transform Infrared Spectroscopy (FT-IR) prospecting for quality markers in stems of flax (Linum usitatissimum L.), velvet leaf (Abutilon theophrasti Medik.), hemp (Cannabis sativa L.) and jute (Corchorus olitorius L.). Analysis confirmed the presence of major components in the stems of the studied plants. Fingerprint regions for cellulose signals were attributed to bands at 1420–1428 cm−1 assigned to the crystalline region and 896–898 cm−1 assigned to the amorphous region of cellulose. The optimization of characterization methods for raw materials is important and can find immediate practical applications.

scholarly journals Morphological and Nutritional Properties of Moroccan Capparis spinosa Seeds

2019 ◽  
Vol 2019 ◽  
pp. 1-8 ◽  
Author(s):  
Nidal El amri ◽  
Faouzi Errachidi ◽  
Abdellatif Bour ◽  
Sara Bouhaddaoui ◽  
Rachida Chabir
Keyword(s):  
Nutritional Value ◽  
Geometric Mean ◽  
Morphological Characteristics ◽  
Dry Weight ◽  
Morphological Properties ◽  
Nutritional Properties ◽  
Capparis Spinosa ◽  
Length Width ◽  
High Level

Capparis spinosa is one of the few shrub species which has so many qualities with many uses. In this case, the present work aimed to study both some morphological characteristics and biochemical components (proteins, lipids, and carotenoids) of fresh C. spinosa seeds with three different sizes, collected from two Moroccan regions. In this study, C. spinosa seeds present a total of proteins ranging from 23.32 to 28.5% on a dry weight basis. Additionally, the total lipids varied between 2.8 and 3.4%. C. spinosa seeds contained a high level of carotenoids. Besides, the analytical values have been variously affected by both size and location. Further, the preliminary morphological and anatomical characterization of leaves, stems, and morphological properties such as length, width, thickness, geometric mean diameter, sphericity, surface area, and mass of 100 seeds have been determined. Consequently, this present study confirms the importance of Moroccan C. spinosa seeds, which represent a significant nutritional value. Also, its good morphological quality is a significant indicator of commercial criteria.

Characterization of frozen hydrated biological specimens by low-loss EELS

1992 ◽  
Vol 50 (2) ◽  
pp. 1572-1573
Author(s):  
Songquan Sun ◽  
Richard D. Leapman
Keyword(s):  
Water Content ◽  
Direct Method ◽  
Internal Standard ◽  
Dry Weight ◽  
Dark Field ◽  
Protein Solutions ◽  
Subcellular Compartment ◽  
Differential Shrinkage ◽  
Electron Energy Loss

Analyses of ultrathin cryosections are generally performed after freeze-drying because the presence of water renders the specimens highly susceptible to radiation damage. The water content of a subcellular compartment is an important quantity that must be known, for example, to convert the dry weight concentrations of ions to the physiologically more relevant molar concentrations. Water content can be determined indirectly from dark-field mass measurements provided that there is no differential shrinkage between compartments and that there exists a suitable internal standard. The potential advantage of a more direct method for measuring water has led us to explore the use of electron energy loss spectroscopy (EELS) for characterizing biological specimens in their frozen hydrated state.We have obtained preliminary EELS measurements from pure amorphous ice and from cryosectioned frozen protein solutions. The specimens were cryotransfered into a VG-HB501 field-emission STEM equipped with a 666 Gatan parallel-detection spectrometer and analyzed at approximately −160 C.

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